Detergent Tablet Production via Optimized Premix Composition

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Solution Overview

Problem

Existing processes for producing detergent or cleaning agent tablets face challenges in achieving a balance between sufficient hardness for handling and transportation without requiring storage, while also ensuring rapid disintegration in aqueous solutions, often necessitating high compression forces and additional additives.

Innovation Solution

A multi-stage process involving a specific powdered premix composition comprising sodium carbonate, sodium percarbonate, methylglycinediacetic acid, non-ionic surfactant, and washing-active polymer, compressed at moderate forces to create tablets with enhanced hardness and disintegration properties, eliminating the need for storage and reducing adhesion to equipment.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If high compression force is applied to increase tablet hardness, then tablet strength is improved, but disintegration time increases (slower disintegration)

Engineering Contradiction:
Improvetablet hardnessVSAvoiddisintegration time
Core Design Contradiction:
StrengthVSDuration of action of moving object

Solution Approach 1:

The patent changes the chemical composition parameters of the premix by incorporating specific builders (sodium carbonate, sodium percarbonate, MGDA) and polymers in optimized ratios. This chemical parameter change allows the tablet to achieve sufficient hardness at lower compression forces while maintaining rapid disintegration, resolving the contradiction between strength and disintegration time

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses a composite premix formulation combining multiple functional ingredients: builders (sodium carbonate, sodium percarbonate, MGDA), non-ionic surfactant, and washing-active polymer. This composite material approach creates synergistic effects that enable both adequate tablet hardness and rapid disintegration without requiring high compression forces

Inventive Principle:
Principle #40Composite materials

2Ease of manufacture

If high compression force is used to produce hard tablets, then manufacturing simplicity is maintained, but energy consumption increases

Engineering Contradiction:
Improvemanufacturing simplicityVSAvoidenergy consumption
Core Design Contradiction:
Ease of manufactureVSUse of energy by stationary object

Solution Approach 1:

The patent optimizes the premix composition parameters to enable compression at lower forces (10-30 kN instead of higher forces). This parameter change reduces energy consumption during tabletting while maintaining manufacturing simplicity through the use of conventional tablet press equipment

Inventive Principle:
Principle #35Parameter changes

3Productivity

If conventional premix formulations are used, then production process is simple, but adhesion to equipment occurs requiring maintenance

Engineering Contradiction:
Improveproduction efficiencyVSAvoidadhesion to equipment
Core Design Contradiction:
ProductivityVSObject-generated harmful factors

Solution Approach 1:

The patent modifies the chemical composition parameters of the premix by incorporating specific builders and polymers that alter the surface properties and flow characteristics. This reduces adhesion to equipment surfaces, minimizing production rejects and maintenance requirements while maintaining efficient production

Inventive Principle:
Principle #35Parameter changes

4Duration of action of moving object

If additional additives like polyethylene glycols and disintegrants are used, then tablet disintegration is improved, but device complexity increases

Engineering Contradiction:
Improvedisintegration timeVSAvoidformulation complexity
Core Design Contradiction:
Duration of action of moving objectVSDevice complexity

Solution Approach 1:

The patent makes the premix composition itself multi-functional: the combination of builders (sodium carbonate, sodium percarbonate, MGDA), non-ionic surfactant, and washing-active polymer serves both as the cleaning active ingredients and as the disintegration mechanism. This eliminates the need for separate disintegrant additives, reducing formulation complexity while ensuring rapid disintegration

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The patent extracts the disintegration function from separate additive components and integrates it into the core premix formulation. The builder-polymer-surfactant system itself provides the disintegration mechanism through its chemical properties, eliminating the need for additional disintegrant additives

Inventive Principle:
Principle #2Taking out (Extraction)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The process enables the production of tablets with high hardness and rapid disintegration in aqueous solutions, minimizing production rejects and maintenance times, and eliminating the need for additional additives like polyethylene glycols and disintegrants.

Implementation Method 1

compressing the powdered premix in the die with a pressing force of 15 to 50 kN

Methodology Applied
Scientific EffectCompression: Compression

Implementation Method 2

rapid disintegration in the aqueous washing or cleaning solution and the rapid release of the washing or cleaning active ingredients contained in the tablet

Methodology Applied
Scientific EffectDissolution: Solvation

Implementation Method 3

The detergent or cleaning agent tablets are introduced into the aqueous washing or cleaning solution

Methodology Applied
Scientific EffectDecomposition: Decomposition (biological)

Data Source

PatentEP4574946A1Production method for washing or cleaning agent tablets
Publication Date: 2025.06.25 HENKEL KGAA
  • EP4574946A1 patent drawing
  • EP4574946A1 patent drawing
  • EP4574946A1 patent drawing

AI summary

A process for producing a washing or cleaning agent tablet or a washing or cleaning agent tablet phase, comprising the steps of: i) providing a first powdered premix containing, based on its total weight a) 15 to 55% by weight of sodium carbonate; b) 8 to 32% by weight of sodium percarbonate; c) 8 to 30% by weight of methylglycinediacetic acid (MGDA) and its salts; d) 0.2 to 8% by weight of non-ionic surfactant; e) 2 to 18% by weight of washing or cleaning-active polymer; f) 0 to 2% by weight.-% citrate; by mixing its components; ii) optionally storing the powdered premix; iii) feeding the powdered premix to a dosing device of a tablet press; iv) dosing the powdered premix into the die of the die table of the tablet press; v) compressing the powdered premix in the die with a pressing force of 15 to 50 kN; vi) ejecting the washing or cleaning agent tablet or the washing or cleaning agent tablet phase from the die; vii) optionally packaging the washing or cleaning agent tablet or the washing or cleaning agent tablet phase.