Emulsification Device Laminar Flow Mixing Chamber

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Solution Overview

Problem

Existing emulsifying devices for continuous production of emulsions and dispersions often fail to produce nanoemulsions and liquid-crystalline structures efficiently, as they either allow cavitation forces or are not designed to prevent turbulence, leading to suboptimal mixing and energy consumption.

Innovation Solution

An emulsifying device with a rotationally symmetric, airtight mixing chamber featuring a stirrer unit that ensures laminar flow, with specific ratios of inlet to outlet line distance and stirrer arm length, and a magnetic coupling system to minimize energy consumption and prevent air inclusion, allowing for the continuous production of emulsions and dispersions with a liquid-crystalline structure.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional continuous emulsifying devices are used, then continuous production is achieved, but cavitation forces and turbulence occur leading to suboptimal mixing and high energy consumption

Engineering Contradiction:
Improvecontinuous production capabilityVSAvoidenergy consumption
Core Design Contradiction:
ProductivityVSLoss of energy

Solution Approach 1:

The invention changes the flow regime parameter from turbulent to laminar flow by designing a specific mixing chamber geometry with controlled dimensions and a centrally positioned stirrer. This parameter change eliminates cavitation forces while maintaining continuous production capability, thereby reducing energy consumption without sacrificing productivity.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention replaces the conventional high-shear mechanical mixing system that generates cavitation with a laminar flow-based mixing system. By substituting the mechanical turbulence-generating approach with a controlled laminar flow approach using specific chamber geometry and stirrer design, energy losses from cavitation are eliminated while continuous production is maintained.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Productivity

If conventional mixing chambers are used, then continuous production is achieved, but air inclusion occurs and mixing precision is insufficient for nanoemulsion production

Engineering Contradiction:
Improvecontinuous production capabilityVSAvoidemulsion droplet size control
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The invention changes the flow regime parameter from turbulent to laminar flow by designing a specific mixing chamber geometry with controlled dimensions and a centrally positioned stirrer. This parameter change eliminates cavitation forces while maintaining continuous production capability, thereby reducing energy consumption without sacrificing productivity.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention positions the stirrer centrally within the mixing chamber, creating a symmetric flow pattern that prevents air inclusion. The asymmetric positioning of inlet and outlet lines relative to the chamber geometry further optimizes flow patterns to eliminate dead zones and prevent air entrapment, thereby improving mixing precision for nanoemulsion production.

Inventive Principle:
Principle #4Asymmetry

3Stability of the object's composition

If high-shear mixing is used to achieve thorough mixing, then mixing efficiency improves, but energy consumption increases and liquid-crystalline structures cannot form

Engineering Contradiction:
Improvemixing thoroughnessVSAvoidenergy consumption
Core Design Contradiction:
Stability of the object's compositionVSUse of energy by moving object

Solution Approach 1:

The invention changes the flow regime parameter from turbulent to laminar flow by designing a specific mixing chamber geometry with controlled dimensions and a centrally positioned stirrer. This parameter change eliminates cavitation forces while maintaining continuous production capability, thereby reducing energy consumption without sacrificing productivity.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention maintains continuous laminar flow through the mixing chamber, ensuring thorough mixing without intermittent high-shear pulses. The continuous laminar flow regime allows sufficient residence time for liquid-crystalline phase formation while maintaining mixing effectiveness, thereby reducing energy consumption compared to intermittent high-shear mixing.

Inventive Principle:
Principle #20Continuity of useful action

4Stability of the object's composition

If conventional stirrer designs are used, then mixing is achieved, but turbulence and cavitation forces prevent liquid-crystalline phase formation

Engineering Contradiction:
Improvemixing effectivenessVSAvoidturbulence and cavitation forces
Core Design Contradiction:
Stability of the object's compositionVSObject-generated harmful factors

Solution Approach 1:

The invention changes the flow regime parameter from turbulent to laminar flow by designing a specific mixing chamber geometry with controlled dimensions and a centrally positioned stirrer. This parameter change eliminates cavitation forces while maintaining continuous production capability, thereby reducing energy consumption without sacrificing productivity.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention divides the mixing chamber into distinct flow zones: a central mixing zone with laminar flow for thorough mixing, and peripheral zones that allow controlled flow transition. This segmentation enables effective mixing without generating harmful turbulence and cavitation forces, while providing the stable conditions necessary for liquid-crystalline phase formation.

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The device achieves efficient, energy-efficient production of emulsions and dispersions with a liquid-crystalline structure, minimizing energy consumption and maintaining a laminar flow to ensure thorough mixing and effective droplet breakup, resulting in a compact and cost-effective process.

Implementation Method 1

the components are mixed turbulently by the shear forces exerted by the stirrer units

Methodology Applied
Scientific EffectShear forces: Shear Stress

Implementation Method 2

the percolating mixing area in which the components are mixed further and the turbulent flow decreases

Methodology Applied
Scientific EffectTurbulent flow to laminar flow transition: Turbulence

Implementation Method 3

the viscosity increases, caused either by constant comminution of the droplets or by formation of liquid-crystalline phases

Methodology Applied
Scientific EffectViscosity increase: Viscoelasticity

Implementation Method 4

in which a lyotropic, liquid-crystalline phase is established in the mixture of the components

Methodology Applied
Scientific EffectLiquid-crystalline phase formation: Liquid Crystals

Implementation Method 5

Controlled and energy-efficient severing of the drops during the mixing process or the formation of liquid-crystalline phases then occurs in the laminar mixing area under conditions of elongational flow

Methodology Applied
Scientific EffectElongational flow: Laminar Flow

Data Source

PatentUS10610835B2Emulsification device for continuously producing emulsions and/or dispersions
Publication Date: 2020.04.07 CLARIANT INT LTD
  • US10610835B2 patent drawing
  • US10610835B2 patent drawing
  • US10610835B2 patent drawing

AI summary

The invention relates to an emulsification device for continuously producing emulsions, nano-emulsions, and/or dispersions having a liquid crystalline structure, comprising a) at least one mixing system, b) at least one drive for the stirring element, and c) at least one delivery unit for each component or each component mixture.