CVI/CVD Reactor with Alternating Gas Inlets

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Solution Overview

Problem

Conventional CVI/CVD reactors result in non-uniform matrix densification due to uneven gas distribution, requiring frequent rearrangement of porous structures to achieve uniformity.

Innovation Solution

A CVI/CVD reactor design with alternating gas feed through opposite inlets and a thermal gradient, reversing gas flow direction multiple times to ensure uniform reactant gas availability across the reactor chamber.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Device complexity

If reactant gas is provided through a single inlet at one end of the reactor chamber, then the gas flow path is simple, but non-uniform matrix densification occurs due to precursor gas consumption near the inlet

Engineering Contradiction:
Improvereactor structureVSAvoidmatrix densification uniformity
Core Design Contradiction:
Device complexityVSManufacturing precision

Solution Approach 1:

The reactor chamber is segmented into multiple zones with separate gas inlets positioned at different locations. This allows reactant gas to be introduced at multiple points simultaneously, creating overlapping flow patterns that ensure uniform precursor gas distribution throughout the chamber and prevent localized depletion near any single inlet.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Different regions of the reactor chamber are provided with tailored gas flow characteristics through strategically positioned inlets. The gas flow rate and distribution are optimized for each local region to account for variations in preform positioning and consumption rates, ensuring uniform matrix densification across the entire chamber.

Inventive Principle:
Principle #3Local quality

2Manufacturing precision

If porous structures are rearranged multiple times during the CVI/CVD process, then uniform matrix densification can be achieved, but manufacturing time and operational complexity increase

Engineering Contradiction:
Improvematrix densification uniformityVSAvoidmanufacturing efficiency
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The reactor is pre-configured with multiple gas inlets positioned to create optimal flow patterns from the start of the process. This preliminary design eliminates the need for subsequent rearrangement of porous structures, as the gas distribution system is already optimized to provide uniform precursor gas availability throughout the chamber for the entire duration of the CVI/CVD process.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The gas flow system is designed to be dynamically adjustable, allowing flow rates through different inlets to be modified during the process. This enables compensation for any developing non-uniformities without requiring physical rearrangement of the porous structures, maintaining both uniformity and productivity.

Inventive Principle:
Principle #15Dynamics

3Speed

If reactant gas diffuses into porous structures positioned nearest the gas inlet, then infiltration occurs efficiently at that location, but less reactant gas remains available for structures near the outlet

Engineering Contradiction:
Improveinfiltration rateVSAvoidreactant gas availability
Core Design Contradiction:
SpeedVSQuantity of substance

Solution Approach 1:

The gas supply system is divided into multiple independent inlet channels positioned at different locations along the reactor chamber. Each inlet supplies reactant gas to its local region, creating multiple independent infiltration zones. This segmentation ensures that precursor gas is replenished continuously at each location, preventing depletion effects that would occur in a single-inlet configuration.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The multiple inlet configuration creates equipotential conditions for reactant gas availability throughout the reactor chamber. By positioning inlets to ensure uniform distribution, the system equalizes the chemical potential of precursor gas across different locations, ensuring that all porous structures receive adequate reactant gas regardless of their position in the flow path.

Inventive Principle:
Principle #12Equipotentiality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach promotes uniform infiltration and densification of fibrous preforms, reducing the need for structure rearrangement and enhancing manufacturing efficiency by maintaining uniform gas distribution and reaction conditions.

Implementation Method 1

CVI/CVD is a known process for making composite structures including ceramic matrix composites. The reactant gas diffuses into one or more porous structures positioned in the reactor chamber and undergoes a reaction to form a matrix material.

Methodology Applied
Scientific EffectChemical vapor deposition: Chemical Vapour Deposition

Implementation Method 2

A CVI/CVD reactor design with alternating gas feed through opposite inlets and a thermal gradient, reversing gas flow direction multiple times to ensure uniform reactant gas availability across the reactor chamber.

Methodology Applied
Scientific EffectThermal gradient: Temperature Gradient

Data Source

PatentEP3653749B1CVI/CVD matrix densification process and apparatus
Publication Date: 2023.12.27 RTX CORP
  • EP3653749B1 patent drawingFigure 1
  • EP3653749B1 patent drawingFigure 2
  • EP3653749B1 patent drawingFigure 3

AI summary

A chemical vapor infiltration and deposition (CVI/CVD) reactor assembly (10) includes a CVI/CVD reactor (12) and a reactant gas feed source (48). The CVI/CVD reactor (12) includes a first inlet (14) at a first end of the CVI/CVD reactor (12), a second inlet (16) at a second end of the CVI/CVD reactor (12) opposite the first end, a first outlet (18) at the second end, a second outlet (20) at the first end, and a chamber (22) in fluid communication with the first and second inlets (14, 16) and first and second outlets (18, 20) and configured to hold a substrate (80). The reactant gas feed source (48) is interchangeably and fluidly connected to the first and second inlets (14, 16) by first and second valved gas lines (54, 56), respectively.