Distillation Flooding Detection via Differential Pressure Phase Inversion

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Solution Overview

Problem

Distillation processes face challenges in detecting and controlling flooding conditions, which disrupt separation efficiency and can lead to product losses and system downtime, particularly in various distillation systems and processes.

Innovation Solution

A method and system that senses differential pressure signals along a distillation flow path, filters the signal based on frequency, and generates a flooding indicator to detect the onset of flooding, allowing for timely intervention to prevent runaway conditions.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If vapor flow rate is increased to improve distillation throughput, then productivity increases, but flooding risk increases causing separation efficiency to deteriorate

Engineering Contradiction:
Improvedistillation throughputVSAvoidseparation efficiency
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The patent applies preliminary action by detecting early signs of flooding through differential pressure monitoring and phase inversion detection before actual flooding occurs. The system continuously monitors pressure differentials across the distillation column and detects phase inversion in the two-phase flow, providing advance warning that allows operators to adjust vapor flow rates before separation efficiency deteriorates and productivity is compromised

Inventive Principle:
Principle #10Preliminary action

2Productivity

If heating rate is increased to improve distillation output, then productivity increases, but flooding occurs causing system stability to deteriorate

Engineering Contradiction:
Improvedistillation outputVSAvoidprocess stability
Core Design Contradiction:
ProductivityVSStability of the object's composition

Solution Approach 1:

The patent implements feedback control by continuously monitoring differential pressure across the distillation column and using this information to detect flooding conditions. The system measures pressure differentials between multiple points in the column, processes these signals to detect phase inversion, and provides feedback that allows operators to adjust heating rates to maintain process stability while maximizing distillation output

Inventive Principle:
Principle #23Feedback

3Stability of the object's composition

If vapor flow rate is increased to prevent runaway conditions, then system stability improves, but separation efficiency deteriorates due to axial mixing

Engineering Contradiction:
Improveprocess controlVSAvoidseparation efficiency
Core Design Contradiction:
Stability of the object's compositionVSManufacturing precision

Solution Approach 1:

The patent applies preliminary action by detecting early signs of flooding through differential pressure monitoring and phase inversion detection before actual flooding occurs. The system continuously monitors pressure differentials across the distillation column and detects phase inversion in the two-phase flow, providing advance warning that allows operators to adjust vapor flow rates before separation efficiency deteriorates and productivity is compromised

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Effectively detects the onset of flooding, enabling proactive control measures to maintain separation efficiency and prevent system disruptions, adaptable to different distillation systems and processes.

Implementation Method 1

sensing a differential pressure signal along a distillation flow path

Methodology Applied
Scientific EffectDifferential pressure sensing: Pressure Gradient

Implementation Method 2

filtering the signal as a function of frequency

Methodology Applied
Scientific EffectFrequency filtering: Filter (electronic)

Implementation Method 3

The filtered differential pressure signal is responsive to a phase inversion along the flow path

Methodology Applied
Scientific EffectPhase inversion detection: Two-Phase Flow

Data Source

PatentEP2300116B1method and device for the DETECTION OF DISTILLATION COLUMN FLOODING
Publication Date: 2019.02.06 ROSEMOUNT INC
  • EP2300116B1 patent drawingFigure 1
  • EP2300116B1 patent drawingFigure 2A~2B
  • EP2300116B1 patent drawingFigure 3

AI summary

A method comprises sensing a differential pressure signal [64, 74], filtering the differential pressure signal [66, 76], generating a flooding indicator as a function of the filtered differential pressure signal, and indicating the onset of flooding [70, 80]. The differential pressure signal is sensed along a distillation flow path [16]. The filtered differential pressure signal is responsive to a phase inversion along the flow path, and the flooding indicator is responsive to an onset of a flooding condition, based on the phase inversion. The onset of the flooding condition is indicated based on a change in the flooding indicator.