Fe-Co-Mn Oxide Catalyst for Selective CO2 Reduction

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Solution Overview

Problem

Conventional methods for chemically reducing CO2 to CO at high temperatures suffer from low selectivity, resulting in high methane production, which increases manufacturing costs and energy consumption.

Innovation Solution

A catalyst composed of a metal oxide with a specific formula, FexCoyMn(1-x-y)Oz, is used to selectively reduce CO2 to CO at lower temperatures, minimizing methane production and optimizing energy efficiency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Speed

If high temperature is used for CO2 reduction, then reaction rate is improved, but selectivity deteriorates and methane production increases

Engineering Contradiction:
Improvereaction rateVSAvoidselectivity
Core Design Contradiction:
SpeedVSManufacturing precision

Solution Approach 1:

The invention changes the temperature parameter from conventional high temperature (600°C) to low temperature (200-400°C) range, which fundamentally alters the reaction pathway selectivity. This parameter change enables the reverse water gas shift reaction to dominate over methanation, achieving high CO selectivity while maintaining acceptable reaction rates through the novel catalyst formulation.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention employs a composite catalyst system consisting of Fe-Co-Mn metal oxides with specific compositional ratios (Fe: 0.7-0.95, Co: 0.01-0.25, Mn: 0.04-0.30). This composite material synergistically combines the properties of different metal oxides to achieve both high activity at low temperatures and high selectivity for CO production, resolving the contradiction between reaction rate and selectivity.

Inventive Principle:
Principle #40Composite materials

2Quantity of substance

If conventional high temperature process is used, then CO production is achieved, but energy consumption and separation costs increase due to low selectivity

Engineering Contradiction:
ImproveCO productionVSAvoidenergy consumption
Core Design Contradiction:
Quantity of substanceVSLoss of energy

Solution Approach 1:

By changing the operating temperature parameter to 200-400°C, the invention reduces energy input requirements while simultaneously improving selectivity to CO. This eliminates the need for energy-intensive separation processes to remove methane, thereby reducing overall energy consumption while maintaining high CO production efficiency.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention converts the thermodynamic limitation that normally favors methanation at low temperatures into a benefit by using the novel Fe-Co-Mn catalyst. The catalyst modifies the reaction pathway so that low temperature operation, which would normally be harmful to reaction rate, actually becomes beneficial by suppressing methanation and enhancing CO selectivity through the reverse water gas shift reaction.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The catalyst efficiently converts CO2 to CO at temperatures below 300°C with high selectivity, reducing energy consumption and separation costs by minimizing methane formation.

Implementation Method 1

CO2 can be chemically reduced into CO using a reverse water gas shift reaction (e.g. H2+CO2→CO+H2O) with a heat of reaction of 41.2 kJ/mole

Methodology Applied
Scientific EffectReverse water gas shift reaction: Chemical Transport Reactions

Implementation Method 2

a methanation reaction also occurs between H2 and CO2. The methanation reaction (e.g. 4H2+CO2→CH4+2H2O) has a heat of reaction of −165 kJ/mole

Methodology Applied
Scientific EffectMethanation reaction: Chemical Transport Reactions

Data Source

PatentUS11981573B2Catalyst for selectively chemically reducing CO<sub>2 </sub>to form CO
Publication Date: 2024.05.14 IND TECH RES INST

AI summary

A method for selectively chemically reducing CO2 to form CO includes providing a catalyst, and contacting H2 and CO2 with the catalyst to chemically reduce CO2 to form CO. The catalyst includes a metal oxide having a chemical formula of FexCoyMn(1-x-y)Oz, in which 0.7≤x≤0.95, 0.01≤y≤0.25, and z is an oxidation coordination number.