Direct Stripping Cyclone for Catalyst Separation

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Solution Overview

Problem

Cyclonic separation of particulate-fluid suspensions often results in the entrapment and adsorption of fluid in the accumulated solids, leading to side-reactions and 'delta coking' in catalytic cracking applications, necessitating a method to separate the suspension while stripping entrained fluid and adsorbed hydrocarbons from the solids.

Innovation Solution

An apparatus with a coaxially arranged vessel having a separation section and a stripping section, where a stripping fluid is introduced through nozzles in the apertures of the transition section to remove entrained gases and residual hydrocarbons from the settled particulates, enhancing the separation efficiency by fluidizing the particulate bed and increasing the upward velocity of the stripping fluid.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If cyclonic separation is used to separate particulate-fluid suspensions, then separation efficiency is improved, but fluid entrapment and adsorption in accumulated solids occurs

Engineering Contradiction:
Improveseparation efficiencyVSAvoidfluid entrapment
Core Design Contradiction:
Manufacturing precisionVSLoss of substance

Solution Approach 1:

The separator is divided into two distinct functional sections: a separation section for cyclonic separation and a stripping section for fluid removal. This segmentation allows each section to optimize its specific function without interfering with the other, resolving the contradiction between separation efficiency and fluid entrapment.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The stripping section performs preliminary action by removing entrained and adsorbed fluids from solids before they are discharged from the separator. This prevents fluid entrapment issues downstream and eliminates side-reactions that would occur with residual fluids.

Inventive Principle:
Principle #10Preliminary action

2Productivity

If solids accumulate at low point for removal, then separation is achieved, but side-reactions and delta coking occur due to residual hydrocarbons

Engineering Contradiction:
Improveseparation rateVSAvoidside-reactions
Core Design Contradiction:
ProductivityVSObject-generated harmful factors

Solution Approach 1:

The stripping section performs preliminary action by removing entrained and adsorbed fluids from solids before they are discharged from the separator. This prevents fluid entrapment issues downstream and eliminates side-reactions that would occur with residual fluids.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The upward-flowing stripping fluid creates controlled turbulence and fluidization that converts the harmful effect of fluid entrapment into a beneficial stripping action, effectively removing residual hydrocarbons that would otherwise cause side-reactions.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

3Device complexity

If a single vessel is used for both separation and stripping, then device complexity is reduced, but flow control becomes more difficult

Engineering Contradiction:
Improvenumber of vesselsVSAvoidflow control
Core Design Contradiction:
Device complexityVSEase of operation

Solution Approach 1:

The separator is divided into two distinct functional sections: a separation section for cyclonic separation and a stripping section for fluid removal. This segmentation allows each section to optimize its specific function without interfering with the other, resolving the contradiction between separation efficiency and fluid entrapment.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

A single vessel performs multiple functions: cyclonic separation in the separation section and fluid stripping in the stripping section. This multi-functionality reduces device complexity while maintaining operational control through proper section design and flow distribution.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution effectively increases the catalyst collection efficiency and vapor containment, reducing the amount of gas entrained in solids, and minimizes side-reactions by efficiently stripping residual hydrocarbons from the particulate catalyst, improving the overall separation process.

Implementation Method 1

The centrifugal force generated by the tangential introduction of the suspension to the separator results in the accumulation of a dense solid phase along the walls of the separator, and, through centripetal motion, a less dense fluid phase in the center of the separator

Methodology Applied
Scientific EffectCentrifugal force: Centrifugal Force

Implementation Method 2

enhancing the separation efficiency by fluidizing the particulate bed and increasing the upward velocity of the stripping fluid

Methodology Applied
Scientific EffectFluidization: Fluidisation

Data Source

PatentUS8398751B2Direct stripping cyclone
Publication Date: 2013.03.19 KELLOGG BROWN & ROOT INC
  • US8398751B2 patent drawing
  • US8398751B2 patent drawing
  • US8398751B2 patent drawing

AI summary

Systems and methods for the separation of a particulate-fluid suspension are provided. An apparatus for the separation of a particulate-fluid suspension can include an enclosed vessel having two or more sections disposed coaxially along a common longitudinal centerline, wherein a first section has a first cross sectional area and a second section has a second cross sectional area. A plurality of apertures can be disposed about the second section. The apparatus can have a cylindrical surface, parallel to the longitudinal centerline of the apparatus, disposed within the first section. A fluid distribution channel having a plurality of apertures can be disposed either about an exterior surface or an interior of the apparatus. A plurality of fluid conduits can provide fluid communication between the fluid distribution channel and the plurality of apertures distributed about the second section.