Electrolyte Composition for Lithium-Ion Anode SEI Stability

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Solution Overview

Problem

Lithium-ion batteries face significant capacity loss due to mechanical and chemical damage of the Solid Electrolyte Interface (SEI) on the anode surface caused by volume changes during lithiation and delithiation, leading to reduced cycle stability and service life.

Innovation Solution

An electrolyte composition comprising aprotic, non-aqueous solvents, a fluorine-containing cyclic carbonate component, and at least two lithium salts, including lithium nitrate, which forms a stable SEI on the anode surface, preventing damage and maintaining capacity over multiple cycles.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If high-capacity anode materials such as silicon are used to increase energy density, then the theoretical capacity increases significantly, but the anode undergoes large volume changes during lithiation and delithiation causing SEI layer damage and continuous capacity loss

Engineering Contradiction:
Improvelithium storage capacityVSAvoidcycle stability
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The electrolyte composition performs preliminary action by forming a stable SEI layer during initial cycles that is specifically designed to withstand subsequent volume changes. The fluorine-containing cyclic carbonate component and lithium nitrate work together during formation to create a pre-compression effect that densifies the SEI layer, preparing it to resist mechanical stress from future anode expansion and contraction cycles.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The invention uses a composite electrolyte system combining fluorine-containing cyclic carbonate component (such as fluoroethylene carbonate) with lithium nitrate. This composite approach creates synergistic effects where the fluorinated compound provides mechanical strength and flexibility to the SEI layer, while lithium nitrate enhances ionic conductivity and stabilizes the interface, together solving both capacity and stability requirements.

Inventive Principle:
Principle #40Composite materials

2Ease of operation

If the SEI layer is formed on the anode surface during initial cycles, then lithium transport is enabled, but the SEI layer is mechanically and chemically damaged by volume changes requiring continuous regeneration and causing capacity loss

Engineering Contradiction:
Improvelithium transportVSAvoidcapacity loss
Core Design Contradiction:
Ease of operationVSLoss of substance

Solution Approach 1:

The electrolyte composition provides beforehand cushioning by creating an over-protected SEI layer that is more robust than conventional SEI layers. The fluorine-containing cyclic carbonate component forms a flexible, mechanically strong interface that cushions against the mechanical stress of volume changes, while lithium nitrate provides chemical stabilization. This pre-cushioned SEI layer reduces the need for continuous regeneration and minimizes electrolyte decomposition.

Inventive Principle:
Principle #11Beforehand cushioning (Prior cushioning)

Solution Approach 2:

The invention changes the chemical composition parameters of the electrolyte by introducing fluorine-containing cyclic carbonate and lithium nitrate. These parameter changes alter the properties of the formed SEI layer, making it more mechanically resilient and chemically stable. The fluorine substitution and nitrate addition modify the SEI's elastic modulus, fracture toughness, and ionic conductivity to better withstand operational stress.

Inventive Principle:
Principle #35Parameter changes

3Productivity

If conventional electrolyte compositions are used with high-capacity anodes, then the battery can operate, but the service life and cycle stability are reduced due to continuous SEI regeneration

Engineering Contradiction:
Improvebattery operationVSAvoidservice life
Core Design Contradiction:
ProductivityVSDuration of action of stationary object

Solution Approach 1:

The fluorine-containing cyclic carbonate component and lithium nitrate act as intermediaries between the anode and the bulk electrolyte. This intermediary SEI layer mediates the interaction by providing a stable interface that protects the anode from direct contact with aggressive electrolyte components while maintaining efficient lithium transport. The intermediary layer absorbs mechanical stress and prevents direct damage to the underlying anode structure.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The invention achieves continuity of useful action by creating an SEI layer that maintains its integrity over many cycles without requiring continuous regeneration. The stable SEI formed by the fluorinated electrolyte composition allows lithium transport to continue uninterrupted, eliminating the periodic breakdown and reforming cycles that normally occur with conventional electrolytes, thus extending service life.

Inventive Principle:
Principle #20Continuity of useful action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The electrolyte composition significantly enhances the cycle stability and service life of lithium-ion batteries by maintaining capacity at 80-95% after 60-100 cycles, with improved lithium transport and electrochemical stability.

Implementation Method 1

The surface layer that forms on the anode surface during the first cycles, also called SEI (Solid Electrolyte Interface), is mechanically and/or chemically damaged due to the volume changes of the anode during repeated lithiation and delthiation

Methodology Applied
Scientific EffectSEI formation:

Implementation Method 2

The electrolyte composition significantly enhances the cycle stability and service life of lithium-ion batteries by maintaining capacity at 80-95% after 60-100 cycles, with improved lithium transport and electrochemical stability

Methodology Applied
Scientific EffectElectrochemical stability:

Implementation Method 3

improved lithium transport and electrochemical stability

Methodology Applied
Scientific EffectLithium ion transport: Ion Exchange

Data Source

PatentEP3005449B1New electrolyte composition for high-energy anodes
Publication Date: 2020.08.05 VOLKSWAGEN AG
  • EP3005449B1 patent drawingFigure 1
  • EP3005449B1 patent drawingFigure 2
  • EP3005449B1 patent drawingFigure 3

AI summary

The present invention relates to an electrolyte composition for a lithium-ion battery, a lithium-ion battery and the use of a fluorine-containing cyclic carbonate component and lithium nitrate for improving the cycle stability and/or for increasing battery performance of a lithium-ion battery.