Elemental Tag Oligonucleotide Probes for Single Cell Gene Expression

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Solution Overview

Problem

Current gene and protein expression analysis methods lack sensitivity and multiplexing capabilities, especially for single cells, leading to incomplete genomic information and interference from heterogeneous cell populations.

Innovation Solution

The use of elemental tags attached to oligonucleotide probes and microspheres for hybridization, followed by inductively coupled plasma mass spectrometry (ICP-MS) analysis, allows for sensitive and quantitative detection of multiple mRNA species in single cells without fluorescent labeling, enabling simultaneous analysis of gene and protein expression.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If fluorescent labeling is used for gene expression analysis, then detection capability is improved, but sensitivity and multiplexing capabilities are limited

Engineering Contradiction:
Improvedetection capabilityVSAvoidsensitivity and multiplexing capabilities
Core Design Contradiction:
Measurement precisionVSReliability

Solution Approach 1:

The patent changes the detection parameter from fluorescent labeling to elemental tags detectable by ICP-MS. This parameter change enables simultaneous detection of multiple mRNA species (multiplexing) with high sensitivity, as ICP-MS can distinguish between different elements and isotopes, allowing up to 70-plex detection compared to limited fluorescent channels

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent replaces the optical detection system (fluorescence microscopy/flow cytometry) with a mass spectrometry-based detection system (ICP-MS). This substitution eliminates the limitations of fluorescent labeling by using elemental tags that can be detected with superior sensitivity and multiplexing capability, as mass spectrometry can simultaneously resolve multiple elemental signals without spectral overlap

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Ease of operation

If conventional gene expression methods are used, then analysis is simpler, but sensitivity for single cells is insufficient

Engineering Contradiction:
Improveanalysis simplicityVSAvoidsensitivity for single cells
Core Design Contradiction:
Ease of operationVSMeasurement precision

Solution Approach 1:

The patent introduces elemental tags as intermediaries that attach to oligonucleotide probes for hybridization to target mRNA. These elemental tags serve as detectable mediators that amplify the signal from single cell mRNA, enabling sensitive detection by ICP-MS while maintaining the simplicity of hybridization-based analysis

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent segments the detection approach by using multiple distinct elemental tags (different elements or isotopes) to label different probes targeting different mRNA species. This segmentation allows simultaneous analysis of multiple genes in single cells, with each element providing an independent detection channel that contributes to overall sensitivity

Inventive Principle:
Principle #1Segmentation

3Quantity of substance

If heterogeneous cell populations are analyzed, then sample representivity is improved, but genomic information completeness deteriorates due to interference

Engineering Contradiction:
Improvesample representivityVSAvoidgenomic information completeness
Core Design Contradiction:
Quantity of substanceVSLoss of information

Solution Approach 1:

The patent replaces conventional detection methods with ICP-MS-based detection of elemental tags. This substitution provides superior signal-to-noise ratio and sensitivity, enabling clear distinction of hybridization signals from heterogeneous cell populations without interference, thus preserving complete genomic information even in mixed samples

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach provides high sensitivity and accuracy in analyzing hundreds of thousands of mRNA molecules, improving detection efficiency and excluding fluorescent labeling, thus offering a robust and quantitative measurement of RNA levels in biological samples.

Implementation Method 1

hybridization of complementary oligonucleotides to target mRNA

Methodology Applied
Scientific EffectHybridization: Chemical Bonding

Implementation Method 2

inductively coupled plasma mass spectrometry (ICP-MS) analysis

Methodology Applied
Scientific EffectInductive coupling plasma ionization: Electromagnetic Induction

Implementation Method 3

elemental analysis by ICP-MS

Methodology Applied
Scientific EffectMass spectrometry detection:

Data Source

PatentEP3561071B1Gene expression assays conducted by elemental analysis
Publication Date: 2020.12.16 FLUIDIGM CANADA INC
  • EP3561071B1 patent drawingFigure 1A~1B
  • EP3561071B1 patent drawingFigure 2A~2B
  • EP3561071B1 patent drawingFigure 3

AI summary

Methods and kits for gene expression analysis are disclosed. The methods utilize element-tagged oligonucleotides as probes which are subsequently analyzed by elemental analysis. Also disclosed are methods and kits for the analysis of biological molecules using element labeled supports such as beads, followed by elemental analysis. The elemental analysis can be done using inductively coupled plasma mass spectrometry (ICP-MS).