Distillation column minimum flow arrangement

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Distillation columns face inefficiencies and operational challenges when feed rates drop below designed minimum levels, leading to poor separation efficiency and the need for costly upgrades to maintain performance, particularly in NGL stripper units experiencing disruptions from upstream production issues.

Innovation Solution

A minimum flow arrangement is implemented in the distillation system, where a portion of the bottom product is recycled back into the feed through a bottom return line, using a control valve to manage flow rates, thereby maintaining adequate internal loading and separation efficiency without requiring expensive upgrades to mass transfer internals.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If the distillation column operates below minimum feed flow rate, then productivity is reduced, but separation efficiency deteriorates

Engineering Contradiction:
Improvefeed flow rateVSAvoidseparation efficiency
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

A feed surge drum is introduced as an intermediary device between the feed source and the distillation column. The surge drum accumulates feed and releases it at a controlled rate to maintain minimum flow into the column, allowing the system to operate below minimum feed flow rate while preserving separation efficiency through the mediator's flow regulation function.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The system changes the flow rate parameter by recycling a portion of the bottom product back to the feed surge drum through a control valve. This creates a minimum flow arrangement that ensures the distillation column receives adequate flow even when fresh feed is low, thereby maintaining separation efficiency while allowing reduced overall productivity.

Inventive Principle:
Principle #35Parameter changes

2Manufacturing precision

If mass transfer internals are upgraded to handle low flow rates, then separation efficiency is maintained, but device complexity and cost increase

Engineering Contradiction:
Improveseparation efficiencyVSAvoidmass transfer internals
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

Instead of modifying the mass transfer internals, a feed surge drum and control valve are introduced as intermediary devices to regulate flow into the column. This approach maintains separation efficiency through flow management rather than through complex internal modifications, thereby avoiding increased device complexity and cost.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The system uses a portion of its own bottom product output and recycles it back to the feed surge drum to maintain minimum flow. This self-service approach allows the distillation column to maintain separation efficiency using its own product stream, eliminating the need for external upgrades to mass transfer internals.

Inventive Principle:
Principle #25Self-service

3Productivity

If the distillation column operates at low feed rates, then productivity is reduced, but operating cost increases due to inefficient operation

Engineering Contradiction:
Improvefeed flow rateVSAvoidoperating efficiency
Core Design Contradiction:
ProductivityVSLoss of energy

Solution Approach 1:

The feed surge drum and minimum flow arrangement ensure continuous useful action within the distillation column by maintaining minimum flow rates. This prevents the column from operating in an inefficient regime, ensuring that mass transfer processes continue effectively even when overall productivity is reduced, thereby minimizing energy loss and maintaining operating efficiency.

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

The system changes the flow rate parameter by implementing a minimum flow arrangement that recycles bottom product through a control valve. This maintains adequate flow velocity and contact conditions within the column, preventing energy-wasting inefficient operation while allowing reduced overall productivity during low feed availability.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This configuration allows distillation columns to operate effectively even at low feed rates, extending their operational range without the need for sophisticated or costly internal upgrades, thereby reducing capital expenditures and ensuring continuous operation by maintaining separation efficiency.

Implementation Method 1

a distillation column configured for separating a mixed feed into one or more fractional mixtures, producing an overhead product and a bottom product

Methodology Applied
Scientific EffectDistillation: Distillation

Implementation Method 2

A control valve is configured for controlling a flow rate in the bottom return line

Methodology Applied
Scientific EffectFlow control: Valve

Data Source

PatentUS20240350940A1Distillation column minimum flow arrangement
Publication Date: 2024.10.24 SAUDI ARABIAN OIL CO
  • US20240350940A1 patent drawing

AI summary

A distillation system operating below minimum flow. The distillation column is configured for separating a mixed feed into one or more fractional mixtures, producing an overhead product and a bottom product. A bottom return line is provided for returning at least a portion of the bottom product to supplement the mixed feed to the distillation column. A control valve is configured for controlling a flow rate in the bottom return line. A feed surge drum is configured for receiving a feed from the bottom return line and fresh feed, producing the mixed feed.