Digital Bottle Test Prediction for Demulsifier Composition Selection

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Solution Overview

Problem

Existing methods for determining optimal demulsifier compositions for breaking complex oil-water emulsions in subterranean formations are laborious, time-consuming, and require numerous iterations, limiting the efficiency of finding the best product recommendation due to the complexity of each formation's unique chemical makeup.

Innovation Solution

A machine-learning model is used to predict demulsifier compositions by inputting bottle test results and composition data, allowing for the generation of new conditions that meet desired Key Performance Indicators (KPIs) in a more time-efficient manner, optimizing the demulsification process.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If traditional iterative bottle testing methods are used to determine optimal demulsifier compositions, then the accuracy of emulsion breaking performance is improved, but the time and labor required for testing increases significantly

Engineering Contradiction:
Improveemulsion breaking performance accuracyVSAvoidtesting time
Core Design Contradiction:
Measurement precisionVSLoss of time

Solution Approach 1:

The patent creates a virtual copy of the physical bottle test through a digital twin model. This virtual model replicates the complex emulsion breaking process, allowing multiple iterations and optimizations to be performed computationally rather than physically. The digital twin maintains the same input-output relationships as the actual bottle test but eliminates the time-consuming physical iteration cycle, thereby preserving measurement precision while dramatically reducing testing time.

Inventive Principle:
Principle #26Copying

Solution Approach 2:

The patent performs preliminary computational work by pre-training machine learning models on historical bottle test data before actual optimization needs arise. This preliminary action creates a ready-to-use digital framework that can quickly evaluate demulsifier compositions without requiring new physical tests. The pre-established digital twin and trained models enable rapid prediction and optimization, reducing the need for iterative physical testing while maintaining accuracy.

Inventive Principle:
Principle #10Preliminary action

2Adaptability or versatility

If multiple iterations of bottle testing are performed to account for unique formation chemical makeup, then the adaptability of demulsifier selection is improved, but the complexity of the testing process increases

Engineering Contradiction:
Improvedemulsifier composition optimizationVSAvoidtesting process complexity
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The patent develops a universal digital twin framework that can handle multiple different formation types and emulsion compositions through a single adaptable system. Rather than creating separate testing protocols for each formation type, the digital model universally processes various input parameters (oil composition, water cut, temperature, pressure) and provides optimized demulsifier recommendations. This multi-functional approach maintains high adaptability across different geological formations while reducing the complexity of managing multiple specialized testing procedures.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The patent transforms the complex chemical composition data of various formations into standardized numerical parameters that can be processed by the digital twin model. By converting diverse chemical makeup information into comparable parameter formats (molecular weight distributions, polarity indices, boiling point ranges), the system can adapt to different formations through parameter variation rather than procedural complexity. This allows the same digital framework to handle unique formation characteristics without increasing testing process complexity.

Inventive Principle:
Principle #35Parameter changes

3Reliability

If specialized demulsifiers are designed for specific oil types and production systems, then the effectiveness of water separation is improved, but the cost and environmental impact increase

Engineering Contradiction:
Improvewater separation effectivenessVSAvoidenvironmental impact
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent implements a feedback-driven optimization system where the digital twin model continuously refines demulsifier recommendations based on predicted performance metrics and constraint satisfaction. The model incorporates feedback loops that evaluate water separation effectiveness predictions against environmental constraints and cost parameters, iteratively optimizing the demulsifier composition. This feedback mechanism ensures high reliability of water separation while systematically minimizing environmental impact by selecting greener chemical options that meet performance thresholds.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The patent utilizes parameter optimization to transition from traditional high-dosage demulsifier approaches to optimized lower-dosage formulations. By adjusting key parameters in the digital model (demulsifier concentration, molecular structure parameters, injection timing), the system identifies compositions that achieve effective water separation at reduced chemical dosages. This parameter optimization directly reduces environmental impact and cost while maintaining separation effectiveness, as the digital twin predicts and validates performance at these optimized parameter settings.

Inventive Principle:
Principle #35Parameter changes

Data Source

PatentUS12529690B2Digital bottle test constraint optimization and predictor
Publication Date: 2026.01.20 HALLIBURTON ENERGY SERVICES INC
  • US12529690B2 patent drawing
  • US12529690B2 patent drawing
  • US12529690B2 patent drawing

AI summary

A method can be used to determine the optimal inputs for a bottle test performed by a user for separating water from oil. The bottle test model for predicting inputs to achieve desired KPIs may decrease times required for a user to predict a demulsifier composition. The methods and model may then be utilized for predicting a demulsifier composition based upon inputs of a crude oil product to predict a demulsifier composition for most efficiently separating the oil from water for new production sites.