Ethylene Copolymer Insulation with TAP Crosslinking

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Solution Overview

Problem

Existing ethylene/alpha-olefin copolymer compositions used in insulated electrical/optical conductors lack sufficient flexibility and heat/oxidative stability for medium-to-ultra-high voltage applications, leading to reduced performance over time due to embrittlement and oxidation.

Innovation Solution

A peroxide-curable ethylene copolymer composition comprising a crosslinkable ethylene/alpha-olefin copolymer, triallyl phosphate, and an organic peroxide, which is cured to form a crosslinked product with enhanced flexibility, heat stability, and reduced dissipation factor, suitable for use as a single or multilayer insulation in insulated electrical/optical conductors.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional ethylene/alpha-olefin copolymer compositions are used, then the material provides basic insulation properties, but the flexibility and heat/oxidative stability are insufficient for medium-to-ultra-high voltage applications

Engineering Contradiction:
Improveheat and oxidative stabilityVSAvoidflexibility
Core Design Contradiction:
ReliabilityVSAdaptability or versatility

Solution Approach 1:

The patent creates a composite crosslinked system by combining ethylene/alpha-olefin copolymer with triallyl phosphate crosslinking agent and peroxide initiator. This composite approach produces a network structure that simultaneously delivers enhanced heat/oxidative stability and maintains flexibility, resolving the contradiction between these two properties in medium-to-ultra-high voltage insulation applications

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The patent modifies the chemical structure and crosslinking density parameters of the polyolefin insulation material through controlled crosslinking reactions. By adjusting crosslinking agent content, peroxide concentration, and curing conditions, the material achieves optimal balance between flexibility and heat/oxidative stability for high-voltage applications

Inventive Principle:
Principle #35Parameter changes

2Temperature

If polyolefin coverings are exposed to heat for prolonged periods, then the material provides thermal resistance, but the flexibility is reduced and oxidation and embrittlement occur

Engineering Contradiction:
Improveheat resistanceVSAvoidservice life under heat exposure
Core Design Contradiction:
TemperatureVSDuration of action of stationary object

Solution Approach 1:

The patent converts the harmful effect of heat exposure that causes oxidation and embrittlement into a beneficial crosslinking process. The peroxide initiator decomposes under heat to generate radicals that crosslink the polymer chains, transforming thermal energy that would normally degrade the material into a mechanism that enhances its thermal stability and service life

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Solution Approach 2:

The patent applies crosslinking agents and initiators in advance during material fabrication, creating a pre-formed crosslinked network structure before the insulation is installed. This preliminary crosslinking action ensures the material is pre-conditioned to resist heat-induced oxidation and embrittlement throughout its service life

Inventive Principle:
Principle #10Preliminary action

3Reliability

If crosslinking is increased to improve heat stability, then the oxidative induction time increases, but the dissipation factor may worsen

Engineering Contradiction:
Improveoxidative induction timeVSAvoiddissipation factor
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent optimizes the chemical composition parameters including the type and concentration of crosslinking agent, peroxide initiator, and catalyst system to achieve the desired balance. By carefully controlling these parameters, the material attains high oxidative induction time while maintaining acceptable dissipation factor for electrical insulation performance

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The resulting crosslinked product exhibits improved tensile elongation retention, oxidative induction time, and reduced dissipation factor, ensuring enhanced performance and durability in high-voltage applications.

Implementation Method 1

a crosslinkable ethylene/alpha-olefin copolymer, triallyl phosphate, and an organic peroxide, which is cured to form a crosslinked product

Methodology Applied
Scientific EffectFree radical polymerization: Photopolymerisation

Implementation Method 2

copolymerizing ethylene and an olefin-functional comonomer

Methodology Applied
Scientific EffectCopolymerization: Chemical Bonding

Data Source

PatentUS11299613B2Ethylene-alpha-olefin copolymer-triallyl phosphate composition
Publication Date: 2022.04.12 DOW GLOBAL TECHNOLOGIES LLC

AI summary

A peroxide-curable ethylene copolymer composition comprising (A) a crosslinkable ethylene/alpha-olefin copolymer, (B) an effective amount of triallyl phosphate (TAP), (C) an organic peroxide; and, optionally, (D) a supplemental polymer; wherein the (A) crosslinkable ethylene/alpha-olefin copolymer is made by copolymerizing ethylene and an olefin-functional comonomer in the presence of a molecular catalyst useful therefor. Also provided are a cured product made from the composition, methods of making and using same, and articles containing same.