Encapsulated Water-Soluble Benefit Agents That Resist Emulsification Loss

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Solution Overview

Problem

Existing encapsulation processes for solid, water-soluble benefit agents, such as melamine formaldehyde and urea formaldehyde, fail to effectively encapsulate these agents due to dissolution during the emulsification step and interaction with encapsulating materials, leading to instability and loss of benefit in consumer products.

Innovation Solution

A process using cross-linked melamine formaldehyde and urea formaldehyde encapsulation that stabilizes solid, water-soluble benefit agents by forming particles with a shell material and a core material, including a protective suspension agent and an optional hydrophobic organic material, ensuring at least 75% of particles have a fracture strength of 0.1 MPa to 5 MPa, allowing for controlled release when the product is used.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If melamine formaldehyde or urea formaldehyde encapsulation process is used, then protection system is provided, but solid, water soluble benefit agents dissolve during emulsification step and interact with melamine or urea during polymerization

Engineering Contradiction:
Improveprotection systemVSAvoidstability of benefit agent
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The patent introduces a protective suspension agent as an intermediary substance that coats the solid, water-soluble benefit agent before encapsulation. This protective layer prevents the benefit agent from dissolving during the emulsification step and from interacting with melamine or urea during polymerization, thereby resolving the contradiction between providing protection and maintaining stability.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Reliability

If encapsulation process is used to protect benefit agents, then degradation is prevented, but benefit agents cannot be released when product is used

Engineering Contradiction:
Improveprotection against degradationVSAvoidrelease mechanism
Core Design Contradiction:
ReliabilityVSEase of operation

Solution Approach 1:

The patent modifies the encapsulation shell parameters by using cross-linked melamine formaldehyde or urea formaldehyde polymers with specific fracture strength characteristics. The shell is designed to be stable during storage but to fracture and release the benefit agent under specific usage conditions, thus resolving the contradiction between protection and release.

Inventive Principle:
Principle #35Parameter changes

3Reliability

If solid, water soluble benefit agents are encapsulated, then protection is provided, but dissolution during emulsification prevents effective encapsulation

Engineering Contradiction:
Improveencapsulation protectionVSAvoidencapsulation process
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent applies preliminary action by coating the solid, water-soluble benefit agent with a protective suspension agent before the encapsulation process begins. This pre-protection ensures that the benefit agent does not dissolve during subsequent emulsification steps, making the encapsulation process feasible and effective.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The encapsulation process results in stable consumer products that effectively release the majority of the solid, water-soluble benefit agent when needed, maintaining product performance and extending shelf life.

Implementation Method 1

a protective suspension agent that prevents the solid, water soluble benefit agent from dissolving during the emulsification step

Methodology Applied
Scientific EffectPhysical barrier formation: Adsorption

Implementation Method 2

cross-linked melamine formaldehyde and/or urea formaldehyde encapsulation, where a core material comprising a solid, water-soluble benefit agent and a protective suspension agent is coated with a shell material

Methodology Applied
Scientific EffectPolymerization: Photopolymerisation

Data Source

PatentUS20110245134A1encapsulates
Publication Date: 2011.10.06 PROCTER & GAMBLE CO
  • US20110245134A1 patent drawing
  • US20110245134A1 patent drawing
  • US20110245134A1 patent drawing

AI summary

The present application relates to encapsulated, solid, water soluble benefit agents and products comprising such encapsulates, as well as processes for making and using such encapsulates and products comprising such encapsulates. In one aspect, the present application relates to a melamine formaldehyde and/or urea formaldehyde encapsulation process that offers as solution to the dissolution of solid, water soluble benefit agents during the process's emulsification step.