Electrochromic Layer Deposition via Pressure Difference

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Solution Overview

Problem

Current electrochromic devices face challenges in achieving high reliability, enhanced electrochromic efficiency, simplified processing, and cost reduction, particularly in large-area fabrication, with existing methods being unsuitable for large-scale production due to high vacuum conditions and material limitations.

Innovation Solution

The electrochromic device incorporates an ion storage layer and electrochromic layer formed using nickel oxide and titanium oxide particles, and tungsten oxide, respectively, with a non-PMMA electrolyte, where the source powders are accelerated and deposited onto substrates using a pressure difference method, allowing for improved layer formation and reduced thermal treatment requirements.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional electrochromic devices are fabricated using existing methods, then basic functionality is achieved, but reliability and electrochromic efficiency are insufficient

Engineering Contradiction:
Improvedevice reliabilityVSAvoidlayer formation quality
Core Design Contradiction:
ReliabilityVSManufacturing precision

Solution Approach 1:

The patent changes the material parameters by using nickel oxide and titanium oxide particles with specific size ranges (5-50 nm and 10-60 nm respectively) and controls deposition parameters through pressure difference method, achieving improved layer formation quality and device reliability simultaneously

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs composite materials by combining nickel oxide and titanium oxide in the ion storage layer, and tungsten oxide in the electrochromic layer, creating synergistic effects that enhance both reliability and electrochromic efficiency

Inventive Principle:
Principle #40Composite materials

2Area of stationary object

If existing fabrication methods are used, then small-scale devices can be produced, but large-area fabrication is not suitable due to high vacuum conditions and material limitations

Engineering Contradiction:
Improvefabrication areaVSAvoidprocess complexity
Core Design Contradiction:
Area of stationary objectVSEase of manufacture

Solution Approach 1:

The patent replaces the complex high vacuum mechanical system with a pressure difference-based deposition system, eliminating the need for high vacuum conditions and enabling simple large-area fabrication processes

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The patent extracts and eliminates the requirement for high vacuum conditions from the fabrication process, retaining only the essential pressure difference mechanism, thereby simplifying the process for large-scale production

Inventive Principle:
Principle #2Taking out (Extraction)

3Reliability

If traditional electrolytes and materials are used, then basic device operation is achieved, but electrochromic efficiency and response speed are limited

Engineering Contradiction:
Improveelectrochromic efficiencyVSAvoidresponse speed
Core Design Contradiction:
ReliabilityVSSpeed

Solution Approach 1:

The patent uses porous nickel oxide and titanium oxide particles that provide high surface area and efficient ion transport pathways, significantly enhancing electrochromic efficiency and response speed compared to traditional dense materials

Inventive Principle:
Principle #31Porous materials

Solution Approach 2:

The patent optimizes the local structure by controlling particle size and distribution within specific ranges, creating optimal local environments for ion insertion/extraction that enhance both efficiency and response speed

Inventive Principle:
Principle #3Local quality

4Productivity

If conventional fabrication processes are applied, then devices can be manufactured, but process cost and complexity are high

Engineering Contradiction:
Improveproduction efficiencyVSAvoidprocess complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The patent merges the ion storage layer and electrochromic layer formation into a single pressure difference deposition process, reducing the number of separate manufacturing steps and lowering overall process complexity and cost

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach results in improved characteristics of the ion storage and electrochromic layers, enhancing electrochromic efficiency, reliability, and simplifying the manufacturing process, making it suitable for large-area production while reducing costs.

Implementation Method 1

accelerating the source powder using pressure difference between the powder storage tank and a chamber

Methodology Applied
Scientific EffectPressure difference: Pressure Gradient

Implementation Method 2

providing the accelerated source powder to the heated substrate to form at least one of an ion storage layer or an electrochromic layer

Methodology Applied
Scientific EffectDeposition: Deposition (physical)

Implementation Method 3

heating a substrate in the chamber

Methodology Applied
Scientific EffectHeating: Heating

Implementation Method 4

the color of material is transformed by oxidation and reduction reactions when electric current flows to the material

Methodology Applied
Scientific EffectOxidation and reduction reactions: Redox Reactions

Implementation Method 5

A display in which reactive material moves and changes its color by oxidation and reduction reactions to occur a chemical change when voltage is applied from the outside using the electrochromic phenomenon

Methodology Applied
Scientific EffectElectrochromism: Electrochromism

Data Source

PatentEP3467582B1Electrochromic element comprising electrochromic layer and ion storage layer and method for preparing same
Publication Date: 2021.06.30 IND UNIV COOP FOUND HANYANG UNIV ERICA CAMPUS
  • EP3467582B1 patent drawingFigure 1
  • EP3467582B1 patent drawingFigure 2
  • EP3467582B1 patent drawingFigure 3

AI summary

An electrochromic device including an electrochromic layer and an ion storage layer is provided. The electrochromic device including the electrochromic layer and the ion storage layer includes a first substrate, a second substrate opposite the first substrate, an electrolyte provided between the first substrate and the second substrate, a first electrode provided between the first substrate and the electrolyte, an ion storage layer including titanium oxide and nickel oxide provided between the first electrode and the electrolyte, a second electrode provided between the second substrate and the electrolyte, and an electrochromic layer provided between the second electrode and the electrolyte.