Doped Lithium Transition Metal Oxide for Low-Gas Cathode Additives

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Solution Overview

Problem

Existing lithium secondary batteries face challenges in increasing capacity and efficiency due to irreversible reactions and gas generation during charging and discharging, particularly with over-lithiated positive electrode materials like Li6CoO4, which can lead to pressure buildup and safety risks.

Innovation Solution

A lithium transition metal oxide, represented by Li6Co1-x-yZnxMyO4, is introduced with hetero-elements such as Al, Zn, or other transition metals to stabilize the crystal phase, minimizing side reactions and gas generation by suppressing oxidative properties of Co4+ cations, thereby enhancing safety and lifespan.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Loss of substance

If over-lithiated positive electrode material (Li6CoO4) is used to compensate for lithium loss in the negative electrode, then lithium loss is reduced, but gas generation increases causing pressure buildup and safety risks

Engineering Contradiction:
Improvelithium lossVSAvoidgas generation
Core Design Contradiction:
Loss of substanceVSObject-generated harmful factors

Solution Approach 1:

The patent modifies the chemical composition parameters of the positive electrode material by introducing hetero-elements (Mg, Al, Ti, Zr, Nb) to replace some Co4+ cations. This changes the electrochemical properties to reduce gas-generating side reactions while maintaining lithium release capability. The specific composition ratios (0.01 ≤ x ≤ 0.50 for hetero-element content) are optimized parameters to balance lithium compensation and gas suppression.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite positive electrode material combining Li6CoO4 with hetero-element dopants (Mg, Al, Ti, Zr, Nb). This composite structure maintains the high-capacity lithium release properties of Li6CoO4 while the hetero-elements suppress unwanted side reactions with the electrolyte, reducing gas generation. The composite material integrates multiple functional properties in a single electrode component.

Inventive Principle:
Principle #40Composite materials

2Quantity of substance

If Li6CoO4 is used as sacrificial positive electrode material, then initial capacity is improved, but crystal phase instability occurs leading to continuous gas generation

Engineering Contradiction:
Improveinitial capacityVSAvoidcrystal phase stability
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

The patent stabilizes the crystal phase by introducing hetero-elements that modify the lattice structure parameters. The dopants (Mg2+, Al3+, Ti4+, Zr4+, Nb5+) have different ionic radii and charges compared to Co4+, which stabilizes the spinel structure and prevents Jahn-Teller distortion. This maintains the crystal phase stability while preserving the high initial capacity needed for lithium compensation.

Inventive Principle:
Principle #35Parameter changes

3Quantity of substance

If high-capacity negative electrode material (metal or metal oxide) is used to increase battery capacity, then capacity increases, but volume change during charging/discharging increases making it difficult to achieve 15% or more content

Engineering Contradiction:
Improvebattery capacityVSAvoidvolume stability
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

The patent applies preliminary anti-action by using the Li6CoO4-based positive electrode material to pre-compensate for lithium loss that would otherwise occur during negative electrode formation. This preliminary lithium compensation prevents the need for excessive metal oxide content in the negative electrode, thereby reducing volume expansion issues while still achieving high capacity.

Inventive Principle:
Principle #9Preliminary anti-action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The stabilized lithium transition metal oxide suppresses gas generation and maintains excellent battery performance by stabilizing the crystal phase, improving safety and extending the lifespan of lithium secondary batteries.

Implementation Method 1

minimizing side reactions and gas generation by suppressing oxidative properties of Co4+ cations

Methodology Applied
Scientific EffectOxidation suppression: Oxidation

Data Source

PatentEP4084151B1Lithium transition metal oxide, positive electrode additive for lithium secondary battery, and lithium secondary battery comprising same
Publication Date: 2026.01.28 LG CHEM LTD
  • EP4084151B1 patent drawingFigure 1
  • EP4084151B1 patent drawingFigure 2
  • EP4084151B1 patent drawingFigure 3

AI summary

The present disclosure relates to a lithium transition metal oxide, a positive electrode additive for a lithium secondary battery, and a lithium secondary battery including the same. According to the present disclosure, there is provided a lithium transition metal oxide capable of minimizing a side reaction with an electrolyte, thereby suppressing the generation of gas during charging and discharging of a lithium secondary battery.