CVD Reactor Cleaning via Thermal Response Monitoring

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Solution Overview

Problem

Current methods for removing parasitic depositions from CVD reactor process chambers are inefficient, leading to increased costs and reduced component lifespan due to prolonged etching cycles, which are not adequately controlled to ensure complete removal without over-processing.

Innovation Solution

Monitoring the thermal response of components within or near the process chamber, using temperature measurements to determine when parasitic coatings are sufficiently removed by comparing measured values with predetermined comparison values, allowing for precise termination of the etching process, and employing a temperature control system to maintain a constant heat output or emissivity-based feedback for optimal cleaning.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If the etching gas is supplied for a specified time in multiple successive phases to remove parasitic depositions, then the cleaning process can be completed, but the etching cycles are prolonged leading to increased costs and reduced component lifespan

Engineering Contradiction:
Improvecomplete removal of parasitic depositionsVSAvoidetching cycle time
Core Design Contradiction:
ReliabilityVSDuration of action of moving object

Solution Approach 1:

The patent employs a sensor to monitor the thermal response of the susceptor in real-time during the etching process. The measured temperature values are fed back to the control device, which automatically adjusts or terminates the etching gas supply when the susceptor temperature reaches a predetermined threshold, eliminating the need for fixed-duration etching cycles and preventing over-processing.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The invention changes the control parameter from fixed time duration to temperature-based threshold control. By monitoring the thermal response (temperature) of the susceptor and comparing it against a predetermined comparison value, the etching process is dynamically adjusted to achieve complete cleaning while minimizing cycle time and avoiding component damage.

Inventive Principle:
Principle #35Parameter changes

2Reliability

If the etching cycles are extended to ensure complete removal of parasitic depositions, then cleaning effectiveness is improved, but component lifespan is reduced due to over-processing

Engineering Contradiction:
Improvecleaning effectivenessVSAvoidcomponent lifespan
Core Design Contradiction:
ReliabilityVSDuration of action of stationary object

Solution Approach 1:

The control device continuously monitors the thermal response of the susceptor and automatically terminates the etching gas supply when the predetermined temperature threshold is reached. This feedback mechanism ensures that etching stops at the optimal point, preventing over-processing that would reduce component lifespan while maintaining effective removal of parasitic depositions.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The patent applies etching gas only until the temperature threshold is reached, rather than using fixed extended cycles. This partial action approach provides just enough etching to remove parasitic depositions completely without excessive exposure that would damage components, thereby extending component lifespan while maintaining cleaning effectiveness.

Inventive Principle:
Principle #16Partial or excessive action

3Ease of operation

If fixed-duration etching cycles are used, then the process control is simple, but the costs increase due to prolonged etching and reduced component lifespan

Engineering Contradiction:
Improveprocess control simplicityVSAvoidetching process costs
Core Design Contradiction:
Ease of operationVSLoss of energy

Solution Approach 1:

The control device automatically monitors temperature and manages the etching gas supply based on real-time thermal response data. This automated feedback system maintains operational simplicity while eliminating wasteful prolonged etching cycles, thereby reducing energy consumption and associated costs without requiring complex manual intervention.

Inventive Principle:
Principle #23Feedback

4Reliability

If multiple successive etching phases are executed for specified time, then parasitic depositions are removed, but productivity is reduced due to prolonged processing time

Engineering Contradiction:
Improveparasitic deposition removalVSAvoidprocessing throughput
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

The invention changes the control parameter from fixed time duration to temperature-based threshold control. By monitoring the thermal response of the susceptor and terminating etching when the predetermined temperature is reached, the process achieves complete parasitic deposition removal in shorter time, thereby increasing processing throughput and productivity.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach ensures the etching cycle is of sufficient length to remove parasitic depositions effectively while preventing over-processing, thereby reducing costs and extending the life of components by precisely controlling the etching process based on thermal feedback.

Implementation Method 1

a susceptor that can be heated by a heating device

Methodology Applied
Scientific EffectHeating: Heating

Implementation Method 2

a heating device for the heating of the susceptor

Methodology Applied
Scientific EffectThermal conduction: Conduction (thermal)

Implementation Method 3

measured values are obtained by monitoring a thermal response of at least one object in, or in the region near, the process chamber

Methodology Applied
Scientific EffectThermal radiation: Thermal Radiation

Implementation Method 4

an etching gas, which can contain chlorine, or can be chlorine, is supplied into the process chamber... to remove carbon residues

Methodology Applied
Scientific EffectChemical etching: Chemical Bonding

Implementation Method 5

in the course of the supply of the etching gas, a temperature control body is regulated to a specified temperature, or is heated with a constant heat output

Methodology Applied
Scientific EffectThermal regulation: Heating

Data Source

PatentUS20230160062A1Method for ascertaining the end of a cleaning process for a process chamber of a mocvd reactor
Publication Date: 2023.05.25 AIXTRON AG
  • US20230160062A1 patent drawing
  • US20230160062A1 patent drawing
  • US20230160062A1 patent drawing

AI summary

In a cleaning process for removing parasitic depositions on surfaces of a process chamber of a CVD reactor, a susceptor of the CVD reactor is heated by a heating device, and the susceptor is regulated to a specified temperature or is heated with a constant heat output. Concurrently, an etching gas is supplied to the heated process chamber. The thermal response of at least one object is monitored, in which the thermal response is the temperature of the wide face of a process chamber cover, the wide face facing away from the process chamber. The parasitic depositions influence the emissivity of the surface of the process chamber cover, the emissivity influencing the temperature distribution in the process chamber. The supply of etching gas is terminated when the temperature reaches a comparison value, the temperature changing in response to changes in the surface emissivity during the cleaning process.