Infrared Ellipsometer Speckle Reduction via QCL Dynamics

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Solution Overview

Problem

Ellipsometer systems operating in the infrared spectral range face challenges with speckle and standing wave effects due to the long coherence length of quantum cascade laser sources, which affect data accuracy and measurement speed, and existing solutions do not effectively mitigate these issues.

Innovation Solution

A mid-infrared ellipsometer or polarimeter system utilizing a tunable quantum cascade laser source in sweep mode, combined with dual-rotatable optical elements and a single-point detector, employs coherence length reduction through wavelength scrambling and averaging multiple pulses to minimize speckle and standing wave effects, allowing for faster and more accurate data acquisition.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Illumination intensity

If a quantum cascade laser source with long coherence length is used in an infrared ellipsometer, then high brilliance and tunability are achieved, but speckle and standing wave effects occur which degrade measurement accuracy

Engineering Contradiction:
ImprovebrillianceVSAvoidmeasurement accuracy
Core Design Contradiction:
Illumination intensityVSMeasurement precision

Solution Approach 1:

The patent applies dynamics by rotating optical elements (compensators, polarizers, or the entire sample) during measurement. This dynamic motion changes the interference conditions for speckle and standing wave patterns, allowing the system to average out these artifacts over time while maintaining the high brilliance of the QCL source

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

The patent implements periodic action through synchronized rotation of optical elements at specific frequencies. By modulating the optical path periodically and synchronizing detection with this modulation, the system can separate the periodic signal from non-periodic speckle and standing wave artifacts, improving measurement accuracy

Inventive Principle:
Principle #19Periodic action

2Illumination intensity

If a quantum cascade laser source with long coherence length is used in an infrared ellipsometer, then high brilliance and tunability are achieved, but measurement speed is reduced due to speckle and standing wave effects

Engineering Contradiction:
ImprovebrillianceVSAvoidmeasurement speed
Core Design Contradiction:
Illumination intensityVSProductivity

Solution Approach 1:

By implementing dynamic rotation of optical elements during measurement, the system can rapidly average out speckle and standing wave artifacts. This allows faster convergence to accurate measurements without sacrificing the high brilliance of the QCL source, thereby improving measurement speed

Inventive Principle:
Principle #15Dynamics

3Measurement precision

If coherence length is reduced to minimize speckle and standing wave effects, then measurement accuracy improves, but the high brilliance advantage of the quantum cascade laser is compromised

Engineering Contradiction:
Improvemeasurement accuracyVSAvoidbrilliance
Core Design Contradiction:
Measurement precisionVSIllumination intensity

Solution Approach 1:

The patent extracts or separates the harmful speckle and standing wave effects from the useful measurement signal through dynamic rotation and periodic modulation. This allows the system to maintain the full brilliance of the QCL source while removing the detrimental coherence effects through signal processing and temporal averaging

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent introduces rotating optical elements as intermediaries that mediate between the high-coherence QCL source and the sample. These intermediaries dynamically modify the optical path to average out speckle and standing wave patterns while preserving the high brilliance and coherence advantages of the laser source for the actual measurement

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables the determination of advanced data types like Mueller matrices and generalized ellipsometry for anisotropic samples with improved accuracy and speed, overcoming the limitations of existing systems by reducing coherence length and enhancing data reliability.

Implementation Method 1

a source of electromagnetic radiation, in particular a tunable quantum cascade laser source

Methodology Applied
Scientific EffectLaser emission: Laser

Implementation Method 2

a first rotatable optical element, in particular a rotatable compensator, a rotatable polarizer, or a rotatable combination of a half-wave plate and a quarter-wave plate

Methodology Applied
Scientific EffectPolarization modulation: Polarisation

Implementation Method 3

a single-point detector for infrared radiation, in particular a pyroelectric detector, a DTGS detector, an MCT detector, or a LiTaO3 detector, which cannot resolve individual laser pulses

Methodology Applied
Scientific EffectElectromagnetic radiation detection:

Implementation Method 4

employs coherence length reduction through wavelength scrambling and averaging multiple pulses

Methodology Applied
Scientific EffectWavelength scrambling:

Implementation Method 5

averaging multiple pulses to minimize speckle and standing wave effects

Methodology Applied
Scientific EffectSignal averaging:

Data Source

PatentUS11821833B2Fast and accurate Mueller matrix infrared ellipsometer
Publication Date: 2023.11.21 J A WOOLLAM CO
  • US11821833B2 patent drawing
  • US11821833B2 patent drawing
  • US11821833B2 patent drawing

AI summary

An ellipsometer, polarimeter and the like system operating in the infrared spectral range (0.75 μm to 1000 μm), utilizing a tunable quantum cascade laser (QCL) source with the capability if reducing speckle and standing wave effects, dual-rotatable optical elements, a single-point detector, as well as optional means of reducing the size of the probe beam at the measurement surface and optional chopper for lock-in detection.