3D DNA Nanostructures for Single Molecule Quantification

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Solution Overview

Problem

Current gene expression profiling (GEP) methods face challenges in achieving simultaneous, high-specificity, and high-sensitivity analysis of multiple genes while being cost-effective, fast, and easy to use, due to issues such as enzymatic errors, long processing times, and complex, expensive equipment.

Innovation Solution

A method utilizing 3D DNA nanostructures and micro-well arrays for the direct detection and quantification of target mRNA molecules, which involves introducing host bodies with target structures into micro-wells, binding 3D DNA nanostructures specifically to the target structures, and measuring fluorescence signals to distinguish bound from unbound nanostructures.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Difficulty of detecting and measuring

If enzymatic reactions (reverse transcription and PCR amplification) are used for GEP analysis, then the detection capability is improved, but systematic errors occur and quantification becomes inaccurate

Engineering Contradiction:
Improvedetection capabilityVSAvoidquantification accuracy
Core Design Contradiction:
Difficulty of detecting and measuringVSMeasurement precision

Solution Approach 1:

The patent replaces enzymatic reactions (chemical/biological processes) with direct hybridization and fluorescence detection (physical/optical processes). This substitution eliminates systematic errors from enzymatic amplification while maintaining detection capability through direct labeling of target molecules with fluorescent reporters.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The patent uses fluorescent DNA reporters as copies that hybridize to target mRNA molecules. These reporter molecules carry fluorescent labels that enable direct detection and quantification without requiring enzymatic amplification of the original target, thus avoiding amplification errors.

Inventive Principle:
Principle #26Copying

2Productivity

If microarray-based methods are used for parallel detection, then the number of detectable sequences increases, but the process time becomes too long for clinical applications

Engineering Contradiction:
Improveparallel detection capabilityVSAvoidprocess time
Core Design Contradiction:
ProductivityVSLoss of time

Solution Approach 1:

The patent extracts the fluorescent reporter molecules from the complex microarray surface hybridization process. By using free-floating fluorescent reporters that hybridize to targets in solution, the method eliminates the time-consuming surface binding and washing steps inherent to microarray methods, dramatically reducing process time while maintaining parallel detection capability.

Inventive Principle:
Principle #2Taking out (Extraction)

3Measurement precision

If dPCR is used for accurate quantification, then the measurement precision improves, but the method is limited to typically two targets

Engineering Contradiction:
Improvequantification accuracyVSAvoidnumber of detectable targets
Core Design Contradiction:
Measurement precisionVSAdaptability or versatility

Solution Approach 1:

The patent creates a universal detection system where multiple fluorescent reporters with different spectral properties can simultaneously detect multiple different target mRNA sequences. Each reporter-target combination provides specific quantification, enabling accurate measurement of many genes in parallel within a single reaction mixture, thus achieving both precision and versatility.

Inventive Principle:
Principle #6Universality (Multi-functionality)

4Measurement precision

If nCounter system is used for enzyme-free detection, then the quantification accuracy improves, but complex purification steps and expensive equipment are required

Engineering Contradiction:
Improvequantification accuracyVSAvoidequipment complexity and cost
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent uses simple, inexpensive fluorescently labeled DNA reporters that can be synthesized commercially at low cost. These disposable-like reporters are used in straightforward hybridization reactions that require only basic laboratory equipment, eliminating the need for expensive specialized instruments while maintaining accurate quantification.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

5Difficulty of detecting and measuring

If fluorescent reporters are stretched after surface immobilization for barcode reading, then the detection capability is improved, but about 80% of target molecules are excluded by unidentifiable barcodes

Engineering Contradiction:
Improvedetection capabilityVSAvoididentification reliability
Core Design Contradiction:
Difficulty of detecting and measuringVSReliability

Solution Approach 1:

The patent inverts the conventional approach by reading the fluorescent barcode signals while the reporters are still in solution or loosely associated with the target, before any stretching or surface immobilization is required. This reversal ensures that all hybridized reporters remain identifiable, eliminating the 80% loss of unidentifiable barcodes while maintaining detection capability.

Inventive Principle:
Principle #13The other way round (Inversion)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables precise, rapid, and cost-effective quantification of multiple target molecules with reduced false positives and negatives, allowing for efficient molecular and phenotypic analysis of individual cells or structures.

Implementation Method 1

The 3D DNA nanostructures and the parameters of the fluorescence measurement are selected such that the at least one measured fluorescence signal of the identification structure formed in a) differs from the fluorescence signal of each of the at least two isolated 3D DNA nanostructures

Methodology Applied
Scientific EffectHybridization:

Implementation Method 2

each of the 3D DNA nanostructures having one or more internal fluorescent dye molecules; Detection of the target structure by measuring at least one fluorescence signal

Methodology Applied
Scientific EffectFluorescence: Fluorescence

Data Source

PatentEP3498865B1Single molecule detection or quantification by means of DNA nanotechnology in micro-wells
Publication Date: 2020.10.07 LUDWIG MAXIMILIANS UNIV MUNCHEN
  • EP3498865B1 patent drawingFigure 1
  • EP3498865B1 patent drawingFigure 2
  • EP3498865B1 patent drawingFigure 3

AI summary

The present invention relates to a method and a DNA nanostructure for the detection of a target structure. In particular, the present invention relates to a DNA nanostructure which, through a suitable choice of its shape and the placement of marker molecules attached to it, ensures a preferably linear dependence of the number of marker molecules and the measurement signal, independent of the spatial arrangement of several such DNA nanostructures. Furthermore, the invention relates to the use of these DNA nanostructures and other nanoreporters, preferably in combination with adapters, which bind specifically to target molecules, in a method for the preferably simultaneous quantification of a plurality of target molecules by a multiplex technique. The method particularly relates to single-cell analysis.