Droplet Jet Reaction Chamber for Uniform Cathode Particles

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Solution Overview

Problem

Conventional manufacturing processes for lithium ion battery cathode active materials are costly, time-consuming, and result in inconsistent quality due to challenges in producing uniform particles with desired crystal structures and morphologies, leading to low energy density and cycle life.

Innovation Solution

A processing system that jets a liquid mixture into droplets and disperses them with gases in a reaction chamber to form particulate materials, allowing for continuous production of high-quality active electrode materials with controlled particle size and morphology, reducing manufacturing time and energy consumption.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Stability of the object's composition

If conventional solid-state processes (grinding and pyrolysis at extreme high temperature) are used to prepare graphite materials, then the crystal structure is formed, but the manufacturing time and energy consumption are extremely high

Engineering Contradiction:
Improvecrystal structureVSAvoidenergy consumption
Core Design Contradiction:
Stability of the object's compositionVSUse of energy by stationary object

Solution Approach 1:

The patent changes the physical state parameter from solid-state to liquid-state processing. By dissolving precursors in a liquid medium and using controlled precipitation, the process achieves crystal formation at much lower temperatures and shorter times compared to conventional solid-state pyrolysis at 3000°C

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent performs preliminary mixing of precursors in a liquid solution before precipitation, ensuring homogeneous distribution of elements. This preliminary homogenization in liquid phase eliminates the need for extensive high-temperature solid-state reaction and grinding steps

Inventive Principle:
Principle #10Preliminary action

2Ease of manufacture

If conventional manufacturing processes are used for cathode active materials, then production can be performed with existing equipment, but the quality consistency is poor due to difficulty in producing uniform particles with desired crystal structures and morphologies

Engineering Contradiction:
Improvemanufacturing processVSAvoidparticle uniformity
Core Design Contradiction:
Ease of manufactureVSManufacturing precision

Solution Approach 1:

The patent enables local control of particle properties through controlled precipitation conditions. By adjusting local parameters such as precipitation rate, temperature, and stirring speed in the liquid medium, uniform particles with consistent crystal structures and morphologies are achieved

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent introduces a liquid medium as an intermediary between precursors and final product. This liquid medium facilitates homogeneous mixing and controlled precipitation, acting as a mediator that enables precise control over particle formation and improves quality consistency

Inventive Principle:
Principle #24Intermediary (Mediator)

3Device complexity

If conventional batch processing methods are used, then equipment complexity is low, but productivity is low due to long manufacturing time and high labor requirements

Engineering Contradiction:
Improveprocessing equipmentVSAvoidproduction rate
Core Design Contradiction:
Device complexityVSProductivity

Solution Approach 1:

The patent enables continuous processing by replacing batch operations with continuous liquid-phase synthesis. The liquid medium allows for continuous feeding of precursors, continuous stirring, and continuous product formation, significantly increasing productivity while maintaining relatively simple equipment

Inventive Principle:
Principle #20Continuity of useful action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The system enables the production of high-quality, consistent active materials with improved energy density and cycle life, reducing production time, labor, and costs compared to conventional methods.

Implementation Method 1

an array of one or more power jet modules adapted to jet the liquid mixture into one or more streams of droplets and to force the one or more streams of droplets into the processing system

Methodology Applied
Scientific EffectGas pressure: Pressure Increase

Implementation Method 2

a dispersion chamber adapted to disperse the one or more gas flows with the one or more streams of droplets jetted from the one or more power jet modules such that gas flows of the one or more gases and droplets streams of the one or more streams of droplets are dispersed into each other

Methodology Applied
Scientific EffectGas-liquid dispersion: Dispersion (of waves)

Implementation Method 3

a reaction chamber adapted to receive the gas-liquid mixture and to process the gas-liquid mixture at a temperature sufficient to form the particulate material

Methodology Applied
Scientific EffectThermal processing: Heating

Data Source

PatentUS12168209B2Processing system and method for producing a particulate material
Publication Date: 2024.12.17 EJOULE INC
  • US12168209B2 patent drawing
  • US12168209B2 patent drawing
  • US12168209B2 patent drawing

AI summary

A processing system and method of producing a particulate material from a liquid mixture are provided. The processing system generally includes a system inlet connected to one or more gas lines to deliver one or more gases into the processing system, one or more power jet modules adapted to jet a liquid mixture into one or more streams of droplets and to force the one or more streams of droplets into the processing system, and a reaction chamber adapted to deliver the one or more streams of droplets in the presence of the one or more gases and process the one or more streams of droplets into the particulate material. The method includes delivering one or more gases into a processing system, jetting the liquid mixture into one or more first droplets streams using one or more power jet modules of the processing system and into the processing system, and reacting the one or more first droplets streams delivered from the processing chamber inside a reaction chamber of the processing system in the presence of the one or more gases into the particulate material at a first temperature.