Dry Powder Thermosetting Resin Composition for Electrostatic Spraying

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Solution Overview

Problem

Existing dry powder compositions for bonding agents often require solvents for processing, leading to increased production and shipping costs and environmental concerns, and lack optimal particle size distributions for efficient electrostatic spraying applications.

Innovation Solution

A dry powder composition comprising a thermosetting resin with a specific particle size distribution (Dv90 ≤ 50 μm, Dv50 between 5.1 and 12.5 μm, and a narrow distribution ratio of 1.5 to 4.2) is developed, achieved through jet milling, suitable for electrostatic spraying and fluidized bed dipping, and includes a curative and optional anti-caking additives and anti-corrosive pigments.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of operation

If wet spraying or roller coating processes are used with solvent-based bonding agents, then application flexibility is improved, but production costs and environmental impact worsen due to solvent removal requirements

Engineering Contradiction:
Improveapplication flexibilityVSAvoidproduction cost
Core Design Contradiction:
Ease of operationVSEase of manufacture

Solution Approach 1:

The invention changes the physical state parameter of the bonding agent from liquid (solvent-based) to solid (dry powder), eliminating the need for solvent removal processes while maintaining application effectiveness through controlled particle size distribution

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention extracts and removes the solvent component from the bonding agent formulation, leaving only the essential thermosetting resin and curative components in dry powder form, thereby eliminating all costs and environmental issues associated with solvent handling

Inventive Principle:
Principle #2Taking out (Extraction)

2Manufacturing precision

If particle size is reduced to improve coating uniformity, then coating quality improves, but fluidization performance worsens due to excessive fine particles

Engineering Contradiction:
Improvecoating uniformityVSAvoidfluidization performance
Core Design Contradiction:
Manufacturing precisionVSEase of operation

Solution Approach 1:

The invention optimizes the particle size distribution parameters within a specific range (Dv10: 3-8 μm, Dv50: 8-15 μm, Dv90: 15-30 μm) to achieve the optimal balance between coating uniformity and fluidization performance, rather than simply minimizing particle size

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention creates different particle size zones within the distribution - finer particles (Dv10) for coating uniformity and slightly coarser particles (Dv90) for fluidization - allowing each portion of the distribution to serve its specific function

Inventive Principle:
Principle #3Local quality

3Ease of operation

If particles larger than 30 μm are present, then fluidization is improved, but coat weight increases unnecessarily

Engineering Contradiction:
ImprovefluidizationVSAvoidcoat weight control
Core Design Contradiction:
Ease of operationVSManufacturing precision

Solution Approach 1:

The invention sets the Dv90 parameter to 15-30 μm, establishing an upper particle size limit that prevents excessive coat weight while maintaining sufficient particle size for adequate fluidization performance

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The composition provides a cost-effective, environmentally friendly bonding agent with improved coating uniformity and adhesion performance, suitable for various applications including brake pads and rubber compounds, while maintaining bonding strength and durability.

Implementation Method 1

jet milling, suitable for electrostatic spraying and fluidized bed dipping

Methodology Applied
Scientific EffectJet milling: Jet Erosion

Implementation Method 2

electrostatic spraying is a coating method which uses a spray gun to create an electrical charge on powder particles, while the substrate to be coated is grounded (made neutral)

Methodology Applied
Scientific EffectElectrostatic deposition: Electrostatic Deposition

Implementation Method 3

the powder to be used as coating is fluidized using air

Methodology Applied
Scientific EffectFluidization: Fluidisation

Data Source

PatentUS11584858B2Dry powder thermosetting resin composition
Publication Date: 2023.02.21 HB FULLER CO

AI summary

The present invention discloses a dry powder composition comprising a thermosetting resin in particulate form, wherein the dry powder composition has a particle size measured according to ISO 13320 (2009) characterized by a Dv90 of 50 μm or lower, a Dv50 in the range of 5.1 to 12.5 μm, and a ratio ofDv⁢⁢90-Dv⁢⁢10Dv⁢⁢50in the range of 1.5 to 4.2. The present invention also discloses processes for preparing the dry powder using jet milling, and processes of applying the dry powder composition to a metal surface. Furthermore, the present invention discloses the uses of the dry powder composition as a bonding material or as an adhesion promoter in a polymer compound.