Encapsulate Stability Using Cross-Linking Inhibitors

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Solution Overview

Problem

The challenge lies in manufacturing liquid consumer product compositions that include borate compounds and encapsulates with polyvinyl alcohol, as aggregation occurs due to cross-linking reactions, leading to poor stability, performance issues, and aesthetics problems.

Innovation Solution

Incorporating a cross-linking inhibitor, such as sorbitol, into the composition before combining the encapsulates and borate compounds to reduce hydrogen bonding and prevent aggregation, thereby maintaining the stability and performance of the product.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If borate compounds and encapsulates with polyvinyl alcohol are combined in liquid consumer product compositions, then enzyme stability and product functionality are improved, but aggregation occurs due to cross-linking reactions leading to poor stability and aesthetics

Engineering Contradiction:
Improveenzyme stabilityVSAvoidproduct stability
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

A cross-linking inhibitor is introduced as an intermediary substance that prevents direct interaction between borate compounds and polyvinyl alcohol. The inhibitor acts as a mediator that blocks the cross-linking reaction pathway, allowing borate and PVOH to coexist without aggregation while maintaining their individual functional benefits

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The harmful cross-linking reaction is extracted or removed from the system by adding a cross-linking inhibitor. This inhibitor selectively eliminates the aggregation mechanism while preserving the desired enzyme stability function of borate compounds and the encapsulate functionality

Inventive Principle:
Principle #2Taking out (Extraction)

2Adaptability or versatility

If borate compounds and encapsulates with polyvinyl alcohol are combined in liquid consumer product compositions, then product functionality is maintained, but aggregation leads to build-up on processing equipment and poor aesthetics

Engineering Contradiction:
Improveproduct functionalityVSAvoidprocessing ease
Core Design Contradiction:
Adaptability or versatilityVSEase of manufacture

Solution Approach 1:

The cross-linking inhibitor serves as a protective intermediary during manufacturing and processing. It prevents aggregation that would cause equipment build-up, thereby maintaining ease of manufacture while allowing the product to retain its full functionality in the final formulation

Inventive Principle:
Principle #24Intermediary (Mediator)

3Stability of the object's composition

If cross-linking inhibitor is added to prevent aggregation, then encapsulate stability and product aesthetics are improved, but additional formulation complexity is introduced

Engineering Contradiction:
Improveencapsulate stabilityVSAvoidformulation complexity
Core Design Contradiction:
Stability of the object's compositionVSDevice complexity

Solution Approach 1:

The formulation complexity is managed by treating the cross-linking inhibitor as a standard formulation parameter rather than a complex process requirement. By selecting inhibitors that can be easily incorporated into existing manufacturing workflows, the additional component becomes a simple parameter adjustment rather than a source of operational complexity

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The use of a cross-linking inhibitor effectively minimizes encapsulate aggregation, enhancing the stability and performance of the final product composition, ensuring consumer-acceptable aesthetics and functionality.

Implementation Method 1

cross-linking due to hydrogen bonding that can occur between hydroxyl groups (—OH) of the borate derivatives and hydroxyl groups of the polyvinyl alcohol

Methodology Applied
Scientific EffectHydrogen bonding:

Data Source

PatentUS10611988B2Methods for making encapsulate-containing product compositions
Publication Date: 2020.04.07 PROCTER & GAMBLE CO
  • US10611988B2 patent drawing
  • US10611988B2 patent drawing
  • US10611988B2 patent drawing

AI summary

Methods relating to making product compositions that include encapsulates and borate compounds, where the encapsulates include polyvinyl alcohol polymer. Compositions made from such methods. Encapsulate slurries.