Epitaxial Wafer Fabrication Reducing Surface Defects

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Solution Overview

Problem

The existing epitaxial wafer fabrication methods face challenges in reducing surface defect density due to lattice mismatch and growth defects, which affect the quality of epitaxial wafers, particularly in silicon carbide-based substrates.

Innovation Solution

A method involving a pre-growth step with a buffer layer formed at a higher temperature and lower growth speed, followed by a subsequent growth step at a lower temperature and higher speed, to reduce lattice mismatch and surface defects, with controlled C/Si ratio and flux of reactive gases, allowing for continuous epitaxial growth without interruption.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If a single-step epitaxial growth process is used, then the fabrication time is short, but the surface defect density is high due to lattice mismatch and growth defects

Engineering Contradiction:
Improvesurface defect densityVSAvoidfabrication time
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The single-step epitaxial growth process is divided into multiple sequential growth steps with different conditions. Each step targets specific defect reduction: initial growth at lower temperature for lattice matching, intermediate growth for defect elimination, and final growth for surface quality. This segmentation allows comprehensive defect control without excessive total fabrication time.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The method performs preliminary epitaxial growth under optimized conditions before final wafer completion. The initial growth steps prepare the crystal structure with proper lattice matching and defect reduction, creating a foundation that prevents subsequent defect formation during faster final growth stages.

Inventive Principle:
Principle #10Preliminary action

2Productivity

If high growth speed is used throughout the epitaxial process, then the fabrication time is reduced, but the surface defect density increases due to growth defects

Engineering Contradiction:
Improvegrowth speedVSAvoidsurface defect density
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The growth speed is dynamically adjusted throughout the epitaxial process rather than maintained at a constant high rate. The process starts with lower growth speeds for initial crystal formation and lattice matching, then progressively increases speed as the crystal structure stabilizes, achieving both high productivity and low defect density.

Inventive Principle:
Principle #15Dynamics

Solution Approach 2:

Multiple growth parameters including temperature, pressure, and growth speed are changed systematically across different growth steps. The method optimizes the combination of these parameters at each stage to balance growth speed and defect reduction, rather than prioritizing speed alone throughout the entire process.

Inventive Principle:
Principle #35Parameter changes

3Manufacturing precision

If low growth temperature is used, then the surface defect density is reduced, but the growth speed decreases

Engineering Contradiction:
Improvesurface defect densityVSAvoidgrowth speed
Core Design Contradiction:
Manufacturing precisionVSSpeed

Solution Approach 1:

The epitaxial growth process uses periodic alternation between different temperature regimes. Lower temperatures are applied periodically during critical initial stages for defect reduction, while higher temperatures are used in later stages to accelerate growth. This periodic temperature variation resolves the trade-off between precision and speed.

Inventive Principle:
Principle #19Periodic action

Solution Approach 2:

The method performs preliminary growth at lower temperatures to establish proper crystal structure and reduce surface defects before transitioning to higher temperature fast growth. This preliminary low-temperature action creates a defect-free foundation that allows subsequent high-speed growth without compromising surface quality.

Inventive Principle:
Principle #10Preliminary action

4Manufacturing precision

If multiple separate processing steps including polishing are used, then the surface quality is improved, but the fabrication complexity and time increase

Engineering Contradiction:
Improvesurface qualityVSAvoidfabrication process complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The method merges the epitaxial growth process with surface quality improvement functions that would traditionally require separate polishing steps. By optimizing growth conditions and sequences, the epitaxial layer is formed with inherently low defect density and high surface quality, eliminating or reducing the need for additional mechanical processing steps.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The epitaxial growth process itself is designed to produce high-quality surfaces without requiring external polishing operations. The controlled growth conditions and multi-step sequence enable the material to self-organize into a low-defect structure, making the process self-sufficient for surface quality improvement.

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach significantly reduces surface defect density to 0.5 or less per cm², enabling high-quality epitaxial wafers with reduced fabrication time and cost, and eliminates the need for separate polishing processes.

Implementation Method 1

a buffer layer being formed on the substrate in a pre-growth step

Methodology Applied
Scientific EffectEpitaxial growth: Epitaxy

Implementation Method 2

reduce lattice mismatch and surface defects

Methodology Applied
Scientific EffectLattice mismatch reduction:

Implementation Method 3

a gas/liquid/solid silicon composite is transferred to a surface of a single crystal silicon wafer (or substrate) to be thermally decomposed

Methodology Applied
Scientific EffectThermal decomposition: Pyrolysis

Implementation Method 4

an epitaxial wafer is fabricated by laminating silicon onto a single crystal silicon wafer through continuous growth of a single crystal structure

Methodology Applied
Scientific EffectEpitaxial growth: Epitaxy

Data Source

PatentEP2728610B1Method for fabricating an epitaxial wafer
Publication Date: 2020.03.18 LG INNOTEK CO LTD
  • EP2728610B1 patent drawingFigure 1(a)~1(c)
  • EP2728610B1 patent drawingFigure 2~3
  • EP2728610B1 patent drawingFigure 4~5

AI summary

Disclosed is an epitaxial wafer (300B) including a substrate (110), and an epitaxial structure (210B) disposed on the substrate (110), wherein the epitaxial structure (210B) includes a first epitaxial layer (212B), a second epitaxial layer (214B) disposed on the first epitaxial layer (212B), and a third epitaxial layer (216) disposed between the first epitaxial layer (212B) and the second epitaxial layer (214B), the third epitaxial layer (216) having a first doping concentration around a first boundary adjacent to the first epitaxial layer (212B) and a second doping concentration different from the first doping concentration around a second boundary adjacent to the second epitaxial layer (214B).