Cycling Valves for Precise Gas Flow Control in Beam Processing

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Solution Overview

Problem

Existing gas injection systems for beam processing systems have limited control over gas flow and pressure in the sample chamber, requiring frequent refilling, coarse flow control, and safety concerns due to hazardous chemicals, with limited ability to maintain precise ratios of process gases.

Innovation Solution

The implementation of cycling valves for each gas source, with microvalves positioned inside the vacuum chamber for rapid response, and gas sources external to the vacuum system for easy connection and disconnection, allowing precise control of gas flow by adjusting the duty cycle and frequency of the valves, eliminating the need for flow-limiting apertures and enabling rapid pressure control.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If a crucible with plunger valve is used to store and deliver precursor gas, then gas flow can be controlled by heat and valve positioning, but the crucible requires frequent refilling and realignment, and safety equipment is needed for hazardous chemicals

Engineering Contradiction:
Improveprecursor gas supplyVSAvoidrefilling frequency
Core Design Contradiction:
Quantity of substanceVSLoss of time

Solution Approach 1:

The gas delivery system is segmented into multiple independent gas sources, each with its own cycling valve, rather than using a single crucible. This allows continuous operation as one source can be refilled while others are in use, eliminating downtime and frequent interruptions.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The precursor gas sources are extracted from the vacuum chamber and placed outside in a cabinet. This eliminates the need for frequent refilling operations inside the vacuum chamber and allows safe handling of hazardous chemicals outside the beam path.

Inventive Principle:
Principle #2Taking out (Extraction)

2Ease of operation

If a diaphragm valve with stepper motor is used to control gas flow, then flow rate can be adjusted, but the control is coarse and pressure regulation is limited

Engineering Contradiction:
Improveflow controlVSAvoidpressure control precision
Core Design Contradiction:
Ease of operationVSManufacturing precision

Solution Approach 1:

The system uses cycling valves that dynamically adjust gas flow by varying the duty cycle (percentage of time valve is open) and frequency of operation. This provides continuous, precise control over gas flow rates and chamber pressure, replacing the coarse static control of traditional diaphragm valves.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The valve operation parameters (duty cycle and frequency) are changed to precisely control gas flow. By adjusting these parameters, the system achieves fine control over precursor gas delivery and chamber pressure, enabling precise process control.

Inventive Principle:
Principle #35Parameter changes

3Stress or pressure

If flow-limiting apertures are used to maintain low pressure in the sample chamber, then pressure control is achieved, but the time to bring the chamber up to operating pressure increases

Engineering Contradiction:
Improvechamber pressureVSAvoidpressure ramp-up time
Core Design Contradiction:
Stress or pressureVSLoss of time

Solution Approach 1:

The cycling valves provide dynamic control of gas flow into the chamber, allowing rapid adjustment of flow rates. This eliminates the need for fixed flow-limiting apertures and enables quick pressure ramp-up when needed, while maintaining precise pressure control during operation.

Inventive Principle:
Principle #15Dynamics

4Ease of manufacture

If the gas source is positioned inside the vacuum chamber, then gas delivery is direct, but refilling requires entry into the chamber and realignment of the needle

Engineering Contradiction:
Improvegas deliveryVSAvoidrefilling operation
Core Design Contradiction:
Ease of manufactureVSEase of operation

Solution Approach 1:

The gas sources are extracted from the vacuum chamber and placed in a cabinet outside the chamber. This allows refilling and source replacement to be performed externally without breaking vacuum or entering the chamber, eliminating realignment requirements and improving safety.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

A cabinet serves as an intermediary between the external environment and the vacuum chamber, housing the gas sources and control valves. This intermediary structure allows easy access for refilling while maintaining vacuum integrity in the chamber.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This solution provides precise and rapid control of gas flow and pressure in the sample chamber, reducing the need for frequent refilling, enhancing safety, and allowing a wider range of pressures and flow rates, while maintaining precise gas ratios, thus improving the efficiency and safety of beam-assisted processes.

Implementation Method 1

gas flow from multiple gas sources into a sample chamber of a beam system is controlled by a cycling valve for each gas source

Methodology Applied
Scientific EffectValve cycling control: Valve

Implementation Method 2

microvalves positioned inside the vacuum chamber for rapid response

Methodology Applied
Scientific EffectRapid valve response: Valve

Implementation Method 3

allowing precise control of gas flow by adjusting the duty cycle and frequency of the valves

Methodology Applied
Scientific EffectDuty cycle control: Valve

Data Source

PatentEP2501839B1Gas delivery for beam processing systems
Publication Date: 2016.01.27 FEI CO
  • EP2501839B1 patent drawingFigure 1
  • EP2501839B1 patent drawingFigure 2
  • EP2501839B1 patent drawingFigure 3

AI summary

Gas flow from multiple gas sources into a sample chamber of a beam system is controlled by a cycling valve for each gas source, with the gas pressure in the sample chamber being determined by the relative time that the valve is opened and the upstream pressure at the valve. A gas valve positioned inside the vacuum chamber allows rapid response in shutting off a gas. In some preferred embodiments, a precursor gas is supplied from a solid or liquid material in a container that remains outside the vacuum system while in use and which is readily connected or disconnected to the gas injection system without significant leakage.