Detergent Granule with Low Aspect Ratio and Salt Composite

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Solution Overview

Problem

Mid-cut alkyl sulfate (MCAS) particles in cleaning compositions face challenges with limited suds-boosting effect due to large size and poor dissolution profile, and are prone to caking and clumping at higher temperatures and humid environments, complicating processing and handling.

Innovation Solution

Forming detergent granules with a small particle size and low aspect ratio, containing 85-95% MCAS and 4-14% water-soluble salts, which enhances dissolution and reduces water absorption, thereby minimizing caking and clumping issues.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If MCAS is used in extruded needle form, then processing ease is improved, but suds-boosting effect deteriorates

Engineering Contradiction:
Improveprocessing easeVSAvoidsuds-boosting effect
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

The patent changes the physical parameters of MCAS from extruded needle form to spherical granule form with specific size range (200-1000 μm) and aspect ratio (≤2). This parameter change improves both dissolution rate (enhancing suds-boosting effect) and processing characteristics (reducing caking and clumping).

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite granule structure combining MCAS with water-soluble salts (sodium sulfate, sodium carbonate, magnesium chloride, magnesium sulfate, or sodium silicate) in specific ratios. This composite approach enhances dissolution profile while maintaining processing ease and reducing caking tendency.

Inventive Principle:
Principle #40Composite materials

2Reliability

If MCAS is used in fine powder form, then suds-boosting effect is improved, but caking and clumping worsens

Engineering Contradiction:
Improvesuds-boosting effectVSAvoidprocessing ease
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent optimizes particle size parameters to a specific range (200-1000 μm) and controls aspect ratio (≤2), creating spherical granules that balance dissolution rate with flowability. This prevents the caking and clumping issues of fine powder while maintaining good suds-boosting effect.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent formulates composite granules containing MCAS (85-95%) combined with water-soluble salts (5-15%). This composition reduces water absorption and caking tendency while preserving the suds-boosting effectiveness of MCAS.

Inventive Principle:
Principle #40Composite materials

3Speed

If MCAS particle size is reduced, then dissolution profile is improved, but water absorption increases

Engineering Contradiction:
Improvedissolution rateVSAvoidwater absorption
Core Design Contradiction:
SpeedVSObject-affected harmful factors

Solution Approach 1:

The patent creates composite granules with MCAS (85-95%) and water-soluble salts (5-15%). The water-soluble salt component modifies the overall water absorption characteristics of the granule, allowing faster dissolution of MCAS while controlling excessive water uptake that would lead to caking.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent maintains particle size in the optimized range (200-1000 μm) with aspect ratio ≤2, achieving a balance between dissolution rate and water absorption. The spherical shape and size control prevent excessive surface area that would increase water uptake while ensuring adequate dissolution performance.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution improves the suds-boosting effect and reduces the likelihood of caking and clumping, making the detergent granules easier to handle and store, while maintaining high detersive activity and flowability.

Implementation Method 1

the dissolution profile of such detergent granule can be improved

Methodology Applied
Scientific EffectDissolution: Solvation

Implementation Method 2

it is less likely to absorb ambient water and therefore less like to cake or form clumps during shipping or storage

Methodology Applied
Scientific EffectDeliquescence: Deliquescence

Data Source

PatentEP3790950B1Detergent granule
Publication Date: 2023.11.01 PROCTER & GAMBLE CO
  • EP3790950B1 patent drawingFigure 1
  • EP3790950B1 patent drawing
  • EP3790950B1 patent drawing

AI summary

A detergent granule is characterized by a Medium Particle Size ranging from 200 μm to 1000 μm and an aspect ratio of no more than 2, and contains from 85 wt% to 95 wt% of an alkyl sulfate (AS) having a branched or linear unalkoxylated C6-C16 alkyl group and from 4 wt% to 14 wt% of a water-soluble salt, with a water or moisture content of from 1 wt% to 5 wt%.