Doped Solid-State Electrolyte Composition for Stable Lithium Anode Contact

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Solution Overview

Problem

Conventional solid-state batteries face issues with the detachment of the solid-state electrolyte from the anode, which affects their stability and safety, and existing materials often have low ionic conductivity.

Innovation Solution

A compound represented by Formula 1: Li4+dH+ < h Sr 2-x M1 a+< x Zr 1-y M2 b+< y O 6-z X c-< z, where M1 and M2 are cationic dopants in the Sr and Zr sites, and X is an anion dopant in the O site, providing enhanced ionic conductivity and stability against lithium metal.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If solid-state electrolyte is used to improve safety, then safety is improved, but detachment from anode occurs

Engineering Contradiction:
ImprovesafetyVSAvoiddetachment
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The patent modifies the chemical composition parameters of the solid-state electrolyte by incorporating specific dopants (M1, M2, X) into the Li4Sr2ZrO6 structure. This changes the physical and chemical properties of the electrolyte to improve both safety and adhesion to the anode, resolving the contradiction between safety improvement and detachment prevention.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite solid-state electrolyte material by combining Li4Sr2ZrO6 with multiple dopants (M1 at Sr sites, M2 at Zr sites, and X at O sites). This composite approach enhances both the safety characteristics and the interfacial adhesion properties, simultaneously addressing both requirements.

Inventive Principle:
Principle #40Composite materials

2Reliability

If conventional solid-state electrolyte materials are used, then safety is improved, but ionic conductivity is low

Engineering Contradiction:
ImprovesafetyVSAvoidionic conductivity
Core Design Contradiction:
ReliabilityVSUse of energy by moving object

Solution Approach 1:

The patent optimizes the ionic conductivity by carefully controlling the dopant concentrations and stoichiometric ratios in the Li4+dSr2-xM1a+xZr1-yM2b+ 106-zXc- 10z compound. The parameter optimization enables high ionic conductivity while maintaining the safety benefits of solid-state electrolytes.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent introduces localized dopant atoms at specific crystallographic sites (M1 at Sr sites, M2 at Zr sites, X at O sites) to create local structural modifications that enhance ion transport pathways. This local quality enhancement improves bulk ionic conductivity without compromising overall material safety.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The compound achieves high ionic conductivity of about 0.3 mS/cm at room temperature and improved stability, reducing the risk of detachment and enhancing the performance of solid-state batteries.

Implementation Method 1

the compound has an ionic conductivity of about 0.3 mS/cm or greater at room temperature

Methodology Applied
Scientific EffectIonic conductivity: Conduction (electrical)

Data Source

PatentEP4296234A1Solid-state electrolyte material and solid-state battery utilizing the same
Publication Date: 2023.12.27 SAMSUNG ELECTRONICS CO LTD
  • EP4296234A1 patent drawingFigure 1
  • EP4296234A1 patent drawingFigure 2
  • EP4296234A1 patent drawingFigure 3

AI summary

A compound represented by Formula 1:          Li4+dH+hSr2-xM1a+xZr1-yM2b+yO6-zXc-z, wherein in Formula 1, M1 is a cationic dopant in Sr site with a valance of a+; a is 1, 2 or 3; M2 is a cationic dopant in Zr site with a valance of b+; b is 2, 3, 4 or 5; X is an anion dopant in O site with a valence of c-; c is 1, 2, or 3; 0 ≤ h ≤ 2, 0 ≤ x ≤ 2, 0 ≤ y ≤ 1, 0 ≤ z ≤ 0.5, x+y+z+h ≥ 0, d=(2-a)*x+(4-b)*y-(2-c)*z-h, and d ≥ 0.