Ellipsometry Correction for Rough Surface Optical Properties

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Solution Overview

Problem

Current methods for investigating thin films on rough or textured surfaces using electromagnetic beams face challenges in accurately determining optical and physical properties due to scattering effects, leading to noisy and depolarized data, which complicates analysis and results in incorrect values for refractive index and extinction coefficient.

Innovation Solution

The approach involves using a spectroscopic ellipsometer system with a stage tilt and rotation mechanism to optimize the orientation of textured surfaces, allowing more electromagnetic radiation to be collected and focused into a detector, and applying correction factors or scattering matrices to align data from rough surfaces with those from smooth surfaces, thereby improving data quality and accuracy.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If a sample with rough or textured surface is measured using conventional spectroscopic ellipsometry, then the measurement can be performed, but the detected light intensity is significantly reduced due to scattering, leading to noisy and depolarized data with incorrect optical properties

Engineering Contradiction:
Improveaccuracy of optical propertiesVSAvoiddata quality
Core Design Contradiction:
Measurement precisionVSReliability

Solution Approach 1:

The patent applies preliminary action by measuring an uncoated rough surface first to determine roughness parameters, then using these parameters as correction factors in subsequent measurements of coated rough surfaces. This preliminary measurement and correction approach resolves the technical contradiction by establishing accurate reference data before performing the actual film measurements, thereby improving both measurement precision and data reliability

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent uses an intermediary approach by introducing correction factors derived from measuring uncoated rough surfaces as mediators between the raw scattered light data and the accurate optical properties. These correction factors act as intermediaries that compensate for scattering effects, enabling accurate determination of refractive index and extinction coefficient despite the rough surface conditions

Inventive Principle:
Principle #24Intermediary (Mediator)

2Illumination intensity

If the beam intensity is increased to compensate for scattering losses, then more light reaches the detector, but the scattered electromagnetic radiation causes noisy and depolarized data that cannot be reliably analyzed

Engineering Contradiction:
Improveintensity of reflected beamVSAvoiddata reliability
Core Design Contradiction:
Illumination intensityVSLoss of information

Solution Approach 1:

The patent converts the harmful scattering effect into a beneficial correction mechanism. By measuring the scattering characteristics of uncoated rough surfaces and using these measurements to create correction factors, the patent transforms the previously harmful scattered light into useful information that improves measurement accuracy. This resolves the contradiction by showing that the scattered radiation, rather than being purely harmful, contains valuable information about surface roughness that can be used to correct subsequent measurements

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method enhances the accuracy of determining physical and optical properties of thin films on textured surfaces by increasing the intensity and quality of reflected radiation, reducing noise, and enabling reliable analysis by aligning results with those from smooth surfaces, thus improving the precision of ellipsometric parameters.

Implementation Method 1

cause a polarized beam of electromagnetic radiation to impinge on a sample at an oblique angle thereto, interact with said sample and then enter a detector

Methodology Applied
Scientific EffectReflection: Reflection

Implementation Method 2

a polarized beam of electromagnetic radiation

Methodology Applied
Scientific EffectPolarization: Polarisation

Implementation Method 3

much of the measurement beam can be scattered away from the detector. This significantly reduces the overall intensity reaching the ellipsometer detector

Methodology Applied
Scientific EffectScattering: Scattering

Data Source

PatentUS8248607B1Empirical correction for spectroscopic ellipsometric measurements of rough or textured surfaces
Publication Date: 2012.08.21 J A WOOLLAM CO
  • US8248607B1 patent drawing
  • US8248607B1 patent drawing
  • US8248607B1 patent drawing

AI summary

A method of applying spectroscopic ellipsometry to arrive at accurate values of optical and physical properties for thin films on samples having rough or textured surfaces.