Electron Beam Sterilization of Flexible Plasma Bags

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Solution Overview

Problem

Current electron-beam sterilization methods for flexible bags containing human plasma protein solutions are inadequate as they fail to effectively sterilize the thicker areas, such as the twist-off caps, due to insufficient energy penetration, leading to potential contamination risks.

Innovation Solution

A sterilization device employing a combination of electron accelerators emitting beams with energies between 400-500 keV and 4-5 MeV, arranged at the top of the device to emit electron beams perpendicular to the ground, with enhanced containment measures to prevent radiation escape, ensuring thorough sterilization of the bag components.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If electron beam energy is increased to penetrate thicker areas like twist-off caps, then sterilization effectiveness is improved, but radiation containment requirements and device complexity increase

Engineering Contradiction:
Improvesterilization effectivenessVSAvoidradiation containment system
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent changes the energy parameter of the electron beam from conventional levels (450-500 keV) to high energy levels (4-5 MeV). This parameter change enables the beam to penetrate thick areas like twist-off caps (up to 3 mm) and bag walls (130 μm) effectively, achieving complete sterilization while managing radiation containment through directional emission perpendicular to the ground

Inventive Principle:
Principle #35Parameter changes

2Device complexity

If electron accelerators are arranged to emit beams parallel to the ground, then device simplicity is maintained, but radiation escape risk increases

Engineering Contradiction:
Improveaccelerator arrangementVSAvoidradiation escape
Core Design Contradiction:
Device complexityVSObject-affected harmful factors

Solution Approach 1:

The patent inverts the conventional horizontal arrangement of electron accelerators to a vertical configuration. Instead of emitting beams parallel to the ground, the accelerators are positioned to emit beams perpendicular to the ground (downwards). This inversion enables effective penetration of thick bag components while the vertical orientation, combined with containment walls, prevents radiation escape into the surrounding environment

Inventive Principle:
Principle #13The other way round (Inversion)

3Reliability

If electron beam energy is increased fivefold to 4 MeV, then penetration depth and sterilization completeness are improved, but energy consumption and equipment requirements increase

Engineering Contradiction:
Improvesterilization completenessVSAvoidelectron beam energy
Core Design Contradiction:
ReliabilityVSUse of energy by moving object

Solution Approach 1:

The patent implements a significant change in the energy parameter of the electron beam, increasing it from 450-500 keV to 4-5 MeV (approximately 10 times higher energy). This parameter change is necessary to achieve complete sterilization of thick areas like twist-off caps and multi-layer bag walls. The high energy enables the beam to penetrate these thick components and deliver sufficient absorbed dose to eliminate microorganisms throughout the entire bag structure

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method achieves complete sterilization of flexible bag components, including the twist-off caps, by increasing the electron beam energy to 4 MeV, five times higher than the previous standard, ensuring safety and efficacy in preventing microbial contamination.

Implementation Method 1

Electron-beam irradiation, also known as 'E-beam', is a form of ionising radiation which is generally characterised by low penetration and high doses of applied energy. Said beam is a stream of concentrated and highly charged electrons. These electrons are generated by an accelerator capable of producing beams which may be continuous or pulsed. The material to be sterilized absorbs the energy of the electrons and said energy absorption, also known as absorbed dose, eliminates microorganisms by destroying their DNA strands.

Methodology Applied
Scientific EffectElectron-beam irradiation: Electron Beam

Data Source

PatentEP3721911B1Method for sterilising flexible bags by electron-beam irradiation
Publication Date: 2023.12.27 GRIFOLS ENG
  • EP3721911B1 patent drawingFigure 1
  • EP3721911B1 patent drawingFigure 2
  • EP3721911B1 patent drawingFigure 3

AI summary

This invention relates to the pharmaceutical sector, specifically to an improved device for electron-beam irradiation sterilisation of flexible bags, in particular the type of flexible bags that may contain human plasma protein solutions for therapeutic use. This device comprises two electron accelerators: a first accelerator emitting an electron beam with energies between 400 and 500 keV and a second accelerator emitting an electron beam with an energy of at least 4 MeV. In addition, the present invention relates to a sterilisation method by electron-beam irradiation of such flexible bags and to an in-line filling process for flexible bags using the sterilisation device and method of this invention.