Two-Component Epoxy Premix for Structural Foam Injection Molding

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Solution Overview

Problem

Conventional expandable and curable epoxy resin mixtures for structural foams in metallic hollow structures face challenges with high viscosity and tackiness, limiting their use in injection molding and requiring costly modifications to equipment, which results in poor quality and high technical effort in production.

Innovation Solution

A two-component premix system is developed, where Component A contains isocyanate and Component B contains diol or polyol, along with epoxy prepolymers and heat-activatable hardeners and blowing agents, allowing for pre-curing at room temperature or above, reducing viscosity and enabling easier processing and improved storage stability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of operation

If conventional expandable and curable epoxy resin mixtures are used for structural foams, then structural integrity and expandability are maintained, but viscosity is high and tackiness is excessive, limiting use in injection molding

Engineering Contradiction:
ImproveprocessabilityVSAvoidviscosity
Core Design Contradiction:
Ease of operationVSStability of the object's composition

Solution Approach 1:

The epoxy resin mixture is divided into two separate components: Component A containing epoxy prepolymers and Component B containing polyol and isocyanate. This segmentation allows each component to be optimized independently, resulting in lower viscosity and reduced tackiness while maintaining the ability to form structural foams with high structural integrity when mixed and cured.

Inventive Principle:
Principle #1Segmentation

2Ease of manufacture

If conventional epoxy resin mixtures are used, then structural strength is achieved, but costly modifications to injection molding equipment are required

Engineering Contradiction:
Improveproduction costVSAvoidproduction quality
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

The invention changes the physical and chemical parameters of the epoxy system by using prepolymers with controlled molecular weight and functionality, along with specific polyol and isocyanate combinations. This results in a two-component system with optimized viscosity and reactivity, enabling standard injection molding equipment to be used without modifications while producing high-quality structural foam parts.

Inventive Principle:
Principle #35Parameter changes

3Manufacturing precision

If high viscosity epoxy mixtures are used, then structural foam integrity is maintained, but production requires high technical effort and results in poor quality

Engineering Contradiction:
Improvepart qualityVSAvoidtechnical effort
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The epoxy prepolymers are pre-synthesized with controlled molecular weight and functionality before use in the injection molding process. This preliminary preparation ensures that the components have optimal viscosity and reactivity characteristics, reducing the technical effort required during production and enabling consistent high-quality part manufacturing using standard equipment.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution allows for the production of dimensionally stable moldings that can be easily introduced into molds, reducing production costs and improving the quality of injection-molded parts by lowering viscosity and minimizing tackiness, while maintaining structural integrity and expandability.

Implementation Method 1

Pre-curing is based on the formation of a polyurethane from an alcohol component in the one component and from an isocyanate component in the other component of the premix

Methodology Applied
Scientific EffectPolyurethane formation reaction: Chemical Bonding

Implementation Method 2

Final curing to form a structural foam takes place later on heating, based on the heat-induced curing reaction of epoxy resin prepolymers

Methodology Applied
Scientific EffectHeat-induced curing reaction: Heating

Implementation Method 3

at least one of components A and B containing a heat-activatable blowing agent

Methodology Applied
Scientific EffectHeat-activatable blowing: Phase Change

Data Source

PatentUS9464153B2Premix and method for producing a thermally expandable and curable epoxy-based compound
Publication Date: 2016.10.11 HENKEL KGAA

AI summary

A two-component premix for preparing a heat-expandable and heat-curable epoxy-based material, comprises an isocyanate, a diol or polyol, an epoxy prepolymer, a heat-activatable hardener for epoxy prepolymers, and a heat-activatable blowing agent.