Divided Wall Column Vapor Control for Heat Integration

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Solution Overview

Problem

Conventional distillation systems for separating multicomponent streams are inefficient in terms of energy use and costly due to poor heat integration and the need for multiple columns, reboilers, condensers, and control circuitry, resulting in a large footprint and high operational expenses.

Innovation Solution

The implementation of a heat-integrated separation system using a divided wall column or thermally coupled columns with active vapor control, which includes a reboiler, condenser, and intermediate sections with vapor-liquid contact elements, allows for improved heat integration and energy efficiency by controlling vapor flow through vapor bypasses and restrictions, reducing the need for separate columns and associated equipment.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If separate distillation columns are used for each component separation, then separation capability is improved, but system complexity and footprint increase

Engineering Contradiction:
Improveseparation capabilityVSAvoidsystem complexity
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The patent combines multiple distillation functions into a single divided wall column that separates multiple components simultaneously. The column contains internal divided walls that create separate separation zones, allowing one column to perform the work of multiple conventional columns while reducing system complexity and footprint.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The divided wall column serves multiple separation functions within a single unit. The internal divided walls enable the column to separate different component ranges (light, intermediate, and heavy components) in simultaneous operations, making the single column universal for multiple separation tasks.

Inventive Principle:
Principle #6Universality (Multi-functionality)

2Manufacturing precision

If separate distillation columns with individual reboilers and condensers are implemented, then separation precision is improved, but energy consumption increases

Engineering Contradiction:
Improveseparation precisionVSAvoidenergy consumption
Core Design Contradiction:
Manufacturing precisionVSUse of energy by moving object

Solution Approach 1:

The patent converts the harmful waste heat from the condenser into a beneficial resource by using it to preheat the feed stream entering the column. This heat integration reduces the energy demand of the reboiler while maintaining separation precision, effectively converting energy waste into useful heating.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Solution Approach 2:

The system recovers thermal energy that would otherwise be discarded in the condenser. By implementing heat exchangers that capture condenser heat and transfer it to the feed stream, the system recovers and reuse thermal energy, reducing overall energy consumption while maintaining separation effectiveness.

Inventive Principle:
Principle #34Discarding and recovering

3Ease of operation

If conventional distillation systems are used, then ease of operation is maintained, but operational costs increase due to poor heat integration

Engineering Contradiction:
Improveoperational simplicityVSAvoidenergy waste
Core Design Contradiction:
Ease of operationVSLoss of energy

Solution Approach 1:

The patent converts the harmful waste heat from the condenser into a beneficial resource by using it to preheat the feed stream entering the column. This heat integration reduces the energy demand of the reboiler while maintaining separation precision, effectively converting energy waste into useful heating.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Solution Approach 2:

The system uses its own internal heat streams to serve its heating needs. The condenser heat automatically preheats the feed stream through integrated heat exchangers, creating a self-sustaining thermal system that reduces external energy requirements without adding operational complexity.

Inventive Principle:
Principle #25Self-service

4Measurement precision

If multiple control valves and control circuitry are added to each column, then control precision is improved, but device complexity increases

Engineering Contradiction:
Improvecontrol precisionVSAvoidcontrol system complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent consolidates control functions by implementing a single control valve at the column overhead that regulates total vapor flow. This unified control approach replaces multiple individual control valves and simplifies the control system while maintaining adequate control precision for the combined separation process.

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enhances energy efficiency, reduces equipment costs and footprint, and provides better control over product composition during disturbances, leading to lower energy consumption and operational costs while maintaining product purity.

Implementation Method 1

a reboiler to receive liquid from a lower end of the column and to provide vapor to the lower end of the stripping section

Methodology Applied
Scientific EffectEvaporation: Evaporation

Implementation Method 2

a condenser to receive vapor from an upper end of the rectifying section and to provide liquid to the upper end of the rectifying section

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 3

intermediate sections with vapor-liquid contact elements

Methodology Applied
Scientific EffectMass transfer: Diffusion

Data Source

PatentUS11103804B2Heat integrated separation system with active vapor control
Publication Date: 2021.08.31 GTI SOLUTIONS INTERNATIONAL LLC
  • US11103804B2 patent drawing
  • US11103804B2 patent drawing
  • US11103804B2 patent drawing

AI summary

A separation system includes a column including a stripping section proximal to a lower end of the column, a rectifying section proximal to an upper end of the column, and an intermediate section disposed between the stripping section and the rectifying section. The intermediate section includes first and second vertical sides separated by a vertical wall. The column includes a feed port to receive a material stream to be separated. The separation system further includes a reboiler in fluid communication with the column. The reboiler provides vapor to the stripping section. The separation system also includes a condenser in fluid communication with the column. The condenser provides liquid to the rectifying section, the condenser to provide a distillate effluent stream. The separation system further includes an active vapor control to control the relative vapor flow rate to the first and second sections.