Densifying Nanofiber Forests via Deformable Substrate Compression

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Solution Overview

Problem

Existing methods for densifying nanofibers often focus on nanofiber sheets or yarns rather than the forest itself, limiting the achievable density and subsequent electrical and mechanical properties.

Innovation Solution

A method involving a deformable substrate with a flowable adhesive is used to attach and then manipulate a nanofiber forest, reducing the substrate's surface area to increase the areal density of nanofibers, allowing them to move closer together, thereby enhancing their electrical and mechanical properties.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If conventional densifying methods are applied to nanofiber sheets or yarns, then some density increase is achieved, but the achievable density is limited and electrical and mechanical properties are not sufficiently enhanced

Engineering Contradiction:
Improvenanofiber densityVSAvoidelectrical and mechanical properties
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent transitions from working with 2D nanofiber sheets to utilizing 3D nanofiber forests grown vertically on substrates. By growing nanofibers in the vertical dimension (perpendicular to substrate surface) and then densifying the forest structure, the method achieves significantly higher nanofiber density and better property enhancement compared to conventional sheet-based approaches.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

Solution Approach 2:

The patent employs substrate deformation (changing the physical state/shape of the substrate) to compress the nanofiber forest and increase density. By deforming the substrate from a relaxed state to a deformed state, the nanofibers are brought closer together, achieving the desired density increase and property enhancement.

Inventive Principle:
Principle #35Parameter changes

2Quantity of substance

If the substrate surface area is reduced to increase nanofiber areal density, then electrical and mechanical properties improve, but the process complexity increases

Engineering Contradiction:
Improveareal densityVSAvoidprocess complexity
Core Design Contradiction:
Quantity of substanceVSDevice complexity

Solution Approach 1:

The patent introduces a deformable substrate as an intermediary carrier that facilitates the densification process. The substrate acts as a mediator between the nanofiber forest and the final high-density product, allowing density control through substrate deformation while simplifying the overall process compared to direct compression methods.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent uses a dynamically deformable substrate that can change shape in response to external stimuli (such as temperature changes or mechanical forces). This dynamic substrate allows for controlled density adjustment of the nanofiber forest without requiring complex rigid compression equipment.

Inventive Principle:
Principle #15Dynamics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach effectively increases the nanofiber density beyond conventional methods, improving thermal and electrical conductivity and mechanical strength, making the densified forests suitable for various applications.

Implementation Method 1

attaching a nanofiber forest to the surface of the deformable substrate using a flowable adhesive

Methodology Applied
Scientific EffectAdhesion: Adhesive

Implementation Method 2

elastically deforming the deformable substrate from the starting surface area to a first surface area larger than the starting surface area

Methodology Applied
Scientific EffectElastic deformation: Elasticity

Implementation Method 3

increasing an areal density of the nanofiber forest by allowing the elastically deformable substrate to relax into a second relaxed state having a third surface area that is less than the second surface area

Methodology Applied
Scientific EffectElastic recovery: Elastic Recovery

Implementation Method 4

the stimulus is heat causing a temperature of the deformable substrate to exceed a glass transition temperature

Methodology Applied
Scientific EffectThermal heating: Heating

Implementation Method 5

plastically deforming the deformable substrate by applying a stimulus, the deformable substrate shrinking from the starting surface area to the second surface area in response to the applied stimulus

Methodology Applied
Scientific EffectPlastic deformation: Plasticity

Implementation Method 6

the flowable adhesive responds to an applied stress by flowing to relax the applied stress

Methodology Applied
Scientific EffectViscous flow: Viscoelasticity

Data Source

PatentUS10894718B2Densifying a nanofiber forest
Publication Date: 2021.01.19 LINTEC OF AMERICA INC
  • US10894718B2 patent drawing
  • US10894718B2 patent drawing
  • US10894718B2 patent drawing

AI summary

A nanofiber forest is described that has been processed to increase a number of nanofibers per unit area (referred to as “areal density” or, equivalently, “density”) compared to the nanofiber forest in its as-synthesized state. This increase in areal density is accomplished by physically manipulating a deformable substrate on which the nanofiber forest is disposed. At a high level, this physical manipulation begins by transferring the nanofiber forest from a growth substrate to a deformable substrate. A surface area of the deformable substrate is reduced relative to a surface area of the substrate when the nanofiber forest was attached. This reduction in area causes the nanofibers in the forest to move closer to one another, thus increasing the number of nanofibers per unit area.