Multi-Effect Evaporation Tower for Condensed Water Purification

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Solution Overview

Problem

Existing short-flow processes for purified terephthalic acid (PTA) face challenges in purifying condensed water due to high energy consumption, high investment costs, and safety concerns related to the use of organic phases as extractants.

Innovation Solution

A novel tower-type water separation tower with low energy consumption, high efficiency, and intrinsic safety is introduced. This tower includes multiple evaporation units with a final-effect condensation unit connected to a vacuum pump, utilizing a pressure difference and gravity to facilitate the separation process without external heat sources for subsequent evaporation units.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If an extraction apparatus is used to purify condensed water, then the quality of condensed water is improved, but energy consumption increases

Engineering Contradiction:
Improvequality of condensed waterVSAvoidenergy consumption
Core Design Contradiction:
Manufacturing precisionVSUse of energy by moving object

Solution Approach 1:

The patent uses evaporation and condensation phase transitions to separate acetic acid and p-toluic acid from condensed water. The evaporation units heat the condensed water to vaporize water, and the condensation units cool the vapor to condense pure water, achieving purification without extraction solvents and with lower energy consumption compared to conventional extraction apparatus

Inventive Principle:
Principle #36Phase transitions

Solution Approach 2:

The purification system is segmented into multiple evaporation units and condensation units arranged in sequence. Each evaporation unit is paired with condensation units, creating a staged separation process that improves efficiency and reduces energy consumption by reusing heat across multiple stages

Inventive Principle:
Principle #1Segmentation

2Manufacturing precision

If an extraction apparatus is used to purify condensed water, then the quality of condensed water is improved, but investment cost increases

Engineering Contradiction:
Improvequality of condensed waterVSAvoidinvestment cost
Core Design Contradiction:
Manufacturing precisionVSEase of manufacture

Solution Approach 1:

The system uses self-service heat exchange where vapor from evaporation units directly provides heat to condensation units without requiring external extraction solvents or complex chemical treatment systems. This reduces equipment complexity and investment cost while achieving the same purification quality

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The patent changes the physical parameters (temperature and pressure) of the condensed water through controlled evaporation and condensation processes. By adjusting these parameters across multiple stages, the system achieves effective separation of contaminants without requiring expensive extraction apparatus

Inventive Principle:
Principle #35Parameter changes

3Manufacturing precision

If an extraction apparatus is used to purify condensed water, then the quality of condensed water is improved, but safety requirements increase

Engineering Contradiction:
Improvequality of condensed waterVSAvoidsafety
Core Design Contradiction:
Manufacturing precisionVSReliability

Solution Approach 1:

The patent extracts and removes the harmful organic phase (extraction solvent) from the purification process entirely. Instead of using extraction apparatus with organic solvents that pose safety risks, the system uses purely physical evaporation and condensation processes, eliminating safety concerns related to flammable or toxic chemicals

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The evaporation and condensation process operates in a controlled environment that avoids the use of reactive or hazardous substances. The system creates a safe operating atmosphere by relying on phase transitions of water itself rather than introducing potentially dangerous extraction chemicals

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

4Use of energy by moving object

If multiple effect evaporation units are used, then energy consumption is reduced, but device complexity increases

Engineering Contradiction:
Improveenergy consumptionVSAvoiddevice complexity
Core Design Contradiction:
Use of energy by moving objectVSDevice complexity

Solution Approach 1:

The patent employs a nested structure where multiple evaporation units and condensation units are arranged in a compact, integrated tower configuration. Each evaporation unit is paired with condensation units in a nested arrangement, allowing the system to achieve multi-stage heat recovery without proportionally increasing overall device complexity

Inventive Principle:
Principle #7Nested doll (Nesting)

Solution Approach 2:

The patent merges the evaporation and condensation functions into a single integrated purification tower. Multiple evaporation units and condensation units are combined in one structure with shared support systems, reducing the overall complexity compared to having separate standalone units for each stage

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution achieves efficient separation of water from contaminants like acetic acid and p-toluic acid, reducing energy consumption, investment costs, and safety risks while maintaining high product quality.

Implementation Method 1

evaporation units for purifying the condensed water are disposed in the tower body

Methodology Applied
Scientific EffectEvaporation: Evaporation

Implementation Method 2

a first heat exchange chamber, an upper portion of the first heat exchange chamber is provided with a first demister for demisting a vapor phase generated after heat exchange of the condensed water

Methodology Applied
Scientific EffectHeat exchange: Heat Exchanger

Implementation Method 3

a final-effect condensation unit is disposed below the evaporation units and connected with a vacuum pump

Methodology Applied
Scientific EffectCondensation: Condensation

Implementation Method 4

The first concentric-square-shaped apparatus is located between the second heat exchange chamber and the second demister to isolate the first-effect evaporation unit from the second-effect evaporation unit to cause a pressure difference between the two

Methodology Applied
Scientific EffectPressure difference: Pressure Gradient

Implementation Method 5

a final-effect condensation unit is disposed below the evaporation units and connected with a vacuum pump

Methodology Applied
Scientific EffectVacuum: Vacuum

Data Source

PatentUS12330086B2Separation tower and method for treating condensed water
Publication Date: 2025.06.17 TIANHUA INSTITUTE OF CHEMICAL MACHINERY AND AUTOMATION CO LTD
  • US12330086B2 patent drawing

AI summary

Provided are a separation tower and method for treating condensed water. In order to overcome the defects that an apparatus has high investment and energy consumption and requires high safety due to the need to use an organic phase as an extractant, the present disclosure provides a separation tower for treating condensed water. The water separation tower includes a tower body. Evaporation units for purifying the condensed water are disposed in the tower body. A final-effect condensation unit is disposed below the evaporation units and connected with a vacuum pump. The present disclosure has the following beneficial effects: 1) the gravity is used, thereby omitting an intermediate pump and saving the power cost and a matching control system; 2) a pressure difference between every two effect evaporation units is designed, and heat energy provided by a first-effect evaporation unit is continuously evaporated to achieve separation, so that subsequent effect evaporation units do not require external heat sources; and 3) the degree of integration is high, the sealing property is good, a vacuum is easy to realize, a subsequent vacuum system is small, the energy consumption is low, a device is small in occupied area, the construction and installation cost is low, and the operation is simple.