Fe-Gradient Metal Magnetic Powder for Oxidation-Resistant Coil Cores

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Solution Overview

Problem

High Fe content in metal magnetic materials leads to oxidation during heat treatment, compromising magnetic properties, and existing methods struggle to balance high Fe content with oxidation inhibition.

Innovation Solution

Metal magnetic powder with a high Fe content at the center and low Fe content at the surface, combined with an oxide film, is produced by heat-treating a material powder with 90-99% Fe and easily oxidizable elements in a controlled oxygen atmosphere, creating a gradient that inhibits oxidation and maintains excellent magnetic properties.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If the content percentage of Fe in metal magnetic material is increased to obtain excellent magnetic properties, then magnetic properties are improved, but oxidation of Fe occurs more easily during heat treatment

Engineering Contradiction:
Improvemagnetic propertiesVSAvoidoxidation of Fe
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent applies local quality by creating a non-uniform Fe distribution within the metal magnetic grains, where the center part has high Fe content (98% by mass or higher) to ensure excellent magnetic properties, while the contour part near the surface has lower Fe content to inhibit oxidation. This spatial variation in composition allows simultaneous achievement of high magnetic performance and oxidation resistance.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent employs composite materials by combining Fe-rich metal phase with an oxide film covering the surface. The metal phase contains high Fe content at the center for magnetic properties, while the oxide film layer provides protection against oxidation. This composite structure integrates the advantages of both metallic Fe (magnetic properties) and oxide (oxidation resistance).

Inventive Principle:
Principle #40Composite materials

2Strength

If oxide layers are formed through heat treatment to bond grains together, then mechanical strength is improved, but Fe oxidation occurs which compromises magnetic properties

Engineering Contradiction:
Improvebonding strength between grainsVSAvoidmagnetic properties
Core Design Contradiction:
StrengthVSReliability

Solution Approach 1:

The patent applies local quality by creating a composition gradient where the contour part has lower Fe content that facilitates oxide layer formation for strong grain bonding, while the center part maintains high Fe content for excellent magnetic properties. This spatial differentiation allows oxide layers to form effectively for mechanical strength without significantly compromising the magnetic properties of the bulk material.

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The resulting metal magnetic powder effectively inhibits Fe oxidation, enabling the production of magnetic bodies with superior magnetic properties, allowing for higher current capacity and reduced size in coil components.

Implementation Method 1

heat-treating the material powder in an atmosphere of 5 to 10 ppm in oxygen concentration... an oxide film covering the metal phase

Methodology Applied
Scientific EffectOxidation: Oxidation

Implementation Method 2

raising its temperature to 850° C. at a rate of rise in temperature of 100° C./min or higher... heat-treating the material powder in the atmosphere at a temperature of 850° C. or above but below 1000° C.

Methodology Applied
Scientific EffectHeat treatment: Heat Treatment

Data Source

PatentUS11823825B2Metal magnetic powder and method for manufacturing same, as well as coil component and circuit board
Publication Date: 2023.11.21 TAIYO YUDEN KK
  • US11823825B2 patent drawing
  • US11823825B2 patent drawing
  • US11823825B2 patent drawing

AI summary

A metal magnetic powder is constituted by metal magnetic grains that each include: a metal phase where the percentage of Fe at its center part is 98 percent by mass or higher, while the mass percentage of Fe at its contour part is lower than that at the center part; and an oxide film covering the metal phase, so as to inhibit oxidation of Fe contained in the metal phase, despite the high content percentage of Fe in the metal phase.