Spectroscopic Analysis of Focused Ion Beam Induced Optical Emission

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Solution Overview

Problem

Focused ion beam induced optical emission (FIB-IOE) signals are challenging to analyze due to overlapping contributions from elemental, molecular, and bandgap emissions, making it difficult to identify the elemental composition of samples.

Innovation Solution

A method for spectroscopic analysis that identifies spectral peaks and determines their emission types based on the spectral resolution of the light collection system, allowing for the differentiation between elemental, molecular, and bandgap emissions, and subsequent identification of elemental composition using databases.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Loss of information

If FIB-IOE signals are collected from the sample, then additional compositional information is obtained, but the analysis becomes challenging due to overlapping emissions from multiple sources

Engineering Contradiction:
Improvecompositional informationVSAvoidsignal analysis difficulty
Core Design Contradiction:
Loss of informationVSDifficulty of detecting and measuring

Solution Approach 1:

The patent segments the complex FIB-IOE signal into distinct emission components (elemental, molecular, and bandgap emissions) by analyzing spectral peaks at different removal rates. This segmentation allows each emission type to be identified and analyzed separately, resolving the overlapping signal problem while preserving all compositional information.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent performs preliminary spectral analysis at multiple removal rates before final composition determination. By collecting and analyzing spectra at different ion beam removal rates, the method prepares and organizes the overlapping emission data in advance, making subsequent compositional analysis more straightforward and accurate.

Inventive Principle:
Principle #10Preliminary action

2Measurement precision

If spectral analysis is performed to identify emission types, then elemental composition can be determined, but the process requires differentiating between multiple overlapping emission sources

Engineering Contradiction:
Improveelemental composition identificationVSAvoidspectral analysis complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent changes the ion beam removal rate parameter to differentiate between emission types. By analyzing how spectral peaks behave at different removal rates, the method identifies which peaks correspond to elemental emissions (which persist), molecular emissions (which diminish), and bandgap emissions (which change characteristics), thereby simplifying the differentiation process while maintaining high measurement precision.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables accurate determination of elemental and molecular compositions by analyzing peak widths and comparing spectra with databases, effectively disentangling overlapping emission types in FIB-IOE signals.

Implementation Method 1

Focused ion beam induced optical emission (FIB-IOE) may provide additional information on sample composition

Methodology Applied
Scientific EffectFocused ion beam induced optical emission:

Implementation Method 2

accessing a spectrum of photons emitted from a sample responsive to irradiating the sample with an ion beam

Methodology Applied
Scientific EffectOptical emission detection:

Data Source

PatentUS20240369505A1Method and system for spectroscopic analysis
Publication Date: 2024.11.07 FEI CO
  • US20240369505A1 patent drawing
  • US20240369505A1 patent drawing
  • US20240369505A1 patent drawing

AI summary

Methods and systems for spectroscopic analysis of focused ion beam induced optical emission include accessing a spectrum acquired from a sample responsive to irradiating the sample with an ion beam and identifying the spectral peaks of the spectrum. The emission type of the spectral peak is determined based on a spectral resolution of a light collection system for collecting the spectrum. The emission types include elemental emission, molecular emission, and bandgap emission.