Depolymerized Carboxylated Cellulose for Mineral Grinding

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Solution Overview

Problem

Current dispersing agents for mineral suspensions, such as acrylic acid polymers, do not offer a sustainable alternative and are inefficient in terms of productivity and cost, particularly in reducing the molecular weight of carboxylated cellulose for effective grinding and dispersion applications.

Innovation Solution

Depolymerized carboxylated cellulose with a molecular weight between 10,000 and 40,000 g/mol and a high dry extract of 25-40% is used as a dispersing agent, obtained through a continuous process involving hydrogen peroxide and controlled temperature, allowing for efficient grinding and dispersion of mineral materials without the need for additional concentration steps.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Length of moving object

If carboxylated cellulose is used as a dispersing agent for mineral suspensions, then bio-sourced sustainability is improved, but the molecular weight reduction efficiency and productivity are insufficient

Engineering Contradiction:
Improvemolecular weightVSAvoidproductivity
Core Design Contradiction:
Length of moving objectVSProductivity

Solution Approach 1:

The patent applies parameter changes by systematically varying the oxidation time, temperature, and hydrogen peroxide concentration to achieve the optimal molecular weight range (10,000-40,000 g/mol) for depolymerized carboxylated cellulose. This controlled parameter adjustment enables efficient molecular weight reduction while maintaining high productivity and bio-sourced sustainability advantages over conventional acrylic acid polymers.

Inventive Principle:
Principle #35Parameter changes

2Productivity

If depolymerization time is reduced to increase productivity, then the molecular weight reduction speed is improved, but the ability to obtain high solids solutions deteriorates

Engineering Contradiction:
Improvedepolymerization speedVSAvoidsolids content
Core Design Contradiction:
ProductivityVSQuantity of substance

Solution Approach 1:

The patent implements continuity of useful action through a controlled oxidation process that maintains optimal reaction conditions throughout the depolymerization. By continuously monitoring and controlling the oxidation parameters, the process achieves both rapid molecular weight reduction and high solids content (25-40%) in the final solution, resolving the contradiction between speed and concentration.

Inventive Principle:
Principle #20Continuity of useful action

3Productivity

If conventional acrylic acid polymers are used as dispersing agents, then grinding efficiency is achieved, but sustainability and cost-effectiveness deteriorate

Engineering Contradiction:
Improvegrinding efficiencyVSAvoidmolecular weight
Core Design Contradiction:
ProductivityVSLength of moving object

Solution Approach 1:

The patent changes the fundamental parameter of molecular weight by using depolymerized carboxylated cellulose with controlled molecular weight (10,000-40,000 g/mol) instead of conventional high molecular weight acrylic acid polymers. This parameter change maintains effective grinding efficiency while providing bio-sourced sustainability and cost advantages, directly addressing the contradiction between conventional effectiveness and sustainable alternatives.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This solution provides a high-solids content depolymerized carboxylated cellulose that enhances productivity and reduces costs by enabling effective grinding and dispersion of mineral materials, such as calcium carbonate, with improved particle size distribution and viscosity, suitable for various industrial applications.

Implementation Method 1

It is known to carry out the depolymerization of CMC, that is to say the reduction of its molecular weight, by means of an oxidative treatment. Document EP 0 465 992 (Aqualon Company) describes a process for depolymerizing CMC using hydrogen peroxide

Methodology Applied
Scientific EffectOxidation: Oxidation

Data Source

PatentEP3065853B1Use of depolymerised carboxylated celluloses for dispersing and grinding mineral materials
Publication Date: 2018.10.17 COATEX SA

AI summary

The present invention concerns the use of depolymerised carboxylated celluloses as an agent for dispersing or assisting in the grinding of aqueous suspensions of mineral materials, intended for paint formulations, plastic formulations, detergent formulations, cosmetic formulations, paper formulations or paper coating slips.