Etching Sulfur-Containing Thermoplastic Resin with Sulfoxide Moderators

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Solution Overview

Problem

Existing methods for etching sulfur-containing thermoplastic resin-substrates, such as PPS, often suffer from destructive etching, insufficient etching, or require harmful and sophisticated conditions, making them unsuitable for modern applications like 5G communication systems.

Innovation Solution

A method involving a liquid etching composition comprising a mineral acid (sulfuric acid or nitric acid) and a dialkyl sulfoxide or phenyl-comprising sulfoxide, which acts as an etching moderator, allowing for controlled etching under moderate conditions.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If common etching methods/compositions are used on sulfur-containing thermoplastic resin-substrates, then the resin-substrate maintains its chemical and thermal resistance, but the etching effectiveness is insufficient

Engineering Contradiction:
Improvechemical and thermal resistanceVSAvoidetching effectiveness
Core Design Contradiction:
ReliabilityVSManufacturing precision

Solution Approach 1:

The patent changes the chemical parameters of the etching composition by introducing a specific combination of mineral acid (sulfuric or nitric acid) with a sulfoxide compound. This parameter change enables effective etching of sulfur-containing thermoplastic resin-substrates while maintaining their inherent chemical and thermal resistance properties through controlled surface modification rather than complete material removal.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The sulfoxide compound acts as an intermediary substance that facilitates the etching process. It mediates between the mineral acid and the sulfur-containing thermoplastic resin-substrate, enabling effective interaction and surface modification without requiring excessive acid concentration or harsh conditions that would compromise the resin's resistance properties.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Manufacturing precision

If aggressive etching compositions are used to achieve sufficient etching, then etching effectiveness improves, but the etching becomes too destructive

Engineering Contradiction:
Improveetching effectivenessVSAvoiddestructive etching
Core Design Contradiction:
Manufacturing precisionVSObject-affected harmful factors

Solution Approach 1:

The patent modifies the etching composition parameters by combining mineral acid with a sulfoxide compound, which changes the etching mechanism from aggressive material removal to controlled surface modification. This parameter change achieves sufficient etching effectiveness while preventing destructive effects on the resin-substrate structure.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent converts the inherent sulfur content of the thermoplastic resin-substrate, which normally provides chemical resistance and prevents etching, into a benefit by using it as the active site for controlled surface modification. The sulfur in the resin substrate serves as both the protective element and the etching target, creating a beneficial balance between resistance and etchability.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

3Manufacturing precision

If traditional etching compositions are used, then etching can be achieved, but harmful substances and sophisticated conditions are required

Engineering Contradiction:
Improveetching capabilityVSAvoidharmful substances and process conditions
Core Design Contradiction:
Manufacturing precisionVSObject-affected harmful factors

Solution Approach 1:

The patent changes the chemical composition parameters by using mineral acid combined with a sulfoxide compound, which allows etching to proceed under moderate conditions without requiring harmful substances. The specific chemical combination enables effective etching through a different mechanism that avoids the need for excessive acid concentration, fluorine compounds, or other harmful agents.

Inventive Principle:
Principle #35Parameter changes

4Manufacturing precision

If fluoride-containing etching compositions are used, then etching effectiveness improves, but environmental and worker safety deteriorates

Engineering Contradiction:
Improveetching effectivenessVSAvoidenvironmental and worker safety
Core Design Contradiction:
Manufacturing precisionVSObject-affected harmful factors

Solution Approach 1:

The patent extracts and eliminates fluoride-containing substances from the etching composition while maintaining effective etching capability. By removing the harmful fluoride component and replacing it with a mineral acid-sulfoxide combination, the patent achieves the same etching effectiveness without the environmental and worker safety hazards associated with fluoride compounds.

Inventive Principle:
Principle #2Taking out (Extraction)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method achieves excellent etching results with a broad working window, is easy to handle, and is less detrimental to the environment and workers, while also being fluoride- and bifluoride-free.

Implementation Method 1

contacting with a liquid etching composition comprising (a) a mineral acid selected from the group consisting of sulfuric acid and nitric acid

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Implementation Method 2

a dialkyl sulfoxide and/or a phenyl-comprising sulfoxide, which acts as an etching moderator, allowing for controlled etching under moderate conditions

Methodology Applied
Scientific EffectChemical moderation: Chemical Bonding

Data Source

PatentUS20250171688A1Etching composition and method for etching at least one surface of a sulfur-containing thermoplastic resin-substrate
Publication Date: 2025.05.29 ATOTECH DEUT GMBH & CO KG

AI summary

The present invention relates to a method for etching at least one surface of a sulfur-containing thermoplastic resin-substrate, the method comprising the steps (A) to (C), wherein step (C) is an etching step including a contacting with a liquid etching composition. The liquid etching composition comprises (a) a mineral acid selected from the group consisting of sulfuric acid and nitric acid, and (b) a dialkyl sulfoxide and/or a phenyl-comprising sulfoxide.