Cyclone Separators for FCCU Catalyst Suspension

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Solution Overview

Problem

Current separation systems in fluid catalytic cracking units (FCCUs) face challenges in efficiently separating spent catalysts and hydrocarbons under varying operational conditions, particularly with high catalyst/hydrocarbon ratios and rapid changes, leading to increased residence time, product degradation, and complex operational demands.

Innovation Solution

A new separation system integrating both inertial and centrifugal separation devices, including cyclones with and without sealing legs, is designed to operate efficiently under extreme conditions, featuring a compact configuration with cyclones arranged circumferentially around the vertical section and a fluidized bed for catalyst regeneration.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional separation systems are used in FCCUs, then separation can be performed, but residence time increases leading to product degradation and excessive coke formation

Engineering Contradiction:
Improveseparation efficiencyVSAvoidresidence time
Core Design Contradiction:
ReliabilityVSLoss of time

Solution Approach 1:

The separation system is divided into multiple cyclone separators arranged in series, where each cyclone handles a portion of the separation task. This segmentation allows the suspension to be processed through multiple separation stages in quick succession, reducing overall residence time while maintaining high separation efficiency. The patent describes a system with multiple cyclones connected in sequence, where spent catalyst particles are progressively separated from hydrocarbon vapors across several stages.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent transitions from conventional single-stage separation to a multi-dimensional arrangement of cyclone separators. The cyclones are positioned at different heights and angular positions around the vertical section, creating a three-dimensional separation architecture. This spatial arrangement optimizes flow patterns and reduces residence time by enabling parallel processing paths while maintaining effective separation.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Adaptability or versatility

If multiple risers operate under different conditions, then operational flexibility increases, but separation system complexity and volume increase

Engineering Contradiction:
Improveoperational flexibilityVSAvoidseparation system complexity
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The separation system is designed as a universal configuration that can handle suspensions from multiple risers operating under different conditions. The same cyclone separator arrangement and operational parameters can process suspensions with varying catalyst-to-hydrocarbon ratios, densities, and flow rates. This multi-functional design eliminates the need for separate specialized separation systems for each riser, reducing overall complexity while maintaining adaptability.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The patent combines the separation outputs from multiple risers into a single integrated separation system. Instead of having separate separation units for each riser, the suspension from all risers is directed to a common set of cyclone separators. This merging approach simplifies the overall system architecture, reduces equipment volume, and maintains operational flexibility through unified control of separation parameters.

Inventive Principle:
Principle #5Merging (Combining)

3Productivity

If high catalyst/hydrocarbon ratios are used, then conversion rates increase, but separation becomes more difficult and residence time increases

Engineering Contradiction:
Improveconversion rateVSAvoidseparation time
Core Design Contradiction:
ProductivityVSLoss of time

Solution Approach 1:

The patent employs multiple cyclone separators that replicate the same separation mechanism in parallel. Each cyclone is an identical copy designed to handle a specific portion of the high-catalyst suspension. This copying approach allows the system to process high catalyst-to-hydrocarbon ratios efficiently by distributing the separation load across multiple identical units, maintaining short residence time while achieving complete separation.

Inventive Principle:
Principle #26Copying

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This system significantly enhances the separation efficiency, reducing the residence time and catalyst flow to cyclones, achieving up to 99.8% catalyst separation with reduced erosion and instability, while maintaining product quality.

Implementation Method 1

a vertical section (6) configured to receive the suspension from the at least one ascending flow reaction tube and deflect it downwards, wherein a first inertial separation of the spent catalysts from the suspension takes place in the vertical section (6)

Methodology Applied
Scientific EffectInertial force: Inertia

Implementation Method 2

The separation device comprises a plurality of cyclone separators arranged circumferentially around the vertical section (6) of the interconnection means (4), each cyclone separator being in fluid communication with the vertical section (6) and configured to separate spent catalysts from the suspension using centrifugal force

Methodology Applied
Scientific EffectCentrifugal force: Centrifugal Force

Implementation Method 3

The separation device comprises a fluidized bed (12) configured to receive spent catalysts from the cyclone separators and regenerate the catalyst particles

Methodology Applied
Scientific EffectFluidization: Fluidisation

Data Source

PatentEP2065458B1System and process for the separation of suspensions
Publication Date: 2018.09.19 PETROLEO BRASILEIRO SA PETROBRAS
  • EP2065458B1 patent drawingFigure 1
  • EP2065458B1 patent drawingFigure 2
  • EP2065458B1 patent drawingFigure 3

AI summary

The present invention relates to a system for the separation of suspensions of spent catalysts and hydrocarbons formed in a fluid catalytic cracking unit with at least one ascending flow reaction tube, said separation device comprising: a vertical section fluidly connected to said at least one ascending flow reaction tube such that said suspension can be transferred from said at least one ascending flow reaction tube to an inlet of said vertical section; an opening device, connected to said vertical section below said inlet, said opening device being configured to allow at least a portion of said spent catalyst to drain there through; a first cyclone separator configured to receive and separate at least a part of the suspension that has not drained from said vertical section through said opening device; and a second cyclone separator configured to receive and separate at least a part of the suspension from said first cyclone separator. The present invention also relates to a process for the separation of suspensions of spent catalysts and hydrocarbons using the said separation system.