Electrospray Device for Fluidized Bed Coating and Spray-Drying

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Existing fluidized bed apparatuses face challenges in achieving uniform coating and spray-drying due to non-uniform electric fields and unstable charging of particles, leading to inefficiencies and quality issues in both coating and spray-drying processes.

Innovation Solution

The integration of an electrospray device with a charged nozzle and partition, along with a magnetic field generator, generates a controlled electromagnetic and magnetic field to stabilize particle charging and optimize the motion of charged droplets and particles, ensuring uniform coating and efficient spray-drying through Coulombic fission and rotational upward paths.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If an electrospray device with charged nozzle and partition is used, then particle charging stability and coating uniformity are improved, but device complexity increases

Engineering Contradiction:
Improvecoating uniformityVSAvoiddevice complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The apparatus is divided into distinct functional zones: a charged nozzle for electrospray generation, a partition structure creating separate spray and fluidization regions, and a charged partition for particle charging. This segmentation allows each component to perform its specific function optimally, improving coating uniformity while maintaining manageable complexity through modular design.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

A magnetic field generator is introduced as an intermediary component to generate a magnetic field that works in conjunction with the electric field from the charged nozzle and partition. This magnetic field mediator helps stabilize particle charging and control droplet motion, enhancing coating uniformity without requiring direct modification of the electrospray system itself.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Productivity

If a magnetic field generator is added to the electrospray device, then particle motion control and spray pattern development are improved, but device complexity and manufacturing cost increase

Engineering Contradiction:
Improvespray-drying efficiencyVSAvoiddevice complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The magnetic field generator is integrated with the existing electrospray device structure, combining electromagnetic field generation capabilities into a unified system. This merging allows the magnetic field to work synergistically with the electric field from the charged components, improving spray pattern development and particle motion control while avoiding the need for completely separate systems.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The charged partition structure serves multiple functions: it acts as an electrode for particle charging, creates a defined spray zone geometry, and works with the magnetic field generator to control particle motion. This multi-functionality reduces the need for additional dedicated components, offsetting the complexity increase from adding the magnetic field generator.

Inventive Principle:
Principle #6Universality (Multi-functionality)

3Adaptability or versatility

If electrospray is applied to both coating and spray-drying processes, then process versatility is improved, but operation complexity increases

Engineering Contradiction:
Improveprocess versatilityVSAvoidoperation complexity
Core Design Contradiction:
Adaptability or versatilityVSEase of operation

Solution Approach 1:

The system employs dynamic control of voltage polarity between the charged nozzle and partition, allowing the same apparatus to be switched between coating mode (attractive electrostatic force) and spray-drying mode (repulsive electrostatic force). This dynamic reconfiguration enables process versatility without requiring physically different equipment for each application.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The versatility between coating and spray-drying processes is achieved by changing key operating parameters: the voltage polarity and magnitude applied to the nozzle and partition, the liquid flow rate, and the particle feed rate. These parameter adjustments allow the same electrospray device to optimize performance for different process requirements without structural modifications.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach results in improved particle size distribution, reduced agglomeration, and enhanced coating quality, with the ability to produce ultrafine particles and guide them efficiently for collection, addressing the inefficiencies and quality issues in previous methods.

Implementation Method 1

a power supply directly or indirectly connected between the nozzle and the partition to apply voltage

Methodology Applied
Scientific EffectElectric field: Electric Field

Implementation Method 2

the liquid supplied to the end of the emission electrode is charged, in order to release charged droplets from the end of the emission electrode

Methodology Applied
Scientific EffectCoulombic force: Coulomb's Law

Implementation Method 3

the sprayer body is provided with a swirl generator for generating a swirling air stream

Methodology Applied
Scientific EffectSwirling air stream: Vortex Ring

Implementation Method 4

a magnetic field generator, the magnetic field generator being a coil which is spirally twined around a circumference of the partition

Methodology Applied
Scientific EffectMagnetic field: Magnetic Field

Implementation Method 5

a Taylor cone is formed by the liquid at the exit of the nozzle at the end of the emission electrode under the electric field force whose orientation is opposite to that of the surface tension force

Methodology Applied
Scientific EffectTaylor cone:

Implementation Method 6

The liquid provided by the liquid pump is retained at an exit of the nozzle under the surface tension force

Methodology Applied
Scientific EffectSurface tension: Surface Tension

Implementation Method 7

When the ratio of the charge intensity on the droplet surface to the droplet radius reaches the Rayleigh instability limit, the droplets incur the Coulombic fission to form a large number of droplets in small particle size

Methodology Applied
Scientific EffectCoulombic fission: Coulomb's Law

Implementation Method 8

During the movement of the charged droplets from the emission electrode to the opposed electrode under the electric field force, the solvent of the charged droplets evaporates continually

Methodology Applied
Scientific EffectEvaporation: Evaporation

Data Source

PatentUS11845100B2Electrospray device for fluidized bed apparatus, fluidized bed apparatus and method
Publication Date: 2023.12.19 TIANJIN CENAX BIOTECH CO LTD
  • US11845100B2 patent drawing
  • US11845100B2 patent drawing
  • US11845100B2 patent drawing

AI summary

The electrospray device comprises a sprayer comprising a sprayer body and nozzle, and a partition positioned vertically and coaxially with the sprayer. The sprayer body is provided with a swirl generator for generating a swirling air stream, and a power supply connected between the nozzle and the partition, to apply voltage to the nozzle and the partition. The electrospray device may be part of a fluidized bed apparatus comprising a product container, a lower plenum base, an air distribution plate resided therebetween. When the power supply applies voltage in opposite polarities to the nozzle and the partition, the fluidized bed apparatus is used for coating particles; and when the power supply applies voltage of the same, the fluidized bed apparatus is used for spray-drying a solution. The electrospray device uses an electromagnetic hydrodynamic method to improve the performance of the fluidized bed apparatus and optimize the process of product.