Dielectric Barrier Discharge Torch for Nanopowder Surface Treatment

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Solution Overview

Problem

Nanopowders exhibit a propensity to agglomerate due to their high specific surface area, which affects their functional properties and makes them difficult to handle, and existing coating methods often operate at low pressures, limiting their application and efficiency.

Innovation Solution

A Dielectric Barrier Discharge Torch operating at atmospheric pressures or soft vacuum conditions is used to modify the surface chemistry of micro- and nanoparticles by reacting with a plasma discharge or depositing a coating material, effectively preventing agglomeration and enhancing handling while maintaining unique properties.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If nanopowders are used to take advantage of their high specific surface area and unique properties, then their functional properties are improved, but they tend to agglomerate making them difficult to handle

Engineering Contradiction:
Improvespecific surface areaVSAvoidhandling difficulty
Core Design Contradiction:
Quantity of substanceVSEase of operation

Solution Approach 1:

A thin film coating is applied to the nanopowder particles to prevent agglomeration. The coating acts as a protective shell that maintains particle separation while preserving the high specific surface area and unique properties of the nanopowder, thereby improving handling characteristics without sacrificing functional performance.

Inventive Principle:
Principle #30Flexible shells and thin films

2Ease of operation

If a thin film coating is deposited on nanopowder particles to prevent agglomeration, then handling is improved, but the coating thickness must be precisely controlled to maintain unique properties

Engineering Contradiction:
Improvehandling easeVSAvoidcoating thickness control
Core Design Contradiction:
Ease of operationVSManufacturing precision

Solution Approach 1:

The plasma processing parameters (power, pressure, gas flow, treatment time) are optimized and controlled to achieve consistent thin film deposition with precise thickness control. By adjusting these parameters, the coating thickness can be maintained within a narrow range that prevents agglomeration while preserving the nanopowder's unique optical, magnetic, and catalytic properties.

Inventive Principle:
Principle #35Parameter changes

3Reliability

If plasma surface treatment is used to modify nanopowder surfaces, then surface characteristics are improved, but the treatment must be performed at low pressures which limits application versatility

Engineering Contradiction:
Improvesurface treatment effectivenessVSAvoidpressure condition flexibility
Core Design Contradiction:
ReliabilityVSAdaptability or versatility

Solution Approach 1:

The plasma treatment system is designed to operate across a range of pressures including atmospheric pressure, in addition to vacuum conditions. This parameter flexibility allows the same plasma surface treatment process to be applied in diverse settings without requiring vacuum equipment, thereby maintaining treatment effectiveness while significantly expanding application versatility and ease of implementation.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The process allows for the controlled deposition of coatings with thickness ranging from less than one nanometer to hundreds of nanometers, improving the dispersion characteristics and stability of nanoparticles without compromising their optical, magnetic, or energetic values.

Implementation Method 1

modifying the surface chemistry of the powder feed material by means of reaction with the plasma discharge

Methodology Applied
Scientific EffectPlasma discharge: Plasma

Implementation Method 2

A Dielectric Barrier Discharge Torch operating at atmospheric pressures or soft vacuum conditions is used to modify the surface chemistry

Methodology Applied
Scientific EffectDielectric barrier discharge:

Data Source

PatentUS8263178B2Plasma surface treatment using dielectric barrier discharges
Publication Date: 2012.09.11 TEKNA PLASMA SYST INC
  • US8263178B2 patent drawing
  • US8263178B2 patent drawing
  • US8263178B2 patent drawing

AI summary

A process for the in-flight surface treatment of powders using a Dielectric Barrier Discharge Torch operating at atmospheric pressures or soft vacuum conditions is described herein. The process comprising feeding a powder material into the Dielectric Barrier Discharge Torch yielding powder particles exhibiting a reduced powder agglomeration feature; in-flight modifying the surface properties of the particles; and collecting coated powder particles. An apparatus for surface treating micro- and nanoparticles comprising a Dielectric Barrier Discharge Torch operating at atmospheric pressure or soft vacuum conditions is also described herein.