Powder Detergent Encapsulated Perfume Stability

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Solution Overview

Problem

Powder detergent compositions face challenges in maintaining fragrance stability and mechanical resistance during high-shearing manufacturing processes, as perfume microcapsules are prone to breakage and leakage, affecting the product's olfactive performance and quality.

Innovation Solution

A powder detergent composition comprising a surfactant system and granulated particles made of a water-soluble polymer matrix with encapsulated oil, where up to 30% of the powder weight is encapsulated oil, enhancing mechanical resistance and stability during processing.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Duration of action of moving object

If perfume microcapsules are incorporated into detergent powder, then olfactive performance and fragrance longevity are enhanced, but mechanical resistance and stability during high-shearing manufacturing processes deteriorate

Engineering Contradiction:
Improvefragrance longevityVSAvoidmechanical resistance
Core Design Contradiction:
Duration of action of moving objectVSStrength

Solution Approach 1:

The invention uses a composite granulated powder structure consisting of a water-soluble polymer matrix (such as starch or maltodextrin) combined with encapsulated oil containing perfume. This composite structure provides both mechanical strength to withstand manufacturing processes and controlled fragrance release, resolving the contradiction between durability and olfactive performance.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The invention optimizes the oil content parameter to a specific range (5-30% by weight, preferably 10-20%) within the granulated powder. This parameter optimization ensures sufficient fragrance loading while maintaining adequate mechanical strength and stability during high-shearing manufacturing processes, balancing fragrance longevity with mechanical resistance.

Inventive Principle:
Principle #35Parameter changes

2Quantity of substance

If high oil content is used in granulated powder particles, then olfactive performance is improved, but particle stability and resistance to abrasion during manufacturing deteriorate

Engineering Contradiction:
Improveperfume contentVSAvoidparticle stability
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The invention establishes an optimal oil content range of 5-30% by weight (preferably 10-20%) in the granulated powder. This parameter optimization balances fragrance quantity with particle stability, ensuring sufficient perfume loading while maintaining mechanical strength and resistance to abrasion during high-shearing manufacturing processes.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention creates a structured granulated powder where oil is dispersed within a water-soluble polymer matrix rather than uniformly distributed. This local quality distribution ensures that fragrance is concentrated in specific regions while the polymer matrix provides structural integrity and stability throughout the particle, maintaining both olfactive performance and particle reliability.

Inventive Principle:
Principle #3Local quality

3Stability of the object's composition

If extensive mixing is performed during manufacturing, then homogeneity of the detergent composition is improved, but particle breakage and perfume leakage increase

Engineering Contradiction:
Improvecomposition homogeneityVSAvoidperfume leakage
Core Design Contradiction:
Stability of the object's compositionVSLoss of substance

Solution Approach 1:

The invention pre-encapsulates perfume oil within a water-soluble polymer matrix to form stable granulated powder particles before the final mixing stage. This preliminary encapsulation protects the perfume from leakage during subsequent mixing operations, allowing extensive mixing to achieve homogeneity without significant perfume loss.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The water-soluble polymer matrix (such as starch or maltodextrin) forms a flexible protective shell around the encapsulated oil and perfume. This shell provides mechanical protection during high-shearing mixing while remaining soluble under washing conditions, enabling homogeneous mixing without excessive particle breakage or perfume leakage.

Inventive Principle:
Principle #30Flexible shells and thin films

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution effectively reduces particle abrasion and breakage during manufacturing, maintaining fragrance performance and stability, allowing for efficient and cost-effective production of detergent powders with improved olfactive retention.

Implementation Method 1

granulated powder comprising particles made of: a) a water soluble polymer matrix, b) an oil phase comprising a perfume dispersed in said polymer matrix, said oil being at least partly encapsulated in microcapsules

Methodology Applied
Scientific EffectEncapsulation: Physical Containment

Data Source

PatentUS11718815B2Powder detergent composition
Publication Date: 2023.08.08 FIRMENICH SA
  • US11718815B2 patent drawing

AI summary

Described herein is a powder detergent composition including a detergent active material including at least a surfactant system, and a granulated powder. The granulated powder includes particles made of: (a) a water soluble polymer matrix, and (b) an oil phase including a perfume dispersed in the water soluble polymer matrix, the oil being at least partly encapsulated in microcapsules. The granulated powder includes up to 30% by weight of encapsulated oil based on the total weight of the powder.