Electrolyzer Membrane Design for CO2 Reduction

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Solution Overview

Problem

Existing carbon dioxide electrolyzers face challenges in reducing hydrogen formation and increasing efficiency due to diffusion limitations, proton concentration issues, and cathode material toxicity, which lead to reduced service life and energy inefficiency.

Innovation Solution

An electrolyzer design featuring a cation-permeable membrane with an anion-selective polymer layer between the anode and cathode compartments, preventing hydrogen protons from reaching the cathode and allowing carbon dioxide to be efficiently converted into valuable products, while using pure water to prevent salt precipitation and enhance conductivity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Object-generated harmful factors

If a gap filled with aqueous electrolyte is placed between the proton conducting membrane and the cathode to suppress hydrogen formation, then hydrogen formation is reduced, but the voltage drop across the cell increases and efficiency decreases

Engineering Contradiction:
Improvehydrogen formationVSAvoidvoltage drop
Core Design Contradiction:
Object-generated harmful factorsVSLoss of energy

Solution Approach 1:

A cation-exchange membrane is introduced as an intermediary component between the proton-conducting membrane and the cathode. This membrane selectively transports cations while preventing direct contact between protons and the cathode surface, thereby suppressing hydrogen formation without creating a large electrolyte-filled gap that would cause excessive voltage drop.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The cation-exchange membrane functions as a thin film barrier that allows selective ion transport. Its thin-film nature minimizes the distance for ion transport and reduces ohmic losses, while still effectively blocking protons from reaching the cathode to form hydrogen.

Inventive Principle:
Principle #30Flexible shells and thin films

2Reliability

If base or conducting salt is added to increase electrolyte conductivity, then conductivity is improved, but hydroxide ions form and react with carbon dioxide to create precipitates that shorten service life

Engineering Contradiction:
Improveservice lifeVSAvoidprecipitate formation
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The cation-exchange membrane acts as a mediator that separates the anode compartment (where base or salt might be added) from the cathode compartment (where carbon dioxide reduction occurs). This prevents hydroxide ions from reaching the cathode and reacting with carbon dioxide to form precipitates, while still allowing cation transport to maintain conductivity.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The electrolyte system is segmented into separate compartments by the cation-exchange membrane. This segmentation allows different electrolyte compositions to be used in each compartment without mixing, enabling conductivity enhancement in the anode compartment without causing precipitate formation in the cathode compartment.

Inventive Principle:
Principle #1Segmentation

3Object-generated harmful factors

If cathode material with high hydrogen overvoltage is selected to suppress hydrogen formation, then hydrogen formation is reduced, but the selection of valuable products is severely restricted

Engineering Contradiction:
Improvehydrogen formationVSAvoidproduct selection
Core Design Contradiction:
Object-generated harmful factorsVSAdaptability or versatility

Solution Approach 1:

The cation-exchange membrane serves as an intermediary that blocks protons from reaching the cathode surface, suppressing hydrogen formation through physical barrier action rather than through cathode material properties. This decouples hydrogen suppression from cathode material selection, allowing versatile product formation based on reaction mechanism and catalyst choice.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The function of suppressing hydrogen formation is extracted from the cathode material and assigned to the cation-exchange membrane. This separation of functions allows the cathode material to be optimized solely for valuable product formation through appropriate catalyst selection, while the membrane handles the hydrogen suppression task.

Inventive Principle:
Principle #2Taking out (Extraction)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This configuration reduces hydrogen formation, increases carbon dioxide yield, and extends the electrolyzer's service life by allowing flexible cathode material selection and maintaining high efficiency, even with pure water, enabling the production of valuable products like carbon monoxide and ethylene.

Implementation Method 1

A first cation-permeable membrane is arranged between the anode compartment and the cathode compartment

Methodology Applied
Scientific EffectIon conduction: Conduction (electrical)

Implementation Method 2

a layer comprising an anion-selective polymer is arranged between the first membrane and the cathode

Methodology Applied
Scientific EffectIon exchange: Ion Exchange

Implementation Method 3

The carbon dioxide is reduced to valuable products at a cathode of the electrochemical cell

Methodology Applied
Scientific EffectElectrochemical reduction: Electrolysis

Implementation Method 4

water is oxidized to oxygen at an anode

Methodology Applied
Scientific EffectElectrochemical oxidation: Electrolysis

Implementation Method 5

The hydrogen ions and the carbonate or bicarbonate then react to form carbon dioxide and water

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Data Source

PatentEP3414363B1Method and device for the electrochemical utilization of carbon dioxide
Publication Date: 2020.08.12 SIEMENS ENERGY GLOBAL GMBH & CO KG
  • EP3414363B1 patent drawingFigure 1

AI summary

The invention relates to an electrolyzer for the electrochemical utilization of carbon dioxide, comprising at least one electrolytic cell, wherein the electrolytic cell comprises an anode chamber having an anode and a cathode chamber having a cathode, a first cation-permeable membrane is arranged between the anode chamber and the cathode chamber, the anode directly adjoins the first membrane, and a layer comprising an anion-selective polymer is arranged between the first membrane and the cathode.