Dental Bulk Block With Crystal Gradient for Strength and Milling

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Conventional dental materials face challenges in achieving high strength, aesthetic appearance, and processability, with limitations in direct mechanical processing due to large crystal phases, and require secondary heat treatments that affect dimensional accuracy and increase economic burden.

Innovation Solution

A method for manufacturing a dental bulk block with a crystalline size gradient and functional properties, using a glass composition that includes lithium disilicate and silicate phases, heat-treated with a temperature gradient to achieve multi-gradation of transmittance and mechanical properties similar to natural teeth.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If conventional lithium disilicate crystallized glass is used to achieve high strength, then strength is improved, but processability deteriorates due to large crystal phase size

Engineering Contradiction:
ImprovestrengthVSAvoidprocessability
Core Design Contradiction:
StrengthVSEase of manufacture

Solution Approach 1:

The patent applies local quality by creating a functionally gradient material where the crystal phase size varies through the depth of the bulk block. The surface region contains fine crystal phases (5-50 μm) for good processability and aesthetics, while the inner region contains coarse crystal phases (50-200 μm) for high strength. This spatial variation in crystal size allows each region to optimize its local properties for its specific function.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent transitions from uniform material properties to dimensionally varied properties by introducing a depth-dependent crystal phase size gradient. This dimensional variation allows the material to simultaneously exhibit different characteristics at different depths, resolving the contradiction between surface processability and bulk strength.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Strength

If secondary heat treatment is performed to form lithium disilicate crystal phase for high strength, then strength is improved, but manufacturing complexity increases due to additional process steps

Engineering Contradiction:
ImprovestrengthVSAvoidmanufacturing process complexity
Core Design Contradiction:
StrengthVSDevice complexity

Solution Approach 1:

The patent applies preliminary action by forming the desired functionally gradient crystal phase structure during the initial heat treatment process. The heat treatment is designed to create different crystal phases at different depths simultaneously, eliminating the need for subsequent secondary heat treatment to form lithium disilicate. This preliminary structuring achieves both strength and processability in a single process.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent merges the functions of creating strength-enhancing crystal phases and ensuring processability into a single heat treatment process. Instead of separate steps for forming different crystal phases, the process combines these functions by controlling heat treatment parameters to generate the gradient structure in one operation.

Inventive Principle:
Principle #5Merging (Combining)

3Strength

If secondary heat treatment is performed to increase strength, then strength is improved, but manufacturing time increases due to additional heat treatment process

Engineering Contradiction:
ImprovestrengthVSAvoidmanufacturing time
Core Design Contradiction:
StrengthVSLoss of time

Solution Approach 1:

The patent performs the crystal phase formation action preliminarily during the first heat treatment process. The heat treatment parameters are optimized to create the functionally gradient structure with appropriate crystal phases for strength in the inner region and processability in the surface region, eliminating the need for time-consuming secondary heat treatment.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent skips the secondary heat treatment step entirely by designing a heat treatment process that directly produces the desired gradient crystal phase structure. This rushing through of the process achieves the strength enhancement without the time delay of additional heat treatment cycles.

Inventive Principle:
Principle #21Skipping (Rushing through)

4Strength

If conventional lithium disilicate crystallized glass is used to achieve high strength, then strength is improved, but aesthetic appearance deteriorates due to coarse crystal phase

Engineering Contradiction:
ImprovestrengthVSAvoidlight transmittance
Core Design Contradiction:
StrengthVSIllumination intensity

Solution Approach 1:

The patent applies local quality by creating a functionally gradient material where the crystal phase size varies through the depth of the bulk block. The surface region contains fine crystal phases (5-50 μm) for good processability and aesthetics, while the inner region contains coarse crystal phases (50-200 μm) for high strength. This spatial variation in crystal size allows each region to optimize its local properties for its specific function.

Inventive Principle:
Principle #3Local quality

5Strength

If heat treatment process is performed to form lithium disilicate crystal phase, then strength is improved, but dimensional accuracy deteriorates due to shrinkage

Engineering Contradiction:
ImprovestrengthVSAvoiddimensional accuracy
Core Design Contradiction:
StrengthVSManufacturing precision

Solution Approach 1:

The patent performs the crystal phase formation action preliminarily during the first heat treatment process. The heat treatment parameters are optimized to create the functionally gradient structure with appropriate crystal phases for strength in the inner region and processability in the surface region, eliminating the need for subsequent secondary heat treatment that would cause additional shrinkage and dimensional changes.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method allows for efficient CAD/CAM processing, reducing manufacturing time and ensuring structural stability by emulating natural tooth characteristics without additional processes, enhancing aesthetic and mechanical properties.

Implementation Method 1

a method of manufacturing a block having a predetermined shape using a glass composition; and heat treating the block

Methodology Applied
Scientific EffectCrystallisation: Crystallisation

Implementation Method 2

2 to 6 wt% of P 2 O 5 serving as a nucleation agent

Methodology Applied
Scientific EffectNucleation: Nucleation

Implementation Method 3

heat treating the block so as to ensure a temperature gradient in a depth direction of the block

Methodology Applied
Scientific EffectTemperature Gradient: Temperature Gradient

Data Source

PatentEP3744696B1Dental bulk block for grinding processing and method of manufacturing the same
Publication Date: 2026.03.18 HAAS CO LTD
  • EP3744696B1 patent drawingFigure 1
  • EP3744696B1 patent drawingFigure 2
  • EP3744696B1 patent drawingFigure 3

AI summary

Disclosed is a dental bulk block for grinding processing. The dental bulk block includes a crystalloid, which includes lithium disilicate as a main crystal phase and silicate as a sub-crystal phase, and hyaline as a remainder. The dental bulk block is a functionally gradient material having a crystalline size gradient with respect to a depth thereof and having no interface at a change point of a crystalline size gradient value. The dental bulk block is useful for manufacturing an artificial dental prosthesis that is similar to natural teeth. Accordingly, the time and process for manufacturing the artificial dental prosthesis are shortened, and structural stability is increased in terms of dispersion of force due to gradient functionalization of mechanical properties.