Delayed Fracture Evaluation Using Chloride Solution Retention

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Solution Overview

Problem

Existing methods for evaluating delayed fracture characteristics of metal materials, particularly at edge faces, do not accurately account for the effects of a wet corrosive environment, such as snowfall, rainfall, or splashing, which are common in real-world automotive usage.

Innovation Solution

A method involving the use of a solution-retaining material impregnated with a chloride solution of pH 3.5 or more, applied to the edge face of the metal material, and maintained at a deliquescence humidity to simulate a wet corrosive environment, thereby accurately evaluating delayed fracture characteristics.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If conventional evaluation methods (acid immersion test, cathodic charging test) are used, then delayed fracture characteristics can be evaluated, but the wet corrosive environment (snowfall, rainfall, splashing) is not taken into consideration

Engineering Contradiction:
Improvedelayed fracture evaluation accuracyVSAvoidenvironmental condition coverage
Core Design Contradiction:
Measurement precisionVSAdaptability or versatility

Solution Approach 1:

The patent changes the environmental parameters by introducing a wet corrosive environment simulation system that controls humidity, temperature, and corrosive solution concentration. This allows the evaluation to account for real-world conditions like snowfall, rainfall, and splashing that were previously ignored in conventional dry environment tests.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent introduces a corrosive solution as an intermediary medium between the test specimen and the environment. This solution simulates the chemical effects of snowfall, rainfall, and splashing, allowing controlled evaluation of delayed fracture in wet corrosive conditions without requiring actual outdoor exposure.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Object-affected harmful factors

If the pH of the corrosive solution is lowered to increase hydrogen introduction, then delayed fracture induction is enhanced, but the test conditions become more severe than actual environment

Engineering Contradiction:
Improvehydrogen introduction amountVSAvoidtest condition representativeness
Core Design Contradiction:
Object-affected harmful factorsVSReliability

Solution Approach 1:

The patent optimizes the pH parameter within a specific range (2.0-4.0) to achieve adequate hydrogen introduction while maintaining test conditions that still represent actual service environments. This balanced parameter selection ensures both sufficient hydrogen embrittlement induction and realistic evaluation of material performance.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent applies partial action by using moderate pH levels rather than extreme acidity, and controlled exposure times. This allows sufficient hydrogen introduction to evaluate delayed fracture without creating test conditions that are excessively severe compared to actual automotive service conditions.

Inventive Principle:
Principle #16Partial or excessive action

3Adaptability or versatility

If test materials are kept in wet state to simulate snowfall/rainfall/splashing, then real-world environment is replicated, but existing methods cannot maintain controlled wet conditions

Engineering Contradiction:
Improvewet environment simulationVSAvoidtest system complexity
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The patent uses a corrosive solution as an intermediary to create and maintain controlled wet conditions. This solution allows the test system to simulate snowfall, rainfall, and splashing environments while maintaining laboratory control over humidity, concentration, and exposure conditions.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent employs hydraulic principles by using liquid corrosive solutions to create wet environments. The system controls the distribution, concentration, and contact time of the liquid solution with test specimens, enabling realistic simulation of wet corrosive conditions without uncontrolled complexity.

Inventive Principle:
Principle #29Pneumatics and hydraulics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method allows for the accurate evaluation of delayed fracture characteristics of metal materials in a wet corrosive environment, replicating the severe corrosive conditions that can lead to edge face failure in actual automotive use.

Implementation Method 1

an object to penetration into a surface-treated film using a water-containing material

Methodology Applied
Scientific EffectElectrochemical corrosion: Crevice Corrosion

Implementation Method 2

maintaining a state in which the solution-retaining material is held at a deliquescence humidity of the chloride

Methodology Applied
Scientific EffectCapillary action: Capillary Action

Implementation Method 3

a cathodic charging test to introduce hydrogen into a steel sheet

Methodology Applied
Scientific EffectDiffusion: Diffusion

Data Source

PatentUS12320739B2Method for evaluating delayed fracture of metal material
Publication Date: 2025.06.03 JFE STEEL CORP
  • US12320739B2 patent drawing
  • US12320739B2 patent drawing

AI summary

A method for evaluating the delayed fracture characteristics of a metal material. The method including placing a solution-retaining material impregnated with a solution containing a chloride and having a pH of 3.5 or more on an edge face of the metal material, and maintaining a state in which the solution-retaining material is held at a deliquescence humidity of the chloride to thereby corrode the edge face.