DLC:Si:B Coating for High-Temperature Cutting Tools

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Solution Overview

Problem

Traditional DLC coatings exhibit limitations in heat resistance and oxidation resistance, particularly in high-efficiency cutting tools and engine components, where increased heat and interfacial pressure lead to early abrasion and friction issues, necessitating enhanced hardness, lubricity, and heat resistance.

Innovation Solution

A multilayer film coating comprising carbon, silicon, boron, and additional modifying elements like nitrogen and oxygen, with a specific chemical composition and deposition method that includes a hydrocarbon-based gas to enhance carbon content and lubrication characteristics, forming a stable and adhesive hard film with improved heat resistance and lubricity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If traditional DLC coatings are used, then sliding characteristics and friction reduction are achieved, but heat resistance and oxidation resistance are limited to ca. 350-400°C phase stability and ca. 400-500°C oxidation in air

Engineering Contradiction:
Improveheat resistanceVSAvoidoxidation resistance
Core Design Contradiction:
TemperatureVSReliability

Solution Approach 1:

The patent applies composite materials by combining carbon with silicon and boron to form a DLC:Si:B coating. This composite structure integrates the low friction properties of carbon with the high-temperature stability of silicon and boron, achieving phase stability up to 700°C and oxidation resistance up to 900°C while maintaining sliding characteristics.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent changes the compositional parameters of the coating by incorporating specific amounts of silicon (0.1-5 at%) and boron (0.1-5 at%) into the carbon matrix. This parameter modification transforms the coating from conventional DLC with limited heat resistance to a high-temperature resistant coating stable up to 700°C.

Inventive Principle:
Principle #35Parameter changes

2Productivity

If cutting speed is accelerated for high-efficiency operation, then productivity is improved, but working heat increases causing greater tool damage

Engineering Contradiction:
Improvecutting speedVSAvoidworking heat
Core Design Contradiction:
ProductivityVSTemperature

Solution Approach 1:

The DLC:Si:B composite coating enables high-speed cutting by providing simultaneous resistance to both the mechanical wear from high cutting speeds and the thermal damage from increased working heat. The silicon and boron components specifically address the heat resistance issue, allowing sustained high-speed operation.

Inventive Principle:
Principle #40Composite materials

3Productivity

If feeding amount is increased for high-efficiency operation, then productivity is improved, but interfacial pressure increases causing early-stage abrasion

Engineering Contradiction:
Improvefeeding amountVSAvoidabrasion resistance
Core Design Contradiction:
ProductivityVSStrength

Solution Approach 1:

The composite coating structure combines carbon's inherent abrasion resistance with the reinforcing effects of silicon and boron. This creates a coating that can withstand the increased interfacial pressure from higher feeding rates without suffering early-stage abrasion, enabling sustained high-productivity operation.

Inventive Principle:
Principle #40Composite materials

4Loss of substance

If lubricant amount is reduced, then environmental performance is improved, but friction must be decreased through coating properties

Engineering Contradiction:
Improvelubricant consumptionVSAvoidfriction characteristics
Core Design Contradiction:
Loss of substanceVSEase of operation

Solution Approach 1:

The DLC:Si:B coating provides self-lubricating properties through its carbon-rich composition and amorphous structure, reducing friction and wear without requiring external lubricants. The coating itself serves the lubrication function, enabling operation with minimal or no lubricant while maintaining excellent friction characteristics.

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The coating achieves significantly enhanced heat resistance and lubricity, maintaining excellent frictional characteristics up to 500°C and providing improved abrasion resistance, outperforming conventional DLC coatings in high-temperature and high-pressure environments.

Implementation Method 1

a multilayer film for a member, which is coated with a hard film A comprising carbon, silicon and boron

Methodology Applied
Scientific EffectPhysical Vapour Deposition: Physical Vapour Deposition

Implementation Method 2

a specific chemical composition and deposition method that includes a hydrocarbon-based gas to enhance carbon content and lubrication characteristics

Methodology Applied
Scientific EffectChemical Vapour Deposition: Chemical Vapour Deposition

Data Source

PatentEP2443267B1Protective coating, a coated member having a protective coating as well as method for producing a protective coating
Publication Date: 2020.01.08 OERLIKON SURFACE SOLUTIONS AG PFAFFIKON
  • EP2443267B1 patent drawingFigure 1
  • EP2443267B1 patent drawingFigure 1a
  • EP2443267B1 patent drawingFigure 2

AI summary

The invention relates to a protective coating, having the chemical composition CaSibBdNeOgHlMem, wherein Me is at least one metal of the group consisting of {Al, Ti, V, Cr, Zr, Nb, Mo, Hf, Ta, W, Y, Sc, La, Ce, Nd, Pm, Sm, Pr, Mg, Ni, Co, Fe, Mn}, with a+b+d+e+g+1+m =1. According to the invention, the following conditions are satisfied: 0.45 = a = 0.98, 0.01 = b = 0.40, 0.01 = d = 0.30, 0 = e = 0.35, 0 = g = 0.20, 0 = 1 = 0.35, 0 = m = 0.20. The invention relates also to a coated member having a protective coating, as well as to a method for producing a protective coating, in particular a multilayer film for a member.