Dual-Doped Cathode Material for Capacity and Thermal Stability

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Solution Overview

Problem

Lithium-nickel composite oxides used in lithium secondary batteries have poor thermal stability, leading to battery rupture and ignition due to internal short circuits, and substituting nickel with cobalt or manganese results in compromised thermal stability and output characteristics.

Innovation Solution

A positive electrode active material comprising a lithium layer doped with a first doping element and a transition metal layer doped with a second doping element, with an I(003)/I(006) peak intensity ratio in X-ray diffraction measurement of 23.8 or less, is developed, improving thermal stability and cell characteristics.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If lithium-nickel composite oxide is used as positive electrode active material, then reversible capacity is improved, but thermal stability deteriorates

Engineering Contradiction:
Improvereversible capacityVSAvoidthermal stability
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The patent applies local quality by creating distinct doped regions within the cathode material structure. Specifically, magnesium is doped into the lithium layer while aluminum is doped into the transition metal layer, creating localized compositional variations that provide different functional properties in different regions of the material, thereby achieving both high capacity and thermal stability

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent employs composite materials by combining multiple elements (lithium, nickel, magnesium, aluminum, and other transition metals) into a multi-element composite oxide structure. This composite approach allows the material to simultaneously exhibit high reversible capacity from the nickel content and improved thermal stability from the magnesium and aluminum doping, resolving the contradiction between capacity and thermal stability

Inventive Principle:
Principle #40Composite materials

2Productivity

If nickel is substituted with cobalt, then charge and discharge characteristics are improved, but thermal stability deteriorates

Engineering Contradiction:
Improvecharge and discharge characteristicsVSAvoidthermal stability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent applies parameter changes by precisely controlling the doping concentrations of magnesium and aluminum, as well as the overall composition ratios of the cathode material. By optimizing these compositional parameters, the material achieves excellent charge and discharge characteristics while maintaining high thermal stability, avoiding the thermal stability issues associated with cobalt substitution

Inventive Principle:
Principle #35Parameter changes

3Reliability

If nickel is substituted with manganese, then thermal stability is improved, but output characteristics deteriorate

Engineering Contradiction:
Improvethermal stabilityVSAvoidoutput characteristics
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

The patent applies local quality by placing magnesium specifically in the lithium layer and aluminum in the transition metal layer, creating localized functional regions. This spatial differentiation allows the material to achieve both improved thermal stability and maintained output characteristics, avoiding the output deterioration that occurs with direct nickel-manganese substitution

Inventive Principle:
Principle #3Local quality

4Reliability

If nickel is substituted with cobalt and manganese, then thermal stability is improved, but metal element elution increases

Engineering Contradiction:
Improvethermal stabilityVSAvoidmetal element elution
Core Design Contradiction:
ReliabilityVSLoss of substance

Solution Approach 1:

The patent employs composite materials by creating a multi-element composite oxide structure with magnesium, aluminum, and other transition metals. This composite approach provides a more stable crystal structure that prevents metal element elution while maintaining thermal stability, overcoming the elution problem associated with cobalt-manganese substitution

Inventive Principle:
Principle #40Composite materials

Data Source

PatentEP4357306A1Positive electrode active material, manufacturing method thereof, and positive electrode for lithium secondary battery comprising the same
Publication Date: 2024.04.24 SK ON CO LTD
  • EP4357306A1 patent drawingFigure 1
  • EP4357306A1 patent drawingFigure 2
  • EP4357306A1 patent drawingFigure 3

AI summary

A positive electrode active material according to an Example of the present invention may comprise a lithium layer doped with a first doping element and a transition metal layer doped with a second doping element, wherein an I(003)/I(006) peak intensity ratio in X-ray diffraction measurement is equal to or less than 23.8.