Dewar Vessel Coolant Recirculation for Ice-Free Sample Access

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Solution Overview

Problem

Dewar vessels face challenges in providing reliable cooling while allowing easy access to samples, as frequent opening leads to ice contamination of the coolant, and samples are typically stored at the bottom for optimal cooling, complicating handling and throughput.

Innovation Solution

A pseudo-static pump is integrated into the Dewar vessel, using a chamber with a closing element and pressure increasing device to recirculate coolant, such as liquid nitrogen, to an upper part of the vessel, maintaining a constant coolant level and minimizing ice contamination, with a simple design that reduces maintenance and external connections.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If samples are stored at the bottom of the Dewar vessel for optimal cooling, then cooling reliability is improved, but sample accessibility and handling are worsened

Engineering Contradiction:
Improvecooling reliabilityVSAvoidsample accessibility
Core Design Contradiction:
ReliabilityVSEase of operation

Solution Approach 1:

The system divides the coolant distribution into two zones: a reservoir at the bottom and a distribution chamber at the top. The pump segments the coolant flow path, extracting coolant from the bottom reservoir and redistributing it to the top chamber, thereby decoupling the cooling source location from the sample storage location.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The pump acts as an intermediary device between the bottom reservoir and top distribution chamber. It mediates the coolant transfer process, enabling coolant to move from the cooling source at the bottom to the distribution point at the top, where samples are stored for easy access.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Ease of operation

If the Dewar vessel is opened frequently for high throughput sample access, then sample accessibility is improved, but ice contamination of the coolant is worsened

Engineering Contradiction:
Improvesample accessibilityVSAvoidice contamination
Core Design Contradiction:
Ease of operationVSObject-affected harmful factors

Solution Approach 1:

The pump operates continuously or in repeated cycles to maintain a constant level of coolant in the top distribution chamber. This continuous action ensures that samples remain immersed in coolant even when the Dewar is opened, eliminating the need to close the vessel to prevent contamination.

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

The system changes the operational parameter of coolant level from variable to constant. By actively maintaining a constant coolant level in the distribution chamber, the system allows the Dewar to remain open without exposing samples to ice contamination, as the coolant continuously covers the samples.

Inventive Principle:
Principle #35Parameter changes

3Productivity

If a complex pump system with moving mechanical parts is used for coolant circulation, then pumping functionality is improved, but maintenance requirements and device complexity are worsened

Engineering Contradiction:
Improvecoolant circulation capabilityVSAvoidmechanical parts complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The invention replaces complex mechanical pump systems with a simplified pressure-based circulation mechanism. By using pressure increases from gas injection or thermal expansion to drive coolant circulation, the system eliminates complicated moving parts while maintaining effective coolant pumping capability.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The simplified pump system requires minimal external control and maintenance. The pressure-based mechanism automatically circulates coolant without requiring complex mechanical assemblies, bearings, or seals that would need regular maintenance, thereby reducing device complexity and maintenance requirements.

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The pump ensures reliable cooling with easy access to samples by maintaining a constant coolant level and minimizing ice contamination, allowing for high throughput and efficient operation with reduced maintenance and external connections.

Implementation Method 1

The closing element is adapted to automatically close the chamber by floating when the chamber is filled by coolant

Methodology Applied
Scientific EffectBuoyancy: Archimedes' Principle (Buoyancy)

Implementation Method 2

the pressure increasing device is adapted to increase the pressure within the chamber after the chamber is partly or totally filled with the coolant, and until part of or all of the fluid is released through the outlet

Methodology Applied
Scientific EffectPressure increase: Pressure Increase

Implementation Method 3

The chamber is adapted to fill automatically by gravity flow through the inlet

Methodology Applied
Scientific EffectGravity flow: Gravitation

Data Source

PatentUS10066788B2Cooling of a Dewar vessel with ice free coolant and for short sample access
Publication Date: 2018.09.04 EURO LAB FUER MOLEKULARBIOLOGIE EMBL
  • US10066788B2 patent drawing
  • US10066788B2 patent drawing
  • US10066788B2 patent drawing

AI summary

The present invention relates to a pump (15) for pumping a coolant (9) within a Dewar vessel (1) and to a corresponding Dewar vessel (1) for storing samples in a coolant (9). The Dewar vessel (1) comprises a thermally insulated reservoir (3) for the coolant (9) and a sample vessel (11) provided separately and arranged in the thermally insulated reservoir (3). The reservoir (3) is connected to the sample vessel (11) in such a way that the level of coolant (9) is constant in the sample vessel (11). Pump (15) may help in keeping the level of coolant (9) in the sample vessel (11) constant. For this purpose the pump (15) comprises a chamber (17) with an inlet (19) and an outlet (21), a closing element (23) and a pressure increasing device (25). Therein, the inlet (19) is connectable to the reservoir (3) and the outlet (21) is connectable to a sample vessel (11) of the Dewar vessel (1). The chamber (17) is adapted to fill with coolant (9) through the inlet (19) by gravity and the closing element (23) is adapted to automatically close the chamber (17) when it is full of coolant (9). The pressure increasing device (25) is adapted to increase the pressure within the chamber (17), after the chamber (17) is closed, until the coolant (9) is released through the outlet (21).