Electrostatic Levitation for Surface Tension Measurement

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Solution Overview

Problem

Conventional methods for measuring thermophysical properties of high-temperature materials like liquid metals and glasses face challenges due to high surface reactivity, and existing levitation techniques suffer from contamination, viscous effects, and asphericity issues, making accurate surface tension measurement difficult.

Innovation Solution

The use of electrostatic levitation with Faraday forcing, where a sinusoidal electric field is applied to an electrostatically levitated liquid droplet to resonate at its natural frequency, allowing for precise measurement of surface tension through continuous frequency sweeps and image analysis using Legendre polynomials.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If conventional measurement methods are used for high-temperature materials, then measurement can be performed, but measurement accuracy deteriorates due to high surface reactivity

Engineering Contradiction:
Improvesurface tension measurement accuracyVSAvoidsurface reactivity
Core Design Contradiction:
Measurement precisionVSObject-affected harmful factors

Solution Approach 1:

The patent uses an electrostatic field as an intermediary to levitate the liquid metal droplet, eliminating contact between the sample and container walls. This mediator (electrostatic field) allows measurement of highly reactive materials without direct interaction that would cause contamination or reaction, thereby improving measurement accuracy while avoiding the harmful effects of surface reactivity

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent replaces mechanical contact-based measurement systems with a non-contact electrostatic levitation system. By substituting mechanical support structures with electrostatic fields, the system eliminates contamination and reaction issues associated with physical contact, enabling accurate measurement of surface tension for highly reactive materials

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Measurement precision

If aerodynamic levitation is used, then levitation can be achieved, but measurement accuracy deteriorates due to contamination and viscous effects

Engineering Contradiction:
Improvesurface tension measurement accuracyVSAvoidcontamination and viscous effects
Core Design Contradiction:
Measurement precisionVSObject-generated harmful factors

Solution Approach 1:

The patent replaces aerodynamic levitation (which uses gas flow and creates viscous effects and contamination) with electrostatic levitation. This substitution eliminates the harmful factors of contamination and viscous drag while maintaining the ability to levitate and measure liquid metal droplets accurately

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The patent introduces an electrostatic field as a cleaner intermediary compared to aerodynamic methods. The electrostatic field provides levitation without requiring fluid medium contact, thereby eliminating contamination and viscous effects that plague aerodynamic levitation systems

Inventive Principle:
Principle #24Intermediary (Mediator)

3Measurement precision

If electromagnetic levitation is used, then levitation in vacuum can be achieved, but measurement accuracy deteriorates due to asphericity

Engineering Contradiction:
Improvesurface tension measurement accuracyVSAvoiddroplet sphericity
Core Design Contradiction:
Measurement precisionVSShape

Solution Approach 1:

The patent uses an electrostatic field instead of electromagnetic fields to levitate the droplet. The electrostatic mediator produces more uniform forces that better maintain droplet sphericity compared to electromagnetic methods, thereby improving measurement accuracy by reducing asphericity-related errors

Inventive Principle:
Principle #24Intermediary (Mediator)

4Reliability

If pulse-decay technique is used, then surface tension can be measured, but measurement reliability deteriorates for high viscosity samples due to control system perturbations

Engineering Contradiction:
Improvemeasurement reliability for high viscosity samplesVSAvoidcontrol system perturbations
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The patent employs periodic sinusoidal forcing at the droplet's natural frequency to induce sustained oscillations, replacing the pulse-decay technique. This periodic action provides reliable measurements for high viscosity samples by avoiding the abrupt perturbations and control system disturbances inherent in pulse-release methods

Inventive Principle:
Principle #19Periodic action

Solution Approach 2:

The patent uses mechanical vibration through sinusoidal electric field forcing to maintain droplet oscillations. This continuous vibration approach is more reliable for high viscosity materials than pulse-decay, as it avoids the harmful perturbations introduced by sudden release and provides stable, measurable oscillation patterns

Inventive Principle:
Principle #18Mechanical vibration

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method provides accurate and reliable surface tension measurements for high viscosity and high-temperature samples, overcoming limitations of pulse-decay techniques and achieving consistent results with literature values for materials like Zirconium, Inconel 625, and Rhodium.

Implementation Method 1

a sample can be levitated using electrostatic levitation

Methodology Applied
Scientific EffectElectrostatic levitation: Electrostatics

Implementation Method 2

levitating a sample using electrostatic levitation; applying a force to the sample using a sinusoidal electric field

Methodology Applied
Scientific EffectCoulomb force: Coulomb's Law

Implementation Method 3

applying a force to the sample using a sinusoidal electric field at a frequency that resonates with a natural frequency of the sample

Methodology Applied
Scientific EffectResonance: Resonance

Implementation Method 4

Faraday forcing uses electrostatic levitation as a means to measure surface tension. The Faraday forcing method in levitated liquid droplets has recently been introduced as a method for measuring surface tension using resonance

Methodology Applied
Scientific EffectFaraday forcing: Faraday Wave

Implementation Method 5

Surface tension, a notably important property, can be measured using levitation technologies by exploiting the natural frequency fn at which a spherical liquid droplet comes to rest, given by... where γ is the surface tension

Methodology Applied
Scientific EffectSurface tension: Surface Tension

Data Source

PatentUS12135269B2System and method for measuring surface tension of a levitated sample
Publication Date: 2024.11.05 UNIV OF FLORIDA RESEARCH FOUNDATION INC
  • US12135269B2 patent drawing
  • US12135269B2 patent drawing
  • US12135269B2 patent drawing

AI summary

Various examples are provided related to measuring surface tension. In one example, a method includes levitating a sample using electrostatic levitation; applying a signal to at least one electrode to excite the sample into a n=3 mode of oscillation; capturing images of the sample with a respective image being associated with a particular frequency that is applied to the sample when the respective image is captured; quantifying sample resonance using a projection method of Legendre polynomials based on the plurality of images; and determining a measured resonance frequency of the sample by an analysis of the sample resonance. The sample can be levitated using a feedback-controlled voltage and the applied signal can be swept over a range of frequencies. A system including electrodes, a position sensor, a camera device, and at least one computing device can be used to carry out the method.