Fiber Pre-Coating with High-Melting Alloy for Uniform Metal Deposition

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Solution Overview

Problem

Existing methods for coating fibers with a metal alloy in the production of composite parts with a metal matrix face challenges such as incomplete wetting at high speeds, leading to uneven coating and the formation of undesirable alloy droplets, which hinder homogeneous distribution and strength of the composite.

Innovation Solution

A method involving a pre-coating with a second metal alloy having a higher melting temperature than the primary alloy, ensuring the fiber is well-wetted and coated uniformly, preventing droplet formation by translating the fiber through the second alloy at a visco-capillary speed, followed by cooling and subsequent coating with the primary alloy.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If the fiber is translated through the liquid alloy mass at high speed to maintain productivity, then the coating process remains efficient, but the contact time becomes too low for complete wetting, resulting in incomplete coating coverage and droplet formation

Engineering Contradiction:
Improvecoating speedVSAvoidcoating uniformity
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The invention applies a preliminary coating of a second alloy with higher melting temperature onto the fiber before the main coating process. This pre-coating layer modifies the surface properties of the fiber, enabling better wetting by the first alloy during high-speed passage through the liquid alloy mass, thus allowing both high productivity and uniform coating coverage

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The invention changes the temperature parameter by using an alloy with a higher melting temperature for the pre-coating step. This temperature parameter change allows the pre-coating layer to remain stable during the subsequent high-speed coating process, facilitating complete wetting and uniform coating formation even at high translation speeds

Inventive Principle:
Principle #35Parameter changes

2Productivity

If the fiber translation speed is increased to improve productivity, then more fibers can be coated per unit time, but the contact time decreases causing the fiber to remain at the periphery of the alloy mass and preventing complete penetration

Engineering Contradiction:
Improvecoating throughputVSAvoidcoating adhesion
Core Design Contradiction:
ProductivityVSStrength

Solution Approach 1:

The pre-coating with the second alloy is applied beforehand to create a surface that promotes complete penetration and adhesion of the first alloy during high-speed processing, ensuring strong coating strength even when translation speed is high

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The second alloy acts as an intermediary layer between the fiber and the first alloy. This intermediate layer facilitates complete wetting and penetration of the first alloy at high speeds, ensuring proper adhesion without requiring reduced translation speed

Inventive Principle:
Principle #24Intermediary (Mediator)

3Manufacturing precision

If vapor phase deposition or electrophoresis is used to deposit the alloy coating, then coating can be achieved, but the process complexity increases compared to the liquid route coating method

Engineering Contradiction:
Improvecoating deposit qualityVSAvoiddeposition system complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The invention uses a pre-coating step with a different alloy composition and temperature regime, then proceeds with liquid route coating. This parameter change approach achieves good coating quality through simplified liquid immersion and translation, avoiding the need for complex vapor phase or electrophoresis equipment

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables uniform and adherent coating of the primary alloy on the fiber even at high speeds, preventing droplet formation and enhancing the mechanical strength and adhesion of the composite.

Implementation Method 1

the carriage rate of the second alloy during this translation is in the visco-capillary domain, so that the fiber is covered, over this portion of its length, with a coating of the second alloy of thickness e2 non-zero over its entire periphery

Methodology Applied
Scientific EffectCapillary action: Capillary Action

Implementation Method 2

The coating of the second alloy is cooled until it becomes solid

Methodology Applied
Scientific EffectCooling and solidification: Freezing

Implementation Method 3

This second mass is heated above its temperature of fusion so that this second alloy is in the liquid state

Methodology Applied
Scientific EffectHeating and melting: Melting

Data Source

PatentEP2834382B1Method for coating a fibre with pre-coating
Publication Date: 2018.08.08 SAFRAN AIRCRAFT ENGINES SAS
  • EP2834382B1 patent drawingFigure 1~2
  • EP2834382B1 patent drawingFigure 3~4

AI summary

The invention concerns a method for depositing a coating of a first metal alloy on a fibre (10) extending in main direction D, comprising the following steps: (a) Providing a first mass (20) of a first metal alloy and heating the first mass (20) higher than the melting temperature of same so that said alloy is liquid and occupies space El, (b) Moving this fibre (10) from upstream to downstream through the first liquid mass (20) in the direction in which the fibre (10) extends at first speed VI such that the fibre (10) is covered, on at least one portion of the length of same, with a coating (25) of the first alloy of a non-zero thickness over the entire periphery of same in a plane perpendicular to main direction D. Before step (a), the following steps are carried out: (i) Providing a second mass (220) of a second metal alloy of which melting temperature TF2 is strictly higher than melting temperature TF1 of the first alloy, (j) Heating the second mass (220) higher than the melting temperature of same so that said second alloy is in the liquid state and occupies space E2, then moving the fibre (10) from upstream to downstream through the second alloy, this movement being carried out at second speed V2 which is such that the coating speed of the second alloy during this movement is in the visco-capillary range, such that the fibre (10) is covered on this portion of the length of same with a coating (225) of the second alloy of a non-zero thickness over the entire periphery of same, (k) Cooling this coating (225) until it becomes solid.