Doped Nickel Cathode Material for High-Temperature Cycle Stability

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Solution Overview

Problem

Lithium-ion secondary batteries using nickel-containing lithium composite oxides exhibit poor high-temperature cycling performance due to structural instability and cracking of the positive electrode active material.

Innovation Solution

A positive electrode active material is developed, comprising secondary particles formed by agglomeration of primary particles with a layered nickel-containing lithium composite oxide that includes a doping element. This material is designed to maintain a maximum lattice shrinkage rate of ≤2.69% in the a-axis direction and ≤2.75% in the c-axis direction during charging from an 11% delithiated state to a 78% delithiated state at a rate of 0.1C.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If nickel-containing lithium composite oxide is used as positive electrode active material, then energy density and capacity performance are improved, but high-temperature cycling performance deteriorates due to structural instability and cracking

Engineering Contradiction:
Improvecapacity performanceVSAvoidhigh-temperature cycling performance
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent applies parameter changes by precisely controlling the lattice shrinkage rate in the a-axis direction and swelling rate in the c-axis direction to specific ranges (Δa max ≤ 2.69% and Δc max ≤ 2.75%). This parameter control prevents excessive structural deformation during charging, thereby improving high-temperature cycling performance while maintaining high capacity performance from nickel-containing lithium composite oxide.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses composite materials by forming secondary particles through agglomeration of multiple primary particles. This composite structure enhances structural stability and prevents cracking during high-temperature cycling, while the nickel-containing lithium composite oxide maintains its high energy density and capacity performance.

Inventive Principle:
Principle #40Composite materials

2Quantity of substance

If nickel-containing lithium composite oxide is used as positive electrode active material, then energy density is improved, but structural stability deteriorates leading to particle cracking

Engineering Contradiction:
Improveenergy densityVSAvoidstructural stability
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

The patent applies parameter changes by precisely controlling the lattice shrinkage rate in the a-axis direction and swelling rate in the c-axis direction to specific ranges (Δa max ≤ 2.69% and Δc max ≤ 2.75%). This parameter control prevents excessive structural deformation during charging, thereby improving high-temperature cycling performance while maintaining high capacity performance from nickel-containing lithium composite oxide.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses composite materials by forming secondary particles through agglomeration of multiple primary particles. This composite structure enhances structural stability and prevents cracking during high-temperature cycling, while the nickel-containing lithium composite oxide maintains its high energy density and capacity performance.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The proposed positive electrode active material enhances the structural stability and capacity of lithium-ion secondary batteries, significantly improving their high-temperature cycling performance and energy density.

Implementation Method 1

when the positive electrode active material is charged from an 11% delithiated state to a 78% delithiated state at a rate of 0.1C, a lattice of the primary particles has a maximum shrinkage rate satisfying Δamax ≤ 2.69% in an a-axis direction, and a maximum swelling rate satisfying Δcmax ≤ 2.75% in a c-axis direction

Methodology Applied
Scientific EffectLattice shrinkage and swelling: Thermal Expansion

Implementation Method 2

Lithium-ion secondary batteries are rechargeable batteries that operate mainly depending on migration of lithium ions between a positive electrode and a negative electrode

Methodology Applied
Scientific EffectIon migration: Diffusion

Data Source

PatentEP3944379B1Positive electrode active material, preparation method therefor, positive electrode plate, lithium ion secondary battery, and battery module, battery pack and device comprising lithium ion secondary battery
Publication Date: 2025.02.12 CONTEMPORARY AMPEREX TECHNOLOGY (HONG KONG) LIMITED
  • EP3944379B1 patent drawingFigure 1~2
  • EP3944379B1 patent drawingFigure 3~4
  • EP3944379B1 patent drawingFigure 5~6

AI summary

A positive electrode active material and a preparation method thereof, a positive electrode plate, a lithium-ion secondary battery (5), and a battery module (4), a battery pack (1), and apparatus containing the lithium-ion secondary battery (5) are provided. The positive electrode active material includes secondary particles formed by agglomeration of primary particles, where the primary particles include a layered nickel-containing lithium composite oxide, and the nickel-containing lithium composite oxide includes a doping element; and when the positive electrode active material is charged from an 11% delithiated state to a 78% delithiated state at a rate of 0.1C, a lattice of the primary particles has a maximum shrinkage rate satisfying Δamax ≤ 3.00% in an a-axis direction, and a maximum swelling rate satisfying Δcmax ≤ 3.02% in a c-axis direction.