Dynamic Pulse Shaping Time Adjustment in X-ray Detectors

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Solution Overview

Problem

Existing radiation detectors face challenges in dynamically adjusting pulse shaping times to meet varying energy resolution requirements during x-ray fluorescence analysis, leading to suboptimal detection of elemental composition, especially when dealing with unknown samples or mixed samples.

Innovation Solution

A method and apparatus that dynamically modify pulse processing parameters, specifically pulse shaping time, in real-time based on energy resolution requirements during x-ray fluorescence analysis, using a digital signal processor and preamplifier to optimize detector resolution and count rate for accurate elemental composition analysis.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If pulse shaping time is extended to improve energy resolution, then measurement precision is improved, but productivity deteriorates due to reduced count rate

Engineering Contradiction:
Improveenergy resolutionVSAvoidcount rate
Core Design Contradiction:
Measurement precisionVSProductivity

Solution Approach 1:

The patent applies dynamics by making the pulse shaping time adjustable and variable rather than fixed. The system dynamically modifies the pulse shaping time constant based on real-time analysis of the x-ray energy spectrum and detected elemental composition, allowing optimization between energy resolution and count rate depending on the specific analytical requirements of each sample.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The patent implements parameter changes by systematically varying the pulse shaping time constant as a controllable parameter. The system changes this parameter based on feedback from spectral analysis, adjusting it to achieve optimal energy resolution for different elemental compositions and concentration levels detected in the sample.

Inventive Principle:
Principle #35Parameter changes

2Productivity

If pulse shaping time is shortened to increase count rate, then productivity is improved, but measurement precision deteriorates due to reduced energy resolution

Engineering Contradiction:
Improvecount rateVSAvoidenergy resolution
Core Design Contradiction:
ProductivityVSMeasurement precision

Solution Approach 1:

The system dynamically adapts the pulse shaping time constant based on real-time spectral analysis. When high count rates are needed for rapid screening or when analyzing samples with simple compositions, the system shortens the shaping time to maximize productivity while maintaining sufficient resolution for the analytical task.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The patent changes the pulse shaping time parameter in response to detected spectral characteristics. By monitoring the energy spectrum and elemental composition in real-time, the system adjusts the shaping time parameter to optimize the balance between count rate and energy resolution for each specific analytical situation.

Inventive Principle:
Principle #35Parameter changes

3Ease of operation

If fixed pulse processing parameters are used to simplify device operation, then ease of operation is improved, but adaptability deteriorates when analyzing different sample types

Engineering Contradiction:
Improveparameter setting simplicityVSAvoidsample type adaptability
Core Design Contradiction:
Ease of operationVSAdaptability or versatility

Solution Approach 1:

The patent implements self-service by enabling the detector system to automatically analyze the x-ray energy spectrum and determine optimal pulse processing parameters without user intervention. The system self-adjusts the pulse shaping time based on the detected sample characteristics, eliminating the need for users to manually configure parameters for different sample types while maintaining high adaptability.

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The system employs feedback by continuously monitoring the detected x-ray spectrum and using this information to dynamically adjust pulse processing parameters. The feedback loop analyzes spectral features and elemental composition in real-time, automatically modifying the pulse shaping time to optimize performance for each specific sample being analyzed.

Inventive Principle:
Principle #23Feedback

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach allows for real-time adjustment of pulse shaping times to achieve optimal energy resolution and count rates, improving the accuracy and efficiency of elemental composition analysis in x-ray fluorescence instruments, particularly in hand-held XRF instruments, by adapting to the specific characteristics of the sample being analyzed.

Implementation Method 1

c. preamplifying the detector signal pulses

Methodology Applied
Scientific EffectPreamplification:

Implementation Method 2

d. processing the detector signal pulses subject to pulse processing parameters

Methodology Applied
Scientific EffectPulse shaping:

Implementation Method 3

a. irradiating the sample with x-rays

Methodology Applied
Scientific EffectX-ray generation: X-Ray

Implementation Method 4

b. detecting x-rays fluoresced by the sample in response to irradiation

Methodology Applied
Scientific EffectX-ray fluorescence: Fluorescence

Data Source

PatentUS8693625B2Dynamic shaping time modification in X-ray detectors
Publication Date: 2014.04.08 THERMO SCIENTIFIC PORTABLE ANALYTICAL INSTRUMENTS INC
  • US8693625B2 patent drawing
  • US8693625B2 patent drawing
  • US8693625B2 patent drawing

AI summary

Methods and apparatus for adapting the shaping time and/or other pulse processing parameters of an x-ray detector (114) in accordance with the elemental composition of a sample and/or energy resolving requirements. X-rays (104) are directed from a source (102) onto a sample (110) and the radiation (108) responsively emitted from the sample (e.g., fluoresced radiation characteristic of the sample's elemental composition) and detected by an x-ray detector (114) that generates pulses representative of the energy and intensity of the incident radiation. Based upon initial analysis of elemental composition, the shaping time and/or other pulse processing parameter (s) are set to optimize count rate subject to constraints of energy resolution in a spectral region of interest.