Lithium Battery Electrolyte Additive for Polysulfide Shuttle Suppression

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Solution Overview

Problem

Lithium-sulfur batteries face issues with low lifetime due to lithium polysulfide dissolution in the electrolyte, leading to capacity loss and decreased ion conductivity, and existing solutions like LiNO3 consume lithium, limiting their effectiveness in repeated charging and discharging.

Innovation Solution

An electrolyte for lithium-secondary batteries incorporating xylylene diamine (XDA) as an additive, which reduces the shuttle phenomenon and enhances charging performance without relying on LiNO3, thereby maintaining lithium metal protection and improving battery efficiency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If LiNO3 is used as an electrolyte additive to form a protective layer on Li metal negative electrode, then the Li negative electrode is protected, but the Li protective layer formation consumes LiNO3 leading to loss of protecting capability after repeated charging and discharging

Engineering Contradiction:
Improveprotective capabilityVSAvoidLiNO3 consumption
Core Design Contradiction:
ReliabilityVSLoss of substance

Solution Approach 1:

The patent changes the chemical composition parameter of the electrolyte additive from LiNO3 to a diamine compound (specifically xylylenediamine or its derivatives). This substitution maintains the protective function on Li metal while eliminating the consumption issue, as the diamine compound forms a stable protective layer without being depleted during cycling.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent replaces the consumable LiNO3 additive with a diamine compound that provides sustained protection. The diamine-based additive creates a stable protective layer that does not require continuous replenishment, effectively transitioning from a disposable protective mechanism to a durable one.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

2Productivity

If lithium polysulfide is dissolved in the electrolyte, then electrochemical reaction occurs, but the lithium polysulfide diffuses toward negative electrode causing capacity loss and shuttle phenomenon

Engineering Contradiction:
Improveelectrochemical reaction activityVSAvoidcapacity loss
Core Design Contradiction:
ProductivityVSLoss of energy

Solution Approach 1:

The diamine compound acts as an intermediary substance that mediates between the lithium polysulfide and the electrodes. It forms a protective layer that prevents direct diffusion of lithium polysulfide to the negative electrode while still allowing necessary electrochemical reactions to occur at the positive electrode, thus reducing the shuttle phenomenon and capacity loss.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent converts the harmful effect of lithium polysulfide dissolution and diffusion into a beneficial outcome. By using the diamine compound, the system allows controlled interaction with lithium polysulfide that results in forming a protective layer, thereby transforming the previously harmful shuttle phenomenon into a protective mechanism.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

3Stability of the object's composition

If lithium polysulfide reacts with lithium metal negative electrode through continuous charge and discharge, then lithium sulfide is fixed on the lithium metal surface, but reaction activity decreases and potential problems worsen

Engineering Contradiction:
Improvelithium sulfide fixationVSAvoiddecreased reaction activity
Core Design Contradiction:
Stability of the object's compositionVSObject-generated harmful factors

Solution Approach 1:

The diamine compound serves as an intermediary that controls the interaction between lithium polysulfide and lithium metal. It allows beneficial fixation of lithium sulfide on the lithium metal surface while preventing excessive or harmful reactions, thus maintaining reaction activity and avoiding potential degradation issues.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The use of xylylene diamine in the electrolyte effectively reduces the shuttle phenomenon and supports stable charging, maintaining battery performance and extending the battery's lifespan by controlling lithium consumption and enhancing ion conductivity.

Implementation Method 1

Lithium polysulfide (Li2Sx, x=8, 6, 4, 2) is an intermediate product produced during an electrochemical reaction of a lithium-sulfur battery, and has high solubility for an organic electrolyte. The lithium polysulfide dissolved in the electrolyte is gradually diffused toward a negative electrode... attempts have been made to form a layer capable of protecting a Li metal negative electrode using an electrolyte additive such as LiNO3

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

The lithium polysulfide dissolved in the electrolyte is gradually diffused toward a negative electrode, and is out of an electrochemical reaction area of a positive electrode, and therefore, is not able to participate in an electrochemical reaction of the positive electrode resulting in capacity loss. In addition, lithium polysulfide elution increases viscosity of an electrolyte decreasing ion conductivity

Methodology Applied
Scientific EffectDiffusion: Diffusion

Implementation Method 3

the lithium polysulfide reacts with a lithium metal negative electrode through a continuous charge and discharge reaction fixing lithium sulfide (Li2S) on the lithium metal surface, which causes problems of decreasing reaction activity and worsening potential problems

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Data Source

PatentEP3671935B1Electrolyte for lithium secondary battery and lithium secondary battery comprising same
Publication Date: 2024.01.17 LG ENERGY SOLUTION LTD
  • EP3671935B1 patent drawingFigure 1
  • EP3671935B1 patent drawingFigure 2
  • EP3671935B1 patent drawingFigure 3

AI summary

The present invention relates to an electrolyte for a lithium-secondary battery including a solvent, a lithium salt and an additive, wherein the additive is a diamine-based compound, and a lithium-secondary battery including the same.