Distillation Tower Radiation Detection for Solid Adherence Control

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Conventional distillation methods face challenges in separating carbon dioxide from methane at cryogenic temperatures, leading to solidification issues and adherence of contaminants to equipment, which interferes with the separation process in natural gas processing.

Innovation Solution

A method and device that utilize a controlled freeze zone in a distillation tower, incorporating a radiation source and detector to monitor radiation levels and determine if solids have adhered to mechanical components, allowing for effective separation of contaminants from hydrocarbons by forming and melting solids under controlled conditions.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional distillation methods are used to separate carbon dioxide from methane at cryogenic temperatures, then separation efficiency is improved, but solidification of CO2 and adherence to equipment occurs

Engineering Contradiction:
Improveseparation efficiencyVSAvoidsolidification and adherence of contaminants
Core Design Contradiction:
ProductivityVSObject-affected harmful factors

Solution Approach 1:

The patent replaces mechanical cleaning methods with radiation detection and heating. Radiation detectors monitor for solid adherence in real-time, and when detected, radiation heating elements melt the solids without mechanical intervention, solving the adherence problem while maintaining separation efficiency

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The patent dynamically changes temperature parameters in the controlled freeze zone. By precisely controlling temperature to remain above the solidification point of CO2 while maintaining cryogenic conditions for separation, the system prevents solidification and adherence while achieving effective contaminant removal

Inventive Principle:
Principle #35Parameter changes

2Reliability

If radiation sources are added to prevent solid adherence, then equipment operation reliability is improved, but device complexity increases

Engineering Contradiction:
Improveequipment operation reliabilityVSAvoiddevice complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent merges the radiation detection and radiation heating functions into a single integrated system. The same radiation infrastructure serves dual purposes: detecting solid adherence and preventing/melting it, thereby improving reliability without proportionally increasing complexity

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The system uses radiation detectors to automatically detect when solids adhere to equipment, triggering radiation heating elements to melt them. This self-monitoring and self-cleaning mechanism improves reliability while minimizing the need for external intervention and complex control systems

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables efficient separation of contaminants from hydrocarbons, preventing adherence and ensuring proper operation of the distillation tower, thereby producing high-quality hydrocarbon products.

Implementation Method 1

detecting radiation emitted by the first radiation source as a first radiation level; detecting radiation emitted by the first radiation source as a second radiation level after detecting the first radiation level

Methodology Applied
Scientific EffectRadiation detection: Radiation

Implementation Method 2

forming solids in a controlled freeze zone section of the distillation tower

Methodology Applied
Scientific EffectSolidification: Freezing

Implementation Method 3

The separation of contaminants from hydrocarbons is difficult and consequently significant work has been applied to the development of hydrocarbon/contaminant separation methods. These methods can be placed into three general classes: absorption by solvents (physical, chemical and hybrids), adsorption by solids, and distillation

Methodology Applied
Scientific EffectDistillation: Distillation

Data Source

PatentUS9829247B2Method and device for separating a feed stream using radiation detectors
Publication Date: 2017.11.28 EXXONMOBIL UPSTREAM RESEARCH COMPANY(US)
  • US9829247B2 patent drawing
  • US9829247B2 patent drawing
  • US9829247B2 patent drawing

AI summary

The present disclosure provides a method for separating a feed stream in a distillation tower. The method may include forming solids in a controlled freeze zone section of the distillation tower; emitting radiation from a first radiation source in the controlled freeze zone section while the controlled freeze zone section forms no solids; detecting radiation emitted by the first radiation source as a first radiation level; detecting radiation emitted by the first radiation source as a second radiation level after detecting the first radiation level; and determining whether the solids adhered to at least one of on and around a first mechanical component included in the controlled freeze zone section based on the first radiation level and the second radiation level.